Bicyclogermacrene


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSRTX-1HP-5 MSHP-5 MSDB-5
Column length (m) 30.60.30.30.35.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.250.20
Phase thickness (μm) 0.250.250.250.250.10
Tstart (C) 60.60.80.40.50.
Tend (C) 230.230.240.250.200.
Heat rate (K/min) 3.2.4.3.4.
Initial hold (min)   3.1. 
Final hold (min)  5.10.3. 
I 1505.1494.1492.1532.1494.
ReferencePripdeevech and Saansoomchai, 2013Bendiabdellah, El Amine Dib, et al., 2012Dutra, Pittella, et al., 2012Jian-Yu, Zhu, et al., 2012Silva, Suzuki, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5 MSHP-1CP-Sil 5 CB
Column length (m) 35.35.30.30.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.200.200.250.250.25
Phase thickness (μm) 0.100.100.250.250.15
Tstart (C) 50.50.50.60.50.
Tend (C) 200.200.250.240.220.
Heat rate (K/min) 4.4.7.3. 
Initial hold (min)   1.  
Final hold (min)   5.  
I 1510.1511.1493.1496.1494.
ReferenceSilva, Suzuki, et al., 2012Silva, Suzuki, et al., 2012Zouari, Ayadi, et al., 2012Alizadeh, Khosh-Khui, et al., 2011Ameen, Usman, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 240.240.240.180.240.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min)     2.
Final hold (min)      
I 1495.1500.1495.1483.1500.
ReferenceAndrade, Cardoso, et al., 2011Bertoli, Lepnardi, et al., 2011Fraternale, Ricci, et al., 2011Hammami, Kamoun, et al., 2011Kahriman, Tosun, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-5ZB-5DB-5DB-5 MS
Column length (m) 30.30.30.30.60.
Carrier gas HeliumNitrogenNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.40.40.60.40.
Tend (C) 240.200.200.250.250.
Heat rate (K/min) 3.5.5.4.5.
Initial hold (min)  5.5.1.15.
Final hold (min)   5.10.15.
I 1494.1510.1512.1502.1504.
ReferenceKarimi, Farmani, et al., 2011Vazques, Aimar, et al., 2011Vazquez, Demmel, et al., 2011Yousefzadi, Heidari, et al., 2011Mesa-Arango, Betancur-Galvis, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5HP-5HP-5 MSHP-5
Column length (m)  30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHydrogen
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.40.50.100.70.
Tend (C) 220.260.240.220.290.
Heat rate (K/min) 5.4.3.2.5.
Initial hold (min) 10. 5.  
Final hold (min) 30.5.   
I 1490.1503.1499.1491.1507.
ReferenceMishra, Chaudhary, et al., 2010Miyazawa, Kawauchi, et al., 2010Monsef-Esfahani, Miri, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Radulovic, Dordevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5 MSDB-1-MSOV-101OV-101
Column length (m) 30.30.60.50.50.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.30.70.70.
Tend (C) 290.240.200.220.220.
Heat rate (K/min) 5.3.2.2.2.
Initial hold (min)   4.  
Final hold (min) 10. 35.  
I 1499.1494.1482.1491.1500.
ReferenceRadulovic, Dordevic, et al., 2010, 2Silva, Pott, et al., 2010Takeoka, Hobbs, et al., 2010Benites, Moiteiro, et al., 2009Benites, Moiteiro, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5 MSBPX-5DB-1DB-1
Column length (m) 30.30.7.560.60.
Carrier gas HeliumHeliumHeliumNitrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.100.250.25
Phase thickness (μm) 0.250.2510.0.250.25
Tstart (C) 50.40.60.60.60.
Tend (C) 250.250.240.250.250.
Heat rate (K/min) 2.4.3.4.4.
Initial hold (min) 5.2. 1.1.
Final hold (min)  2. 10.10.
I 1502.1503.1501.1501.1501.
ReferenceKoba, Sanda, et al., 2009Su, Wang, et al., 2009Shellie, 2008Ghasempour, Shirinpour, et al., 2007Reza, Ebrahim, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5HP-5
Column length (m) 30.30.25.25.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (μm) 0.250.250.530.530.53
Tstart (C) 50.40.40.40.40.
Tend (C) 250.250.280.280.280.
Heat rate (K/min) 3.5.4.4.4.
Initial hold (min) 5.2.   
Final hold (min)  5.   
I 1498.1486.1493.1495.1500.
ReferenceMirza, Navaei, et al., 2006N/AVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-1DB-5
Column length (m) 25.30.
Carrier gas HydrogenHelium
Substrate   
Column diameter (mm) 0.320.25
Phase thickness (μm) 0.300.25
Tstart (C) 50.60.
Tend (C) 200.240.
Heat rate (K/min) 3.3.
Initial hold (min) 1. 
Final hold (min) 10. 
I 1470.1495.
ReferenceBicchi, Binello, et al., 1999Tellez, Estell, et al., 1997
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pripdeevech and Saansoomchai, 2013
Pripdeevech, P.; Saansoomchai, J., Antibacterial activity and chemical composition of essential oil and various extracts of Fagraea fragrans Roxb. flowers, Chiang Mai J. Sci., 2013, 40, 2, 214-223. [all data]

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

Dutra, Pittella, et al., 2012
Dutra, R.C.; Pittella, F.; Dittz, D.; Marcon, R.; Pimenta, D.S.; Lopes, M.T.P.; Raposo, N.R.B., Chemical composition and cytotoxicity activity of the essential oil of Pterodon emarginatus, Braz. J. of Pharmacognosy, 2012, 22, 5, 971-978. [all data]

Jian-Yu, Zhu, et al., 2012
Jian-Yu, S.; Zhu, L.; Tian, Y.-J., Chemical composition and antimicrobial activities of essential oil of Matricaria songarica, Int. J. Agriculture Biology, 2012, 14, 1, 107-110. [all data]

Silva, Suzuki, et al., 2012
Silva, P.S.; Suzuki, E.Y.; Moreira, A.P.; Raposo, N.R.B.; Alves, T.M.A.; Viccini, L.F., Stachytarpheta gesnerioides Cham.: chemical composition of hexane fraction and essential oil, antioxidant and antimicrobial activities, Boletin Latinoamericano y del Caribe de Plantas Medicinales y Aromaticas, 2012, 11, 6, 542-548. [all data]

Zouari, Ayadi, et al., 2012
Zouari, N.; Ayadi, I.; Fakhfakh, N.; Rebai, A.; Zouari, S., Variations of chemical composition of essential oils in wild-populations of Thymus algeriensis Boiss et Reut., a North African endemic species, Lipids in Health and Desease, 2012, 11, 1, 28-39, https://doi.org/10.1186/1476-511X-11-28 . [all data]

Alizadeh, Khosh-Khui, et al., 2011
Alizadeh, A.; Khosh-Khui, M.; Javidnia, K.; Firuzi, O.; Jokar, S.M., Chemical composition of the essential oil, total phenolic content and antioxidant activity in Origanum maiorana L. (Lamiaceae) cultivated in Iran, Adv. Environ. Biol., 2011, 5, 8, 2326-2331. [all data]

Ameen, Usman, et al., 2011
Ameen, O.M.; Usman, L.A.; Oganija, F.S.; Hamid, A.A.; Muhammed, N.O.; Zubair, M.F.; Adebayo, S.A., Chemical composition of leaf essential oil of Annona senegalensis Pers. (Annonaceae) growing in North Central Nigeria, Int. J. Biol. Chem. Sci., 2011, 5, 1, 375-379. [all data]

Andrade, Cardoso, et al., 2011
Andrade, M.A.; Cardoso, M.G.; Batista, L.R.; Freire, J.M.; Nelson, D.L., Antimicrobial activity and chemical composition of essential oil of Pelargonium odoratissimum, Braz. J. Pharmacognosy, 2011, 21, 1, 47-52. [all data]

Bertoli, Lepnardi, et al., 2011
Bertoli, A.; Lepnardi, M.; Krzyzanowska, J.; Oleszek, W.; Pistelli, L., Mentha longifolia in vitro cultures as safe source of flavouring ingradients, Acta Biochem. Polonica, 2011, 58, 4, 581-587. [all data]

Fraternale, Ricci, et al., 2011
Fraternale, D.; Ricci, D.; Flamini, G.; Giomaro, G., Volatile profile of red apple from Marche region (Italy), Rec. Nat. Prod., 2011, 5, 3, 202-207. [all data]

Hammami, Kamoun, et al., 2011
Hammami, I.; Kamoun, N.; Rebai, A., Biocontrol of Botrytis cinerea with essential oil and methanol extract of Viola odorata flowers, Archives of Appl. Sci. Res., 2011, 3, 5, 44-51. [all data]

Kahriman, Tosun, et al., 2011
Kahriman, N.; Tosun, G.; Terzioglu, S.; Karaoglu, S.A.; Yayh, N., Chemical composition and antimicrobial activity of the essential oils from the flower, leaf, and stem of Senecio pandurifolis, Rec. Nat. Prod., 2011, 5, 2, 82-91. [all data]

Karimi, Farmani, et al., 2011
Karimi, H.; Farmani, A.; Nourizadeh, H., A performance comparison of modern statistical technique for molecular descriptor selection and retention prediction of essential oil from leaves, Amer. J. Sci. Res., 2011, 38, 36-40. [all data]

Vazques, Aimar, et al., 2011
Vazques, A.M.; Aimar, M.L.; Demmel, G.I.; Criado, S.G.; Ruiz, G.M.; Cantero, J.J.; Rossi, L.I.; Velasco, M.I., Determination of volatile organic compounds of Tagetes argentina Cabrera (asteraceae) using HS-SPME analysis, Boletin Latinoamericano y del Caribe Plantas Medicinales y Aromaticas, 2011, 10, 5, 463-469. [all data]

Vazquez, Demmel, et al., 2011
Vazquez, A.M.; Demmel, G.I.; Criado, S.G.; Aimar, M.L.; Cantero, J.; Rossi, L.I.; Velasco, M.I., Phytochemistry of TAgetes minuta L. (Asteraceae) from Cordoba, Argentina: comparative study between essential oil and HS-SPME analyses, Boletin Latinoamericano y del Caribe Plantas Medicinales y Aromaticas, 2011, 10, 4, 351-362. [all data]

Yousefzadi, Heidari, et al., 2011
Yousefzadi, M.; Heidari, M.; Akbarpour, M.; Mirjalili, M.H.; Zainali, A.; Parsa, M., in vitro cytotoxic activity of the essential oil of Dorema ammoniacum D. Don., Middle-East J. Sci. Res., 2011, 7, 4, 511-514. [all data]

Mesa-Arango, Betancur-Galvis, et al., 2010
Mesa-Arango, A.C.; Betancur-Galvis, L.; Montiel, J.; Bueno, J.G.; Baena, A.; Duran, D.C.; Martinez, J.R.; Stashenko, E.E., Antifungal activity and chemical composition of the essential oils of Lippia alba (Miller) N.E. Brown grown in different regions of Colombia, J. Essential Oil Res., 2010, 22, 6, 568-574, https://doi.org/10.1080/10412905.2010.9700402 . [all data]

Mishra, Chaudhary, et al., 2010
Mishra, R.K.; Chaudhary, S.; Pandey, R.; Gupta, S.; Mallavarapu, G.R.; Kumar, S., Analysis of linalool content in the inflorescence (flower) essential oil and leaf oil of Lippia alba cultivar Kavach, J. Essen. Oil Res., 2010, 22, 1, 3-7, https://doi.org/10.1080/10412905.2010.9700253 . [all data]

Miyazawa, Kawauchi, et al., 2010
Miyazawa, M.; Kawauchi, Y.; Utsumi, Y.; Takahashi, T., Character impact odorants of wild edible plant - Cacalia hastata L. var. orientalis - used in Japanese traditional food, J. Oleo Sci., 2010, 59, 10, 527-533, https://doi.org/10.5650/jos.59.527 . [all data]

Monsef-Esfahani, Miri, et al., 2010
Monsef-Esfahani, H.R.; Miri, A.; Amini, M.; Amanzadeh, Y.; Hadjiakhoondi, A.; Hajiaghaee, R.; Ajani, Y., Seasonal variations in the chemical composition, antioxidant activity and total phenolic content of Teucrium persicum Boiss. essential oils, Res. J. Biol. Sci., 2010, 5, 7, 492-498, https://doi.org/10.3923/rjbsci.2010.492.498 . [all data]

Pripdeevech, Chumpolsri, et al., 2010
Pripdeevech, P.; Chumpolsri, W.; Suttiarporn, P.; Wongpornchai, S., The chemical composition and antioxidant activities of Basil from Thailand using retention indices and comprehensive two-dimensional gas chromatography, J. Seb. Chem. Soc., 2010, 75, 11, 1503-1513, https://doi.org/10.2298/JSC100203125P . [all data]

Radulovic, Dordevic, et al., 2010
Radulovic, N.S.; Dordevic, N.D.; Palic, R.M., Volatiles of Pleurospermum austriacum (L.) Hoffm. (Apiaceae), J. Serbian Chem. Soc., 2010, 75, 12, 1-11, https://doi.org/10.2298/JSC100323127R . [all data]

Radulovic, Dordevic, et al., 2010, 2
Radulovic, N.; Dordevic, N.; Markovic, M.; Palic, R., Volatile constituents of Glechoma Hirsuta Waldst. Kit. and G. Hederacea L. (Lamiaceae), Bull. Chem. Soc. Ethiop., 2010, 24, 1, 67-76, https://doi.org/10.4314/bcse.v24i1.52962 . [all data]

Silva, Pott, et al., 2010
Silva, D.B.; Pott, A.; Oliveira, D.C.R., Analyses of the headspace volatile constituents of aerial parts (leaves and stems), flowers and fruits of Bidens gardneri Bak. and Bidens sulphurea (Cav.) Sch. Bip. using solid-phase microextraction, J. Essen. Oil Res., 2010, 22, 6, 560-563, https://doi.org/10.1080/10412905.2010.9700400 . [all data]

Takeoka, Hobbs, et al., 2010
Takeoka, G.R.; Hobbs, C.; Byeoung-Soo, P., Volatile constituents of the aerial parts of Salvia apiana Jepson, J. Essential Oil. Res., 2010, 22, 3, 241-244, https://doi.org/10.1080/10412905.2010.9700314 . [all data]

Benites, Moiteiro, et al., 2009
Benites, J.; Moiteiro, C.; Miguel, G.; Rojo, L.; Lopez, J.; Venancio, F.; Ramalho, L.; Feio, S.; Dandlen, S.; Casanova, H.; Torres, I., Composition and biological activity of the essential oil of Peruvial Lantana camara, J. Chilean Chem. Soc., 2009, 54, 4, 379-384, https://doi.org/10.4067/S0717-97072009000400012 . [all data]

Koba, Sanda, et al., 2009
Koba, K.; Sanda, K.; Guyon, C.; Raynaud, C.; Chaumont, J.-P.; Nicod, L., In vitro cytotoxic activity of Cymbopogon citratus L. and Cymbopogon nardus L. essential oils from Togo, J. Bangladesh Pharmacological Soc., 2009, 4, 29-34. [all data]

Su, Wang, et al., 2009
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Shellie, 2008
Shellie, R.A., Comprehensive 2D GC-QPMS with differential flow modulation, LV-GC, 2008, 11, 7-18. [all data]

Ghasempour, Shirinpour, et al., 2007
Ghasempour, H.R.; Shirinpour, E.; Heidari, H., The constituents of essential oils of Ferulago angulata (Schlecht.) Boiss at two different habitats, Nevakoh and Shahoo, Agross mountain, Western Iran, Iranian J. Sci. Technol., 2007, 31, A3, 309-312. [all data]

Reza, Ebrahim, et al., 2007
Reza, G.H.; Ebrahim, S.; Hossein, H., Analysis by gas chromatography - mass spectrometry of essential oil from seeds and aerial parts of Ferulago angulata (Schlecht.) Boiss gatheres in Nevakoh and Shahoo, Zagross mountain, west of Iran, Pakistan J. Biol. Sci., 2007, 10, 5, 814-817, https://doi.org/10.3923/pjbs.2007.814.817 . [all data]

Mirza, Navaei, et al., 2006
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Velickovic, Ristic, et al., 2003
Velickovic, A.S.; Ristic, M.S.; Velickovic, D.T.; Ilic, S.; Mitic, N.D., The possibilities of the application of some species of sage (Salvia L.) as auxiliaries in the treatment of some diseases, J. Serb. Chem. Soc., 2003, 68, 6, 435-445, https://doi.org/10.2298/JSC0306435V . [all data]

Bicchi, Binello, et al., 1999
Bicchi, C.; Binello, A.; D'Amato, A.; Rubiolo, P., Reliability of Van den Dool retention indices in the analysis of essential oils, J. Chromatogr. Sci., 1999, 37, 8, 288-294, https://doi.org/10.1093/chromsci/37.8.288 . [all data]

Tellez, Estell, et al., 1997
Tellez, M.R.; Estell, R.E.; Frederickson, E.L.; Havstad, K.M., Essntial oil of Flourensia cernua DC, J. Essent. Oil Res., 1997, 9, 6, 619-624, https://doi.org/10.1080/10412905.1997.9700799 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References