1,6,10-Dodecatrien-3-ol, 3,7,11-trimethyl-

Phase change data

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: Robert L. Brown and Stephen E. Stein

Reduced pressure boiling point

Tboil (K) Pressure (atm) Reference
387.20.001Aldrich Chemical Company Inc., 1990
385. to 387.0.001Frinton Laboratories Inc., 1986

Mass spectrum (electron ionization)

Go To: Top, Phase change data, Gas Chromatography, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin NIST Mass Spectrometry Data Center, 1994
NIST MS number 135322

All mass spectra in this site (plus many more) are available from the NIST/EPA/NIH Mass Spectral Library. Please see the following for information about the library and its accompanying search program.

Gas Chromatography

Go To: Top, Phase change data, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP Sil 8 CB1562.Schwob, Bessiere, et al., 200430. m/0.25 mm/0.25 μm, H2, 50. C @ 2. min, 3. K/min; Tend: 220. C
CapillaryDB-51566.Viña and Murillo, 200330. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 0.5 K/min, 250. C @ 10. min
CapillaryDB-11562.Mevy, Bessiere, et al., 2002He, 3. K/min; Column length: 25. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 220. C
CapillaryPTE-51570.Gudzic, Dordevic, et al., 200160. m/0.32 mm/0.39 μm, H2, 4.3 K/min; Tstart: 60. C; Tend: 285. C
CapillarySSP-11563.Nagarajan, Rao, et al., 200130. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 2. K/min, 250. C @ 5. min
CapillaryMethyl Silicone1539.Jayaprakasha, Rao, et al., 200030. m/0.32 mm/0.25 μm, He, 60. C @ 2. min, 2. K/min, 225. C @ 5. min
CapillaryMethyl Silicone1539.Adegoke, Rao, et al., 199830. m/0.32 mm/0.25 μm, He, 60. C @ 2. min, 2. K/min, 250. C @ 5. min
CapillaryDB-51565.Zoghbi, Andrade, et al., 199830. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillarySPB-11555.Jayaprakasha, Jaganmohan Rao, et al., 199730. m/0.32 mm/0.25 μm, He, 60. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryOV-1011555.Menut, Molangui, et al., 1995N2, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 200. C
CapillarySPB-11550.Wong and Tie, 1993He, 35. C @ 5. min, 3. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.20 mm
CapillaryBP-11552.Ekundayo, Laakso, et al., 1988H2, 65. C @ 2. min, 5. K/min; Column length: 50. m; Column diameter: 0.33 mm; Tend: 220. C
CapillaryOV-1011551.Yamaguchi and Shibamoto, 1981N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011552.Yamaguchi and Shibamoto, 1981N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Yamaguchi and Shibamoto, 1979N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011550.Yamaguchi and Shibamoto, 1979N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySPB-11553.Riu-Aumatell, Castellari, et al., 200430. m/0.25 mm/0.25 μm; Program: not specified

Kovats' RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySupelcowax1991.Riu-Aumatell, Castellari, et al., 200430. m/0.25 mm/0.25 μm, 60. C @ 5. min, 3. K/min, 240. C @ 10. min
CapillaryInnowax2030.Viña and Murillo, 200330. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 0.5 K/min, 250. C @ 10. min
CapillarySupelcowax-102053.Wong and Teng, 1994He, 35. C @ 5. min, 3. K/min, 200. C @ 20. min; Column length: 60. m; Column diameter: 0.25 mm
CapillarySupelcowax-102053.Wong and Tie, 1993He, 35. C @ 5. min, 3. K/min, 200. C @ 20. min; Column length: 60. m; Column diameter: 0.25 mm
CapillaryCarbowax 20M2009.Gaydou, Randriamiharisoa, et al., 198650. m/0.3 mm/0.15 μm, H2, 2. K/min; Tstart: 70. C; Tend: 210. C
CapillaryCarbowax 20M2000.Yamaguchi and Shibamoto, 1981N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C
CapillaryCarbowax 20M2000.Yamaguchi and Shibamoto, 1981N2, 2. K/min; Column length: 70. m; Column diameter: 0.28 mm; Tstart: 80. C; Tend: 200. C
CapillaryCarbowax 20M2021.Tressl, Friese, et al., 1978He, 2. K/min; Column length: 50. m; Column diameter: 0.28 mm; Tstart: 70. C; Tend: 190. C
CapillaryCarbowax 20M2020.Tressl, Friese, et al., 1978, 2He, 2. K/min; Column length: 50. m; Column diameter: 0.28 mm; Tstart: 70. C; Tend: 190. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-5MS1565.Cho, Namgung, et al., 200830. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min, 200. C @ 10. min
CapillaryZB-51564.Simoniatto, Bonani, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-51583.Batista-Pereira, Fernandes, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryDB-51583.Batista-Pereira, Fernandes, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryHP-5MS1571.Vujisic L., Vuckovic I., et al., 200630. m/0.25 mm/0.25 μm, H2, 4.3 K/min; Tstart: 50. C; Tend: 285. C
CapillaryHP-5MS1565.6Zhao C.X., Li, et al., 200630. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 80. C; Tend: 300. C
CapillaryDB-5MS1568.Seo and Baek, 200560. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 20. min; Tstart: 40. C
CapillarySE-301545.Tundis, Passalacqua, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 3. min, 16. K/min, 280. C @ 10. min
CapillaryHP-5MS1572.5Zhao, Liang, et al., 200530. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 80. C; Tend: 290. C
CapillaryHP-5MS1567.7Zhao, Liang, et al., 200530. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 80. C; Tend: 290. C
CapillaryHP-5MS1568.9Zhao, Liang, et al., 200530. m/0.25 mm/0.25 μm, He, 6. K/min; Tstart: 80. C; Tend: 290. C
CapillaryHP-51562.Javidnia, Miri, et al., 2004He, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 260. C
CapillaryRSL-2001568.Ngassoum, Ousmaila, et al., 200430. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillarySPB-51574.Rodríguez-Burruezo, Kollmannsberger, et al., 200430. m/0.53 mm/1.5 μm, He, 5. K/min; Tstart: 100. C; Tend: 250. C
CapillaryHP-5MS1565.Salido, Valenzuela, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-5MS1573.Yu, Kim, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 4. K/min, 200. C @ 20. min
CapillaryDB-5MS1562.Zheng, Kim, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 4. K/min, 200. C @ 20. min
CapillaryBP-11547.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryOV-11538.Bicchi, Rubiolo, et al., 200325. m/0.25 mm/0.3 μm, H2, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryHP-51564.Ngassapa, Runyoro, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51562.Aligiannis, Kalpoutzakis, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-5MS1565.Salido, Altarejos, et al., 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-51564.Alonzo, Bosco, et al., 200030. m/0.20 mm/0.25 μm, He, 60. C @ 8. min, 4. K/min, 180. C @ 2. min
CapillaryDB-51552.Bartley and Jacobs, 200060. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryHP-51561.Kim, Thuy, et al., 200030. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 200. C @ 20. min
CapillaryHP-51564.Kim, Thuy, et al., 200030. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 200. C @ 20. min
CapillaryHP-51560.Lazari, Skaltsa, et al., 200030. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryOV-1011554.Menut, Bessiere, et al., 2000N2, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 200. C
CapillaryDB-51533.Song, Sawamura, et al., 200030. m/0.25 mm/0.25 μm, N2, 2. K/min; Tstart: 70. C; Tend: 230. C
CapillaryHP-51561.Lazari, Skaltsa, et al., 199930. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-11575.Mirza and Sefidkon, 199960. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 220. C
CapillaryDB-11541.Muselli, Hoi, et al., 199930. m/0.25 mm/0.25 μm, 50. C @ 3. min, 3. K/min; Tend: 220. C
CapillaryDB-11566.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 3.5 K/min; Tend: 250. C
CapillaryDB-51562.Gómez, Ledbetter, et al., 1993He, 4. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 250. C
CapillaryOV-1011548.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryRSL-1501545.Sagrero-Nieves, de Pooter, et al., 198930. m/0.53 mm/1.2 μm, He, 3. K/min; Tstart: 30. C; Tend: 220. C
CapillaryOV-1011546.Pieribattesti, Smadja, et al., 1988H2, 2. K/min; Column length: 50. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C
CapillaryCP Sil 5 CB1544.Montanarella, Bos, et al., 1986N2, 4. K/min; Column length: 25. m; Column diameter: 0.22 mm; Tstart: 70. C; Tend: 295. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51559.Moon, Cliff, et al., 200630. m/0.32 mm/0.25 μm, He; Program: 40C(3min) => 3C/min => 180C => 10C/min => 260C(2min)
CapillaryDB-51539.Özel, Gögüs, et al., 2006Program: not specified
CapillaryDB-51563.Sampaio and Nogueira, 200630. m/0.25 mm/0.25 μm; Program: 40C(2min) => 4C/min => 220C => 20C/min => 280C
CapillaryDB-51550.Wang, Finn, et al., 200530. m/0.32 mm/1. μm, He; Program: 40C(2min) => 5C/min => 100C => 4C/min => 230C (10min)
CapillaryDB-5MS1569.Kim, Lee, et al., 200330. m/0.25 mm/0.25 μm, He; Program: 40C(5min) => 4C/min => 160C => 8C/min => 240C (15min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax2050.Cho, Namgung, et al., 200830. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min, 200. C @ 10. min
CapillaryDB-Wax2046.Aromdee and Sriubolmas, 200630. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min, 250. C @ 10. min
CapillaryDB-Wax2050.Cho, Choi, et al., 200660. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 4. K/min, 200. C @ 10. min
CapillaryZB-Wax2039.Ledauphin, Saint-Clair, et al., 200430. m/0.25 mm/0.15 μm, He, 35. C @ 5. min, 5. K/min, 220. C @ 10. min
CapillaryDB-Wax Etr2037.Ménager, Jost, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 3. min, 3. K/min, 245. C @ 20. min
CapillaryDB-Wax2024.Yu, Kim, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 4. K/min, 200. C @ 20. min
CapillaryDB-Wax2033.Zheng, Kim, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 4. K/min, 200. C @ 20. min
CapillaryBP-202031.Bianchini, Tomi, et al., 200350. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryCarbowax 20M2057.Bicchi, Rubiolo, et al., 200325. m/0.25 mm/0.3 μm, He, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryOV-3511991.Bonvehi and Coll, 200350. m/0.32 mm/0.2 μm, He, 5. K/min; Tstart: 60. C; Tend: 220. C
CapillaryHP-20M1991.Jerkovic, Mastelic, et al., 200350. m/0.2 mm/0.2 μm, He, 70. C @ 4. min, 4. K/min, 180. C @ 10. min
CapillarySupelcowax-102003.Chung, Yung, et al., 200260. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillarySupelcowax-102003.Chung, Yung, et al., 200160. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillaryDB-Wax2056.Bartley and Jacobs, 200060. m/0.5 mm/0.32 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryDB-Wax2041.Kim, Thuy, et al., 200030. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 200. C @ 20. min
CapillarySupelcowax-102044.Chung, 199960. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 2. K/min, 195. C @ 90. min
CapillaryDB-Wax2034.Cha, Kim, et al., 199860. m/0.25 mm/0.25 μm, 40. C @ 5. min, 3. K/min, 200. C @ 60. min
CapillaryDB-Wax2035.Möllenbeck, König, et al., 199725. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 4. K/min; Tend: 240. C
CapillaryDB-Wax2008.Stashenko, Prada, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2.5 K/min; Tend: 180. C
CapillaryDB-Wax2050.Shiratsuchi, Shimoda, et al., 199460. m/0.25 mm/0.25 μm, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillaryDB-Wax2050.Shiratsuchi, Shimoda, et al., 1994, 260. m/0.25 mm/0.25 μm, He, 2. K/min, 230. C @ 60. min; Tstart: 50. C
CapillaryCarbowax 20M2030.Chen and Ho, 1988He, 1.5 K/min, 225. C @ 80. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-Innowax2052.Carrer, Vanderlinde, et al., 2007He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C(8min) => 3C/min => 180C => 20C/min => 230C (20min)
CapillaryStabilwax2012.Wang, Finn, et al., 200530. m/0.32 mm/1. μm, He; Program: 40C(2min) => 5C/min => 100C => 4C/min => 230C (10min)
CapillaryStabilwax2045.Wang, Finn, et al., 200530. m/0.32 mm/1. μm, He; Program: 40C(2min) => 5C/min => 100C => 4C/min => 230C (10min)

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedSE-30175.1520.Thompson, Baker, et al., 1971N2, Chromosorb P (60-80 mesh); Column length: 3.2 m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1570.Zouari, Zouari, et al., 201030. m/0.25 mm/0.25 μm, Helium, 50. C @ 1. min, 7. K/min, 250. C @ 5. min
CapillaryHP-5 MS1608.Sarikurkcu, Tepe, et al., 200830. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51574.Chyau, Tsai, et al., 200760. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryBP-11544.Kiran, Devi, et al., 2007He, 5. K/min, 220. C @ 6. min; Tstart: 60. C
CapillaryHP-5 MS1566.Phutdhawong, Kawaree, et al., 200725. m/0.25 mm/0.25 μm, Helium, 100. C @ 3. min, 4. K/min, 280. C @ 5. min
CapillaryBPX-51578.Rali, Wossa, et al., 200750. m/0.22 mm/1. μm, He, 50. C @ 1. min, 4. K/min, 300. C @ 10. min
CapillaryDB-51556.Smelcerovic, Spiteller, et al., 200730. m/0.25 mm/0.25 μm, He, 10. K/min, 320. C @ 4. min; Tstart: 60. C
CapillarySPB-11545.Cavaleiro, Pinto, et al., 200630. m/0.20 mm/0.20 μm, Helium, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryDB-11548.Chen, Sheu, et al., 2006Nitrogen, 40. C @ 1. min, 2. K/min, 200. C @ 9. min; Column length: 60. m; Column diameter: 0.25 mm
CapillaryBP-11544.Kiran, Bhavani, et al., 2006Helium, 5. K/min, 220. C @ 6. min; Tstart: 60. C
CapillaryDB-51560.Ouamba, Ouabonzi, et al., 200625. m/0.25 mm/0.15 μm, N2, 50. C @ 3. min, 4. K/min; Tend: 200. C
CapillaryHP-51567.Potzernheim, Bizzo, et al., 200625. m/0.32 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51570.Sabulal, Dan, et al., 200630. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 60. C; Tend: 260. C
CapillaryDB-11548.Sawamura, Onishi, et al., 200660. m/0.25 mm/0.25 μm, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryMethyl Silicone1582.Tonzibo, Coffy, et al., 200625. m/0.3 mm/0.15 μm, N2, 50. C @ 5. min, 2. K/min; Tend: 210. C
CapillaryMethyl Silicone1559.Chalchat and Özcan, 2005He, 3. K/min; Column length: 60. m; Column diameter: 0.3 mm; Tstart: 50. C; Tend: 240. C
CapillaryBPX51567.Dickschat, Bode, et al., 200525. m/0.22 mm/0.25 μm, Helium, 50. C @ 5. min, 5. K/min; Tend: 320. C
CapillaryDB-51558.Ferraz, Limberger, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 3. min, 3. K/min; Tend: 300. C
CapillaryCP Sil 5 CB1566.Jassbi, Mehrdad, et al., 200530. m/0.25 mm/0.25 μm, N2, 5. K/min, 250. C @ 10. min; Tstart: 60. C
CapillaryHP-5MS1564.Tesevic, Nikicevic, et al., 200530. m/0.25 mm/0.25 μm, He, 4.3 K/min; Tstart: 60. C; Tend: 285. C
CapillaryHP-5 MS1569.Topçu, Barla, et al., 200530. m/0.25 mm/0.50 μm, He, 3. K/min, 260. C @ 20. min; Tstart: 60. C
CapillaryHP-5MS1561.Malencic, Couladis, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11540.Sarkhail, Amin, et al., 200430. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 2.5 K/min, 265. C @ 20. min
CapillaryHP-51564.Simic, Sokovic, et al., 200425. m/0.32 mm/0.52 μm, H2, 4. K/min; Tstart: 40. C; Tend: 240. C
CapillaryCP Sil 5 CB1561.Thappa, Bakshi, et al., 200420. m/0.25 mm/0.25 μm, He, 100. C @ 2. min, 8. K/min; Tend: 270. C
CapillaryMethyl Silicone1553.Jayaprakasha, Rao, et al., 200330. m/0.32 mm/0.25 μm, He, 60. C @ 2. min, 2. K/min, 250. C @ 5. min
CapillaryRSL-2001555.Jirovetz, Buchbauer, et al., 200330. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryCP Sil 5 CB1527.Taiwo and Bolanle, 200325. m/0.25 mm/0.15 μm, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryPTE-51564.Gudzic, Djokovic, et al., 200260. m/0.32 mm/0.30 μm, H2, 4.3 K/min; Tstart: 60. C; Tend: 285. C
CapillaryRSL-2001533.Jirovetz, Ngassoum, et al., 200230. m/0.32 mm/0.25 μm, H2, 50. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryOV-1011553.Kuiate, Bessière, et al., 2002He, 5. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C
CapillaryDB-51563.Merle, Blázquez, et al., 200225. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min, 280. C @ 5. min
CapillaryDB-51559.Schwob, Bessière, et al., 2002He, 3. K/min; Column length: 25. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 220. C
CapillaryDB-5MS1555.Cherchi, Deidda, et al., 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryRSL-2001548.Jirovetz L., Buchbauer G., et al., 200130. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryOV-1011548.Yang, 2001N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011548.Yang, 2001, 2N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryDB-51543.Mitiku, Sawamura, et al., 200030. m/0.22 mm/0.25 μm, N2, 70. C @ 2. min, 4. K/min, 230. C @ 20. min
CapillaryOV-1011553.Kuiate, Zollo, et al., 19995. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C
CapillaryOV-1011554.Zollo, Biyiti, et al., 19985. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 200. C
CapillaryCBP-11550.Zygadlo, Ariza-Espinar, et al., 1997He, 5. K/min; Column length: 25. m; Column diameter: 0.22 mm; Tstart: 60. C; Tend: 240. C
CapillaryOV-1011552.Chacko, Jayalekshmy, et al., 199650. m/0.25 mm/0.17 μm, N2, 5. K/min; Tstart: 50. C; Tend: 220. C
CapillaryDB-11554.Stashenko, Puertas, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2.5 K/min; Tend: 250. C
CapillaryHP-51578.Larsen and Frisvad, 199535. C @ 2. min, 6. K/min; Tend: 200. C
CapillaryOV-1011548.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryDB-11525.Velasco-Negueruela, Pérez Alonso, et al., 1991N2, 4. K/min; Column length: 30. m; Tstart: 80. C; Tend: 220. C
CapillaryOV-1011550.Yang and Sugisawa, 1990N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Yang and Sugisawa, 1990N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Sugisawa, Yamamoto, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Sugisawa, Yang, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011551.Sugisawa, Yang, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryTR-5 MS1556.Kurashov, Mitrukova, et al., 201415. m/0.25 mm/0.25 μm, Helium; Program: 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min)
Capillary5 % Phenyl methyl siloxane1568.Huang, Qin, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min)
CapillaryDB-5 MS1514.Zhu, Li, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2.8 min) 5.5 0C/min -> 140 0C (1 min) 4.5 oC/min -> 220 0C -> 225 0C (2 min) 3.4 0C/min -> 265 0C (5 min)
CapillaryDB-5 MS1558.Zhu, Li, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (2.8 min) 5.5 0C/min -> 140 0C (1 min) 4.5 oC/min -> 220 0C -> 225 0C (2 min) 3.4 0C/min -> 265 0C (5 min)
CapillaryHP-11541.Barra, Baldovini, et al., 200750. m/0.2 mm/0.33 μm, He; Program: 40C(2min) => 2C/min => 200C => 15C/min => 250C (30min)
CapillarySPB-11530.Borse, Rao, et al., 200730. m/0.25 mm/0.25 μm, Helium; Program: 35 0C (2 min) 1 0C/min -> 90 0C 3 0C/min -> 220 0C
CapillaryHP-51560.Dou, Li, et al., 200730. m/0.32 mm/0.25 μm, He; Program: 40 0C (2 min) 110 0C (2 min) 3 0C/min -> 170 0C (2 min) 4 0C/min -> 220 0C (2 min) 10 0C/min -> 260 0C (5 min)
CapillaryHP-51561.Liolios, Laouer, et al., 2007Program: not specified
CapillaryHP-5MS1564.Takaku, Haber, et al., 2007He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C
CapillarySPB-51564.Navickiene, Morandim, et al., 200630. m/0.25 mm/0.10 μm, Helium; Program: 40 0C (1 min) 10 0C/min -> 120 0C 0.5 0C/min -> 150 0C 20 0C/min -> 280 0C (5 min)
CapillaryHP-5 MS1565.Schmidt, Noletto, et al., 200630. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
CapillaryHP-5 MS1565.Schmidt, Noletto, et al., 200630. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
CapillarySE-541545.Souza, Souza, et al., 200625. m/0.25 mm/0.25 μm, Helium; Program: 110 0C 2 0C/min -> 160 0C 5 0C/min -> 290 0C (5 min)
CapillarySE-541562.Souza, Souza, et al., 200625. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryBPX51553.Dickschat, Bode, et al., 200525. m/0.22 mm/0.25 μm, Helium; Program: not specified
CapillaryBPX-51564.Judzentiene and Mockute, 200530. m/0.25 mm/0.25 μm; Program: 60C(0.2min) => 3K/min => 186C => 10C/min => 240C (5min)
CapillaryCP Sil 8 CB1539.Schwob, Bessière, et al., 2002, 2Program: not specified
CapillaryOV-1011551.Yang, 2001N2; Column length: 50. m; Column diameter: 0.25 mm; Program: not specified
CapillarySE-301553.Prikhod'ko, Klyuev, et al., 199930. m/0.25 mm/0.20 μm, Helium; Program: not specified
CapillaryDB-11547.Binder, Flath, et al., 1989Column length: 60. m; Column diameter: 0.32 mm; Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax1999.Zhao, Xu, et al., 200930. m/0.25 mm/0.25 μm, Helium, 40. C @ 2. min, 3. K/min, 230. C @ 5. min
CapillaryCP-Wax 52CB2034.Chyau, Tsai, et al., 200760. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryBP-202049.Rawat, Gulati, et al., 200730. m/0.25 mm/0.25 μm, He, 70. C @ 4. min, 4. K/min, 220. C @ 5. min
CapillaryCarbowax2048.Singh, Kumar, et al., 200760. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 40. C; Tend: 180. C
CapillarySupelcowax 102037.Cavaleiro, Pinto, et al., 200630. m/0.20 mm/0.20 μm, Helium, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryDB-Wax2039.Sawamura, Onishi, et al., 200660. m/0.25 mm/0.25 μm, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryStabilwax2003.Jirovetz, Buchbauer, et al., 200530. m/0.32 mm/0.5 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryStabilwax2003.Jirovetz, Buchbauer, et al., 2005, 230. m/0.32 mm/0.5 μm, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryPEG-20M2047.Yao, Guo, et al., 200560. C @ 10. min, 3. K/min, 180. C @ 30. min; Column length: 30. m; Column diameter: 0.25 mm
CapillaryDB-Wax2043.Lin, Cai, et al., 200330. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 3. K/min, 230. C @ 20. min
CapillaryDB-Wax2025.Tu, Onishi, et al., 200260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryStabilwax2002.Jirovetz L., Buchbauer G., et al., 200130. m/0.32 mm/0.25 μm, H2, 60. C @ 5. min, 10. K/min, 280. C @ 5. min
CapillaryCarbowax 20M1990.Vernin, Lageot, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 220. C
CapillaryDB-Wax2047.Paniandy, Chane-Ming, et al., 200060. m/0.32 mm/0.25 μm, Helium, 50. C @ 2. min, 5. K/min; Tend: 230. C
CapillaryDB-Wax2031.Ngassoum, Yonkeu, et al., 199960. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryNB-3512041.Onocha, Ekundayo, et al., 199925. m/0.3 mm/0.5 μm, H2, 70. C @ 2. min, 5. K/min; Tend: 250. C
CapillarySupelcowax-102044.Zygadlo, Ariza-Espinar, et al., 1997He, 3. K/min; Column length: 0. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 240. C
CapillaryDB-Wax2043.Stashenko, Puertas, et al., 199660. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 2.5 K/min; Tend: 180. C
CapillaryCarbowax 20M1991.Kawakami, Ganguly, et al., 199560. C @ 4. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 180. C
CapillaryPEG-20M2003.Togari, Kobayashi, et al., 199550. m/0.25 mm/0.15 μm, He, 60. C @ 4. min, 2. K/min; Tend: 180. C
CapillaryPEG-20M2005.Togari, Kobayashi, et al., 199550. m/0.25 mm/0.15 μm, He, 60. C @ 4. min, 2. K/min; Tend: 180. C
CapillaryCarbowax 20M1991.Kawakami, Kobayashi, et al., 1993He, 60. C @ 4. min, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tend: 180. C
CapillaryCarbowax 20M2005.Kawakami and Kobayashi, 1991He, 60. C @ 4. min, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tend: 180. C
CapillarySupelcowax-102056.Loughrin, Hamilton-Kemp, et al., 1990He, 60. C @ 1. min, 2. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tend: 220. C
CapillaryDB-Wax2034.Binder, Flath, et al., 198950. C @ 0.1 min, 4. K/min, 230. C @ 10. min; Column length: 60. m; Column diameter: 0.32 mm

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillarySupelco CO Wax-102065.Prompona, Kandylis, et al., 201260. m/0.32 mm/0.25 μm, Helium; Program: 35 0C (6 min) 2 0C/min -> 60 0C (5 min) 5 0C/min -> 200 0C 25 0C/min -> 250 0C (6 min)
CapillaryDB-Wax2039.Zhao, Xu, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryAquaWax2014.Liolios, Laouer, et al., 2007Program: not specified
CapillaryHP-Innowax2042.Piasenzotto, Gracco, et al., 200330. m/0.32 mm/0.5 μm, He; Program: 50C(4min) => 10C/min => 230C(10min) => 10C/min => 250C
CapillaryNukol2027.López and Dufour, 2001N2; Column length: 25. m; Column diameter: 0.25 mm; Program: 45C(5min) => 20C/min => 100C(1min) => 3C/min => 190C(40min)
CapillaryDB-Wax2044.Paniandy, Chane-Ming, et al., 200060. m/0.32 mm/0.25 μm, Helium; Program: not specified
CapillaryFFAP2034.Lambert, Demazeau, et al., 199930. m/0.32 mm/0.25 μm; Program: not specified
CapillarySupelcowax 102025.Castioni and Kapetanidis, 199660. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (10 min) 2 0C/min -> 80 0C 3 0C/min -> 100 0C 4 0C/min -> 220 0C (30 min)
CapillarySupelcowax 102020.Castioni and Kapetanidis, 199660. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillarySupelcowax 102033.Castioni and Kapetanidis, 199660. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryDB-Wax2037.Binder, Flath, et al., 1989Column length: 60. m; Column diameter: 0.32 mm; Program: not specified
CapillaryCarbowax 20M2000.Peppard and Ramus, 1988He; Program: not specified
CapillaryCarbowax 20M2020.Peppard and Ramus, 1988He; Program: not specified

References

Go To: Top, Phase change data, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Aldrich Chemical Company Inc., 1990
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Schwob, Bessiere, et al., 2004
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Notes

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