1H-Cycloprop[e]azulen-7-ol, decahydro-1,1,7-trimethyl-4-methylene-, [1ar-(1aα,4aα,7β,7aβ,7bα)]-

Formula: C₁₅H₂₄O
Molecular weight: 220.3505
IUPAC Standard InChI: InChI=1S/C15H24O/c1-9-5-6-11-13(14(11,2)3)12-10(9)7-8-15(12,4)16/h10-13,16H,1,5-8H2,2-4H3/t10?,11?,12?,13?,15-/m1/s1
IUPAC Standard InChIKey: FRMCCTDTYSRUBE-OUZJWQAESA-N
CAS Registry Number: 6750-60-3
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
Other names: (1aR,4aR,7S,7aR,7bR)-1,1,7-Trimethyl-4-methylenedecahydro-1H-cyclopropa[e]azulen-7-ol; Spathulenol; 1,1,7-Trimethyl-4-methylenedecahydro-1H-cyclopropa[e]azulen-7-ol-, (1aR-(1aα,4aα,7β,7aβ,7bα))-; (+)-Spathulenol; Espatulenol; Spatulenol
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Information on this page:
Other data available:
- Mass spectrum (electron ionization)
- Gas Chromatography
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Normal alkane RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	RTX-1	HP-5 MS	HP-5 MS	DB-5
Column length (m)	30.	60.	30.	30.	35.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.10
T_start (C)	60.	60.	80.	40.	50.
T_end (C)	240.	230.	240.	250.	200.
Heat rate (K/min)	3.	2.	4.	3.	4.
Initial hold (min)			3.	1.
Final hold (min)		5.	10.	3.
I	1578.	1572.	1570.	1578.	1576.
Reference	Rodriques, Amorim, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Dutra, Pittella, et al., 2012	Jian-Yu, Zhu, et al., 2012	Silva, Suzuki, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5 MS	HP-5 MS	HP-5	DB-1
Column length (m)	35.	30.	30.	30.	30.
Carrier gas	Helium		Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.10	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	50.	60.	40.
T_end (C)	200.	300.	250.	240.	210.
Heat rate (K/min)	4.	15.	7.	3.	5.
Initial hold (min)		2.	1.
Final hold (min)		10.	5.
I	1598.	1572.	1578.	1578.	1578.
Reference	Silva, Suzuki, et al., 2012	Xu, Han, et al., 2012	Zouari, Ayadi, et al., 2012	Bertoli, Lepnardi, et al., 2011	Fathi, Sahari, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	ZB-5	ZB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	40.	40.	60.
T_end (C)	180.	240.	200.	200.	250.
Heat rate (K/min)	2.	3.	5.	5.	4.
Initial hold (min)			5.	5.	1.
Final hold (min)				5.	10.
I	1575.	1576.	1548.	1548.	1576.
Reference	Hammami, Kamoun, et al., 2011	Karimi, Farmani, et al., 2011	Vazques, Aimar, et al., 2011	Vazquez, Demmel, et al., 2011	Yousefzadi, Heidari, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	SPB-1	HP-5 MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.252	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	70.	60.
T_end (C)	240.	250.	250.	290.	240.
Heat rate (K/min)	3.	2.	5.	5.	3.
Initial hold (min)			3.
Final hold (min)			15.
I	1574.	1578.	1563.	1585.	1576.
Reference	Cavar, Maksimovic, et al., 2010	Ho, Wang, et al., 2010	Lazarevic, Palic, et al., 2010	Lazarevic, Radulovic, et al., 2010	Magalhaes, Lima, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	DB-1	DB-1	BP-1	HP-5 MS
Column length (m)	60.	60.	25.		30.
Carrier gas	Helium	Nitrogen	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25		0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	250.	250.	250.	220.	220.
Heat rate (K/min)	5.	5.	4.	5.	5.
Initial hold (min)	15.		1.	10.	10.
Final hold (min)	15.		10.	30.
I	1590.	1563.	1574.	1569.	1577.
Reference	Mesa-Arango, Betancur-Galvis, et al., 2010	Meshkatalsadat, Safaei-Ghomi. J., et al., 2010	Mirjalili, Salehi, et al., 2010	Mishra, Chaudhary, et al., 2010	Ogunwande, Flamini, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	HP-5	HP-5 MS	DB-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Helium	Helium	Hydrogen	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	100.	70.	70.	70.	60.
T_end (C)	220.	290.	290.	290.	250.
Heat rate (K/min)	2.	5.	5.	5.	4.
Initial hold (min)					1.
Final hold (min)		10.		10.	10.
I	1573.	1586.	1587.	1581.	1570.
Reference	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Blagojevic, et al., 2010	Radulovic, Dordevic, et al., 2010	Radulovic, Dordevic, et al., 2010, 2	Safaei-Ghomi, Meshkatalsadat, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5 MS	DB-5	DB-1	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	50.	50.
T_end (C)	240.	240.	240.	220.	250.
Heat rate (K/min)	3.	3.	3.	4.	7.
Initial hold (min)			1.	2.	1.
Final hold (min)				2.	5.
I	1577.	1572.	1567.	1580.	1593.
Reference	Scherer, Wagner, et al., 2010	Silva, Pott, et al., 2010	de Souza, Lopes, et al., 2010	Xu, Tang, et al., 2010	Zouari, Zouari, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	VF-1 MS	HP-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	60.	35.	70.	60.	60.
T_end (C)	240.	220.	240.	280.	240.
Heat rate (K/min)	3.	3.	5.	4.	3.
Initial hold (min)				5.
Final hold (min)		40.		10.	7.
I	1578.	1563.	1572.	1569.	1586.
Reference	Alim, Goze, et al., 2009	El-Massry, El-Ghorab, et al., 2009	Lawal and Oyedelji, 2009	Marchesini, Prada, et al., 2009	Maridass, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	OV-1	DB-5	DB-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	45.	40.
T_end (C)	230.	230.	300.	250.	250.
Heat rate (K/min)	2.	2.	4.	3.	3.
Initial hold (min)			2.	3.	1.
Final hold (min)	30.	30.	10.	5.	10.
I	1560.	1572.	1542.	1589.	1576.
Reference	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Nibret and Wink, 2009	Porto, Decorti, et al., 2009	Rahimi-Nasrabadi, Gholivand, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5MS	HP-5 MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Nitrogen	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	40.	60.	40.	50.	60.
T_end (C)	230.	220.	240.	240.	300.
Heat rate (K/min)	2.	5.	3.	5.	15.
Initial hold (min)		3.	1.		2.
Final hold (min)		5.			10.
I	1580.	1578.	1567.	1576.	1572.
Reference	Scrivanti, Anton, et al., 2009	Shafaghat and Sadeghi, 2009	de Souza, Lopes, et al., 2009	Wannes, Mhamdi, et al., 2009	Xu, Han, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-5	Ultra 2	DB-5
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	Helium		Nitrogen	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.22
Phase thickness (μm)	0.25		0.25	0.11	0.25
T_start (C)	50.	60.	50.	60.	50.
T_end (C)	280.	280.	280.	230.	300.
Heat rate (K/min)	9.	3.	5.	2.	6.5
Initial hold (min)	3.		1.	5.	2.
Final hold (min)	3.		1.	30.	7.
I	1576.	1577.	1599.	1576.	1617.
Reference	Aicha, Ines, et al., 2008	Baziou, Couladis, et al., 2008	Bousaada, Ammar, et al., 2008	Byun and Shin, 2008	Chieng, Assim, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-52	VF-5MS	HP-5	SLB-5 MS	ZB-1
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	240.	100.	50.	45.
T_end (C)	280.	320.	240.	250.	230.
Heat rate (K/min)	3.	20.	5.	3.	3.
Initial hold (min)		1.	2.	2.
Final hold (min)	20.		5.	10.
I	1590.	1588.	1576.	1580.	1561.
Reference	Djarri, Medjroubi, et al., 2008	Kowalski, 2008	Lago, Romoff, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	RTX-1	HP-5 MS	BPX-5	HP-5
Column length (m)	30.	60.	30.	7.5	25.
Carrier gas	Helium	He	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.10	0.25
Phase thickness (μm)	0.25	0.25	0.25	10.	0.25
T_start (C)	50.	60.	50.	60.	60.
T_end (C)	300.	230.	240.	240.	240.
Heat rate (K/min)	5.	2.	3.	3.	4.
Initial hold (min)	5.				2.
Final hold (min)	5.	35.
I	1572.	1563.	1624.	1580.	1577.
Reference	Noudogbessi, Yedomonhan, et al., 2008	Paolini, Tomi, et al., 2008	Sarikurkcu, Tepe, et al., 2008	Shellie, 2008	Verdian-rizi, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-5MS	HP-5MS	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Nitrogen	He	He	He
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.32	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	250.	220.	240.	240.	280.
Heat rate (K/min)	5.	5.	3.	3.	3.
Initial hold (min)	30.	3.
Final hold (min)		5.
I	1575.	1589.	1577.	1597.	1562.
Reference	Yassa and Akhani, 2008	Amiri, 2007	Andrade, Oliveira, et al., 2007	Argyropoulou, Daferera, et al., 2007	Basta, Pavlovic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	HP-5MS	HP-5 MS	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.26	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	240.	280.	280.	240.
Heat rate (K/min)	3.	3.	3.	4.	3.
Initial hold (min)				5.
Final hold (min)
I	1557.	1574.	1576.	1578.	1578.
Reference	Basta, Tzakou, et al., 2007	Bos, Woerdenbag, et al., 2007	Bozin B., Mlmica-Dukic N., et al., 2007	Capetanos, Saroglou, et al., 2007	Da Silva J.K.R., Sousa P.J.C., et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5MS	DB-1	5 % Phenyl methyl siloxane
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	Helium	He	Nitrogen	He
Substrate
Column diameter (mm)	0.26	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.26	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	90.
T_end (C)	290.	240.	250.	250.	225.
Heat rate (K/min)	3.	4.	2.	4.	3.
Initial hold (min)		2.	8.	1.
Final hold (min)		20.	15.	10.	15.
I	1574.	1583.	1574.	1576.	1578.
Reference	Elfami, Bos, et al., 2007	Farsam, Amanlou, et al., 2007	Ferhat, Tigrine-Kordjani, et al., 2007	Ghasempour, Shirinpour, et al., 2007	Gil A., Van Baren C.M., et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Col-Elite 5MS	HP-1	BP-1	DB-5	AT-5
Column length (m)	30.	30.		30.	60.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	30.	60.	60.	60.	60.
T_end (C)	246.	240.	220.	300.	260.
Heat rate (K/min)	3.	2.	5.	3.	4.
Initial hold (min)
Final hold (min)		20.	6.
I	1598.	1577.	1564.	1566.	1580.
Reference	Gudaityte and Venskutonis R.P., 2007	Hachicha, Skanji, et al., 2007	Kiran, Devi, et al., 2007	Limberger, Scopel, et al., 2007	Meccia, Rojas, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	DB-1	DB-5	DB-5	DB-1
Column length (m)	30.	30.	30.	30.	50.
Carrier gas		Helium	Helium	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	95.
T_end (C)	220.	260.	300.	220.	240.
Heat rate (K/min)	4.	2.5	3.	4.	4.
Initial hold (min)	5.	1.
Final hold (min)	20.	20.
I	1577.	1545.	1548.	1579.	1576.
Reference	Mohottalage, Tabacchi, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007	Moreno, Lima, et al., 2007	Morteza-Semnani, Saeedi, et al., 2007	Pala-Paul, Brophy, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	SPB-1	SPB-5	DB-1	HP-5
Column length (m)	25.	30.	30.	60.	30.
Carrier gas	Helium	He	He	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.2	0.25	0.25	0.25
T_start (C)	100.	70.	50.	60.	40.
T_end (C)	280.	220.	250.	250.	260.
Heat rate (K/min)	4.	3.	2.	4.	4.
Initial hold (min)	3.			1.
Final hold (min)	5.	15.		10.
I	1581.	1553.	1574.	1576.	1572.
Reference	Phutdhawong, Kawaree, et al., 2007	Pinto, Salgueiro, et al., 2007	Raal, Orav, et al., 2007	Reza, Ebrahim, et al., 2007	Ristic, Krivokuca-Dokic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	DB-5	HP-5 MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	He	Nitrogen		Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	40.	60.
T_end (C)	240.	320.	250.	250.	280.
Heat rate (K/min)	4.	10.	5.	2.	3.
Initial hold (min)
Final hold (min)		4.	10.	33.
I	1579.	1575.	1574.	1573.	1578.
Reference	Sefidkon, Abbasi, et al., 2007	Smelcerovic, Spiteller, et al., 2007	Sonboli, Kanani, et al., 2007	Sylvestre, Pichette, et al., 2007	Tsokou, Georgopoulos, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	60.	60.
T_end (C)	280.	250.	260.	300.	300.
Heat rate (K/min)	3.	3.	4.	3.	3.
Initial hold (min)		5.
Final hold (min)		10.
I	1578.	1571.	1573.4	1567.	1573.
Reference	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Zizovic, Stamenic, et al., 2007	Apel, Sobral, et al., 2006	Apel, Sobral, et al., 2006, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	ZB-5	AT-5	HP-5MS
Column length (m)	30.	25.	30.	60.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25		0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	40.	80.	40.	60.	60.
T_end (C)	260.	270.	300.	200.	280.
Heat rate (K/min)	4.	10.	2.	4.	3.
Initial hold (min)	5.
Final hold (min)				20.
I	1574.	1572.	1556.	1574.	1578.
Reference	Askari and Sefidkon, 2006	Ayoub, Al-Azizi, et al., 2006	Biondi, Sari, et al., 2006	Borges, Rojas, et al., 2006	Bozin, Mimicá-Dukic, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-5	HP-5	HP-1
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.26	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	246.	280.	290.	300.	250.
Heat rate (K/min)	3.	4.	3.	5.	2.
Initial hold (min)				5.
Final hold (min)				5.	40.
I	1578.	1574.	1574.	1578.	1557.
Reference	Coronel, Cerda-Garcia-Rojas, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-1	HP-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas		He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	210.	240.	240.	250.	240.
Heat rate (K/min)	2.	5.	5.	5.	4.
Initial hold (min)	2.	2.	2.
Final hold (min)	33.			10.
I	1573.	1575.	1575.	1577.	1576.
Reference	Garneau F.X., Collin G., et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006	Hadian, Sonboli, et al., 2006	Ibañez and Usubillaga, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	BP-1	Methyl Silicone	HP-5
Column length (m)	30.	30.		25.	30.
Carrier gas	He	Helium	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.32
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	60.	90.	60.
T_end (C)	260.	260.	220.	220.	260.
Heat rate (K/min)	4.	3.	5.	7.	5.
Initial hold (min)				2.	2.
Final hold (min)			6.		13.
I	1576.	1580.	1564.	1563.	1580.
Reference	Ibanez and Usubillaga, 2006	Javidnia, Miri, et al., 2006	Kiran, Bhavani, et al., 2006	Kitchlu, Bakshi, et al., 2006	Kucuk, Gulec, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	HP-5	CP Sil 5 CB	CP Sil 5 CB	5 % Phenyl methyl siloxane
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	N2	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	100.	50.	50.	60.
T_end (C)	300.	240.	300.	200.	280.
Heat rate (K/min)	4.	5.	4.	5.	3.
Initial hold (min)		2.
Final hold (min)		5.			30.
I	1568.	1576.	1568.	1578.	1543.
Reference	Kula, Izydorczyk, et al., 2006	Lago, Soares, et al., 2006	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006	Marongiu, Piras, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	220.	220.	260.	220.	265.
Heat rate (K/min)	4.	4.	4.	4.	2.5
Initial hold (min)		5.	4.	5.	0.5
Final hold (min)
I	1579.	1580.	1579.	1581.	1607.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Morteza-Semnani, Saeedi, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Nickavar B., Kamalinejad M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	DB-1	HP-5MS	HP-5
Column length (m)	30.	25.	50.	30.	30.
Carrier gas	He	N2	N2	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.15	0.25	0.25	0.25
T_start (C)	50.	50.	95.	40.	60.
T_end (C)	250.	200.	240.	260.	220.
Heat rate (K/min)	2.	4.	4.	4.	5.
Initial hold (min)		3.			10.
Final hold (min)
I	1568.	1575.	1599.	1583.	1570.
Reference	Orav, Raal, et al., 2006	Ouamba, Ouabonzi, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Petrovic, Ristic, et al., 2006	Pintore G., Chessa M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5MS	HP-5	HP-5MS
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	Hydrogen	Hydrogen	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	70.	60.	60.	50.
T_end (C)	280.	280.	280.	240.	250.
Heat rate (K/min)	4.	4.	3.	3.	10.
Initial hold (min)	4.	4.			5.
Final hold (min)
I	1576.	1576.	1545.	1581.	1590.
Reference	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006	Pitarokili, Tzakou, et al., 2006	Potzernheim, Bizzo, et al., 2006	Robinson, 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5	DB-1	DB-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	40.	40.	40.
T_end (C)	200.	280.	240.	250.	260.
Heat rate (K/min)	2.	4.	4.	4.	2.
Initial hold (min)					5.
Final hold (min)	60.				20.
I	1576.	1579.	1576.	1560.	1572.
Reference	Rout, Naik, et al., 2006	Sajjadi, 2006	Sefidkon and Jamzad, 2006	Sefidkon, Jamzad, et al., 2006	Senatore, Landolfi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	SPB-5	CP Sil 5 CB	Methyl Silicone	HP-5
Column length (m)	60.		25.	25.	25.
Carrier gas	Helium	He	H2	N2	H2
Substrate
Column diameter (mm)	0.25		0.25	0.3	0.32
Phase thickness (μm)	0.25			0.15	0.52
T_start (C)	60.	50.	50.	50.	50.
T_end (C)	250.	250.	230.	210.	280.
Heat rate (K/min)	5.	5.	3.	2.	2.5
Initial hold (min)		3.		5.	5.
Final hold (min)	10.	15.
I	1570.	1576.	1567.	1600.	1583.
Reference	Sonboli, Mirjalili, et al., 2006	Stojanovic, Palic, et al., 2006	Tesso, König, et al., 2006	Tonzibo, Coffy, et al., 2006	Wang, Kong, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	SPB-1	DB-5	DB-5	HP-1
Column length (m)	30.	50.	30.	30.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.5
T_start (C)	60.	50.	40.	60.	60.
T_end (C)	250.	220.	250.	210.	250.
Heat rate (K/min)	10.	4.	4.	3.	2.
Initial hold (min)	2.	1.		5.
Final hold (min)	10.	10.			60.
I	1595.	1558.	1562.	1574.	1564.
Reference	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006	Yadegarinia, Gachkar, et al., 2006	Askari and Sefidkon, 2005	Bendimerad and Bendiab, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5	CP Sil 8 CB	DB-1
Column length (m)	50.	30.	25.	30.	60.
Carrier gas		He	He	He	N2
Substrate
Column diameter (mm)	0.3	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	60.	60.	60.	80.	60.
T_end (C)	240.	240.	240.	200.	250.
Heat rate (K/min)	2.	3.	3.	3.	5.
Initial hold (min)				5.
Final hold (min)			7.	5.	10.
I	1579.	1577.	1572.	1577.	1578.
Reference	Chagonda and Chalchat, 2005	Chaverri and Cicció, 2005	Duarte, Figueira, et al., 2005	Facey, Porter, et al., 2005	Fakhari A.R., Sonboli A., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	300.	30.	300.	250.	250.
Heat rate (K/min)	3.	4.	5.	5.	5.
Initial hold (min)	3.	3.	5.
Final hold (min)		15.	5.	10.	10.
I	1573.	1577.	1578.	1578.	1580.
Reference	Ferraz, Limberger, et al., 2005	Ferretti, Maggi, et al., 2005	Figuérédo, Cabassu, et al., 2005	Jassbi, Mehrdad, et al., 2005	Jassbi, Mehrdad, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-1	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.52	0.25	0.25
T_start (C)	40.	50.	50.	60.	60.
T_end (C)	240.	265.	265.	240.	240.
Heat rate (K/min)	4.	2.5	2.5	3.	3.
Initial hold (min)		1.	1.
Final hold (min)		20.	30.
I	1571.	1562.	1553.	1571.	1573.
Reference	Jovanovic, Kitic, et al., 2005	Khanavi, Ghasemian, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005	Khayyat and Karimi, 2005	Khayyat and Karimi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	35.	35.	60.	60.
T_end (C)	240.	280.	280.	230.	280.
Heat rate (K/min)	3.	4.	4.	3.	3.
Initial hold (min)		2.	2.		30.
Final hold (min)
I	1579.	1588.	1588.	1569.	1545.
Reference	Khayyat and Karimi, 2005	Kowalski and Wolski, 2005	Kowalski, 2005	Limberger, Sobral, et al., 2005	Marongiu, Piras, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	CP Sil 5 CB	CP Sil 5 CB	HP-5
Column length (m)	30.	30.	25.	25.	30.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.15	0.25
T_start (C)	60.	60.	50.	50.	70.
T_end (C)	220.	220.	230.	230.	240.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)	5.	5.
Final hold (min)
I	1578.	1578.	1579.	1573.	1577.
Reference	Morteza-Semnani, Akbarzadeh, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005, 2	Ogunwande, Olawore, et al., 2005	Olawore, Ogunwande, et al., 2005	Oyedeji, Yani, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	HP-5	HP-5MS
Column length (m)	50.	50.	30.	30.	30.
Carrier gas	N2	N2		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	95.	95.	60.	60.	60.
T_end (C)	240.	240.	280.	240.	220.
Heat rate (K/min)	4.	4.	3.	5.	6.
Initial hold (min)					3.
Final hold (min)
I	1576.	1576.	1578.	1575.	1596.
Reference	Palá-Paúl, Pérez-Alonso, et al., 2005	Pala-Paul, Perez-Alonso, et al., 2005	Petrakis, Roussis, et al., 2005	Saeidnia, Gohari, et al., 2005	Safaei-Ghomi, Bamoniri, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-5MS	DB-5	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	280.	275.	280.	220.	265.
Heat rate (K/min)	4.	4.	4.	3.	2.5
Initial hold (min)				4.	1.
Final hold (min)					20.
I	1578.	1578.	1576.	1580.	1543.
Reference	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005	Sajjadi, 2005	Salehi, Sefidkon, et al., 2005	Sarkhail, Amin, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	240.	260.	280.	300.	300.
Heat rate (K/min)	4.	2.	3.	3.	3.
Initial hold (min)		5.	5.
Final hold (min)		20.
I	1575.	1572.	1576.	1571.	1571.
Reference	Sefidkon and Jamzad, 2005	Senatore, Apostolides Arnold, et al., 2005	Setzer, Noletto, et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005	Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	RTX-1	DB-1	DB-5
Column length (m)	30.	30.	60.	60.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	300.	280.	25.	250.	210.
Heat rate (K/min)	3.	3.	5.	5.	2.
Initial hold (min)					2.
Final hold (min)			10.	10.	33.
I	1572.	1572.	1574.	1571.	1578.
Reference	Simoes-Pires C.A., Debenedetti S., et al., 2005	Slavkovska, Couladis, et al., 2005	Sonboli, Salehi, et al., 2005	Sonboli, Salehi, et al., 2005, 2	Stevanovic, Garneau, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 8 CB	HP-5 MS	HP-5MS	DB-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)		0.50	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	290.	260.	280.	280.	240.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)	5.
Final hold (min)		20.
I	1567.	1579.	1543.	1558.	1578.
Reference	Suárez, Vásquez, et al., 2005	Topçu, Barla, et al., 2005	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005	Urdampilleta, Amat, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	DB-5	CP Sil 5 CB	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	H2	N2	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	50.	50.
T_end (C)	220.	260.	290.	200.	200.
Heat rate (K/min)	3.	5.	4.	5.	5.
Initial hold (min)	5.	2.
Final hold (min)	10.	13.
I	1571.	1579.	1576.	1574.	1574.
Reference	Vichi, Riu-Aumatell, et al., 2005	Yayli, Yasar, et al., 2005	Abreu, Reis, et al., 2004	Agnaniet, Menut, et al., 2004	Fekam Boyom, Fotio, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	DB-5	RTX-1
Column length (m)	30.	25.	25.	60.	30.
Carrier gas	N2		Nitrogen	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	40.	60.
T_end (C)	230.	180.	240.	280.	300.
Heat rate (K/min)	2.	3.	3.	4.	4.
Initial hold (min)		10.		4.
Final hold (min)		10.
I	1576.	1575.	1577.	1577.	1568.
Reference	González, Guerra, et al., 2004	bin Jantan, Ayop, et al., 2004	JAvidnia, Mojab, et al., 2004	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-5	DB-5MS	DB-5	RTX-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	260.	300.	240.	300.	300.
Heat rate (K/min)	2.	3.	3.	3.	4.
Initial hold (min)	5.
Final hold (min)
I	1568.	1556.	1576.	1572.	1567.
Reference	Kilic, Hafizoglu, et al., 2004	Lago, de Ávila, et al., 2004	paz Lima, Silva, et al., 2004	Limberger, Sobral, et al., 2004	Lis, Boczek, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	HP-5MS	HP-5MS	BP-1
Column length (m)	30.	30.	30.	30.	25.
Carrier gas		He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	210.	280.	280.	280.	220.
Heat rate (K/min)	2.	3.	3.	3.	5.
Initial hold (min)	2.
Final hold (min)	33.
I	1574.	1586.	1573.	1574.	1572.
Reference	Lopez Arze, Collin, et al., 2004	Malencic, Couladis, et al., 2004	Malencic, Couladis, et al., 2004	Malencic, Couladis, et al., 2004	Mallavarapu, Kulkarni, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-1	DB-5	DB-1
Column length (m)	30.	30.	60.	30.	50.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.25	0.15	0.25	0.25	0.25
T_start (C)	60.	60.	50.	35.	70.
T_end (C)	275.	220.	270.	220.	220.
Heat rate (K/min)	4.	3.	4.	3.	4.
Initial hold (min)		3.
Final hold (min)
I	1590.	1575.	1560.	1579.	1568.
Reference	Mehrabani, Asadipour, et al., 2004	Mevy, Bessiere, et al., 2004	Nik, Mirza, et al., 2004	Palá-Paúl, Brophy, et al., 2004	Palá-Paúl, García-Jiménez, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	HP-5MS	DB-5	HP-1
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	50.	35.	60.	50.	40.
T_end (C)	250.	220.	280.	250.	260.
Heat rate (K/min)	2.	2.5	4.	3.	2.
Initial hold (min)				5.	5.
Final hold (min)		6.			20.
I	1572.	1578.	1578.	1576.	1574.
Reference	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004	Sajjadi and Shahpiri, 2004	Sefidkon, Jamzad, et al., 2004	Senatore, Napolitano, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	CP Sil 5 CB	BPX-5	DB-5
Column length (m)	30.	30.	20.	25.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	1.	0.25
T_start (C)	40.	60.	100.	60.	60.
T_end (C)	250.	300.	270.	250.	240.
Heat rate (K/min)	2.	3.	8.	3.	4.
Initial hold (min)	5.		2.	5.
Final hold (min)	20.			10.
I	1575.	1567.	1575.	1612.	1570.
Reference	Senatore, Rigano, et al., 2004	Suyenaga, Apel, et al., 2004	Thappa, Bakshi, et al., 2004	Vilaseca, Guy, et al., 2004	Cabanillas, Lopez, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	DB-1	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	100.	60.	50.	60.	60.
T_end (C)	240.	220.	200.	275.	280.
Heat rate (K/min)	5.	5.	5.	4.	4.
Initial hold (min)	2.	20.
Final hold (min)	5.	20.
I	1576.	1582.	1551.	1580.	1576.
Reference	Chaves, Lago, et al., 2003	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Ngouana, et al., 2003	Ghannadi, Aghazari, et al., 2003	Ghasemi, Asghari, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	Methyl Silicone	RSL-200	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	H2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	280.	275.	250.	280.	280.
Heat rate (K/min)	4.	4.	2.	6.	6.
Initial hold (min)			2.	5.	5.
Final hold (min)			5.	5.	5.
I	1568.	1586.	1555.	1573.	1562.
Reference	Ghassemi, Sajjadi, et al., 2003	Ghannadi and Zolfaghari, 2003	Jayaprakasha, Rao, et al., 2003	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CP Sil 5 CB	CP Sil 5 CB	DB-5	DB-5
Column length (m)	50.	25.	25.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.39	0.25	0.25
T_start (C)	50.	35.	60.	60.	60.
T_end (C)	220.	280.	220.	280.	250.
Heat rate (K/min)	3.	5.	5.	5.	3.
Initial hold (min)	2.	2.5
Final hold (min)	10.
I	1575.	1557.	1568.	1568.	1573.
Reference	Juteau, Jerkovic, et al., 2003	Kanjilal, Kotoky, et al., 2003	Khanavi, Hadjiakhoondi, et al., 2003	Lago, de Ávila, et al., 2003	Limberger, Simões-Pires, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5	CP Sil 5 CB	ZB-1	DB-1
Column length (m)	30.	50.	25.	30.	60.
Carrier gas	He	He		N2	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.39	0.25	0.25
T_start (C)	60.	50.	60.	45.	50.
T_end (C)	240.	220.	220.	230.	270.
Heat rate (K/min)	3.	3.	5.	3.	4.
Initial hold (min)		2.
Final hold (min)
I	1581.	1574.	1570.	1561.	1560.
Reference	Maia, Taveira, et al., 2003	Masotti, Juteau, et al., 2003	Mazloomifar, Saber-Tehrani, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003	Mirza and Nik, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5	DB-5	HP-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	Helium	H2	H2	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	70.	60.	60.	60.
T_end (C)	270.	210.	280.	280.	280.
Heat rate (K/min)	4.	2.	4.	4.	3.
Initial hold (min)			10.	10.
Final hold (min)		60.	40.	40.
I	1560.	1575.	1576.	1576.	1557.
Reference	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003	Pino, Marbot, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	NB-30	DB-1	DB-5	Methyl Silicone
Column length (m)	30.	50.	60.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.2	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.5	0.25	0.25
T_start (C)	75.	50.	40.	40.	35.
T_end (C)	220.	250.	220.	230.	180.
Heat rate (K/min)	3.	2.	4.	2.	4.
Initial hold (min)	4.
Final hold (min)
I	1578.	1570.	1568.	1576.	1556.
Reference	Priestap, van Baren, et al., 2003	Raal, Arak, et al., 2003	Rasooli and Mirmostafa, 2003	Rotman, Ahumada, et al., 2003	Santos and Cordeiro, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	Cross-Linked Methylsilicone	HP-5
Column length (m)	60.	30.	60.	25.	25.
Carrier gas	He	He		He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.53
T_start (C)	40.	60.	40.	70.	40.
T_end (C)	260.	240.	250.	250.	280.
Heat rate (K/min)	4.	3.	5.	4.	4.
Initial hold (min)	5.		15.
Final hold (min)
I	1558.	1580.	1576.	1556.	1573.
Reference	Sefidkon, Naderi Nik, et al., 2003	da Silva, Luz, et al., 2003	Stashenko, Jaramillo, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	DB-5	DB-5
Column length (m)	25.	25.	30.	30.	25.
Carrier gas	Helium	Helium	He	He	N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.53	0.53	0.32	0.25	0.25
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	280.	280.	250.	240.	250.
Heat rate (K/min)	4.	4.	5.	3.	4.
Initial hold (min)			30.
Final hold (min)					10.
I	1574.	1578.	1581.	1579.	1576.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003	Zrira, Elamrani, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	CP Sil 5 CB	OV-101	DB-5	5 % Phenyl methyl siloxane
Column length (m)	60.	25.	25.	30.	30.
Carrier gas	He	N2		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.4		0.25	0.25
T_start (C)	50.	60.	50.	60.	75.
T_end (C)	280.	260.	200.	280.	200.
Heat rate (K/min)	4.	5.	5.	3.	3.
Initial hold (min)					4.
Final hold (min)		40.		30.	8.
I	1560.	1563.	1573.	1563.	1578.
Reference	Ahmadi, Mirza, et al., 2002	Azaz. D., Demirci, et al., 2002	Boyom, Keumedjio, et al., 2002	Caredda, Marongiu, et al., 2002	Cicció and Gómez-Laurito, 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	HP-5	DB-5	DB-1
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	N2	N2	N2	He	H2
Substrate
Column diameter (mm)	0.50	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	40.
T_end (C)	220.	250.	250.	240.	245.
Heat rate (K/min)	5.	4.	4.	3.	3.
Initial hold (min)			5.		20.
Final hold (min)	10.
I	1570.	1576.	1576.	1578.	1560.
Reference	Das, Ram, et al., 2002	Farah, Fechtal, et al., 2002	Farah, Fechtal. M., et al., 2002	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	PTE-5	SE-30	RSL-200	RSL-200	CP Sil 8 CB
Column length (m)	60.	50.	30.	30.	30.
Carrier gas	H2	He	H2	H2	He
Substrate
Column diameter (mm)	0.32	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.30	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	40.	50.	50.
T_end (C)	285.	240.	280.	280.	220.
Heat rate (K/min)	4.3	4.	6.	6.	3.
Initial hold (min)			5.	5.	2.
Final hold (min)			5.	5.
I	1576.	1571.	1619.	1619.	1575.
Reference	Gudzic, Djokovic, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002	Juteau, Masotti, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	DB-5	HP-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	35.	50.	60.	60.
T_end (C)	240.	280.	200.	250.	275.
Heat rate (K/min)	3.	3.	5.	3.	4.
Initial hold (min)		2.			4.
Final hold (min)		15.
I	1577.	1588.	1574.	1573.	1571.
Reference	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Kuiate, Bessière, et al., 2002	Limberger, Simões-Pires, et al., 2002	Lockwood, Asghari, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5MS	CP Sil 5 CB	DB-5	HP-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.39	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	240.	220.	220.	240.
Heat rate (K/min)	3.	3.	5.	4.	3.
Initial hold (min)				5.
Final hold (min)
I	1579.	1578.	1565.	1578.	1585.
Reference	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Mojab, Rustaiyan, et al., 2002	Morteza-Semnani, Saeedi, et al., 2002	Novak, Langbehn, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	HP-1	DB-5	DB-1
Column length (m)	30.	50.	50.	25.	60.
Carrier gas		N2	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25
T_start (C)	60.	80.	90.	60.	40.
T_end (C)	240.	225.	220.	220.	250.
Heat rate (K/min)	3.	4.	3.	3.	4.
Initial hold (min)
Final hold (min)
I	1587.	1557.	1570.	1574.	1555.
Reference	Novak, Langbehn, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Priestap, van Baren, et al., 2002	Schwob, Bessière, et al., 2002	Sefidkon, Dabiri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5MS	DB-5	DB-1
Column length (m)	60.	60.	30.	30.	60.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.248
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	280.	280.	270.	240.	220.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)	5.	5.			5.
Final hold (min)					22.
I	1562.	1562.	1577.	1578.	1579.
Reference	Sefidkon, Jalili, et al., 2002	Sefidkon, 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Bailac, Dellacasa, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	SPB-5	HP-5	BP-1	Optima-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.2
Phase thickness (μm)	0.25		0.25	0.25
T_start (C)	60.	40.	60.	60.	50.
T_end (C)	240.	220.	220.	220.	250.
Heat rate (K/min)	3.	3.	5.	5.	3.
Initial hold (min)		5.	10.		3.
Final hold (min)		15.
I	1567.	1585.	1577.	1571.	1584.
Reference	Cherchi, Deidda, et al., 2001	Cornu, Carnat, et al., 2001	Gallori, Flamini, et al., 2001	Gupta, Mallavarapu, et al., 2001	Jacquemond-Collet, Bessière, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RTX-1	CBP-1	DB-5MS	DB-1
Column length (m)	30.	30.	25.	30.	60.
Carrier gas	H2	N2	Nitrogen	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	50.
T_end (C)	280.	300.	210.	240.	270.
Heat rate (K/min)	6.	4.	3.	3.	4.
Initial hold (min)	5.		2.
Final hold (min)	5.			30.
I	1618.	1569.	1615.	1565.	1559.
Reference	Jirovetz L., Buchbauer G., et al., 2001	Kalemba, Marschall, et al., 2001	Ly, Yamauchi, et al., 2001	Marongiu, Porcedda, et al., 2001	Mirza, Ahmadi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5	DB-1	DB-1	PTE-5
Column length (m)	50.	30.	30.	30.	60.
Carrier gas	He	He	N2	He	H2
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.2	0.32
Phase thickness (μm)	0.5	0.25	0.25		0.3
T_start (C)	50.	60.	80.	60.	60.
T_end (C)	250.	270.	225.	240.	285.
Heat rate (K/min)	2.	3.	4.	3.	4.3
Initial hold (min)
Final hold (min)
I	1558.	1580.	1545.	1577.5	1576.
Reference	Orav, Kailas, et al., 2001	Palmeira, Conserva, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Santos, Moreira, et al., 2001	Stojanovic, Palic, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	DB-1	HP-1	BP-1
Column length (m)	25.	60.	25.	60.	25.
Carrier gas		N2	Nitrogen	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.50	0.25	0.33
Phase thickness (μm)	0.15	0.25	0.25	0.25	1.0
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	230.	220.	220.	200.	275.
Heat rate (K/min)	3.	3.	5.	4.	4.
Initial hold (min)		5.		5.
Final hold (min)		22.		25.
I	1579.	1581.	1570.	1587.	1575.
Reference	Asekun and Ekundayo, 2000	Bailac, Dellacasa, et al., 2000	Mallavarapu, Rao, et al., 2000	Meccia, Rojas, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	OV-101	DB-1	RTX-1
Column length (m)	30.	30.	25.	60.	30.
Carrier gas	He	He	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	40.	50.	75.	60.
T_end (C)	275.	240.	200.	220.	300.
Heat rate (K/min)	4.	3.	5.	4.	4.
Initial hold (min)		5.		1.
Final hold (min)				8.
I	1572.	1582.	1573.	1579.	1568.
Reference	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2	Novak, Novak, et al., 2000	Ayedoun, Adéoti, et al., 1999	Bailac, Dellacasa, et al., 1999	Kalemba, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CBP-1	CP Sil 5 CB	DB-1	DB-5	CP Sil 5 CB
Column length (m)	25.	25.	50.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.3	0.25	0.25	0.25	0.25
Phase thickness (μm)			0.25	0.25	0.39
T_start (C)	60.	50.	70.	40.	60.
T_end (C)	240.	230.	240.	250.	220.
Heat rate (K/min)	4.	3.	4.	2.	5.
Initial hold (min)				5.	5.
Final hold (min)				60.	20.
I	1570.	1550.	1545.	1553.	1569.
Reference	Labuckas, Zygadlo, et al., 1999	Oyedeji, Olawore, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Porta, Porcedda, et al., 1999	Rustaiyan, Masoudi, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-1	DB-5	CP Sil 5 CB
Column length (m)	60.	60.	60.	30.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.39
T_start (C)	40.	50.	60.	60.	60.
T_end (C)	280.	220.	230.	240.	220.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)	5.
Final hold (min)			5.
I	1571.	1568.	1568.	1575.	1571.
Reference	Sefidkon, Dabiri, et al., 1999	Sefidkon and Mirza, 1999	Shafiee, Javidnia, et al., 1999	Tellez, Canel, et al., 1999	Weyerstahl, Marschall, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SPB-5	DB-5	OV-1	CBP-1
Column length (m)	30.	50.	30.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	240.	240.	240.	250.	240.
Heat rate (K/min)	3.	3.	3.	10.	4.
Initial hold (min)				5.
Final hold (min)		20.		20.
I	1576.	1587.	1576.	1567.	1576.
Reference	Zoghbi, Andrade, et al., 1999	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998	Kökdil, Kurucu, et al., 1998	Lamarque, Maestri, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	OV-101	DB-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	Helium		He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25			0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	240.	240.	200.	250.	240.
Heat rate (K/min)	3.	3.	5.	3.	3.
Initial hold (min)
Final hold (min)
I	1579.	1579.	1573.	1577.	1576.
Reference	Maia, Zohhbi, et al., 1998	Santos, Andrade, et al., 1998	Zollo, Biyiti, et al., 1998	Abreu and Noronha, 1997	Tellez, Estell, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	CBP-1	DB-5	DB-5	SPB-1
Column length (m)	30.	25.	30.	30.	50.
Carrier gas	He	He			He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.2
Phase thickness (μm)			0.25		0.33
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	240.	240.	300.	210.	200.
Heat rate (K/min)	4.	5.	4.	2.	3.
Initial hold (min)			2.	2.	3.
Final hold (min)			5.	33.	30.
I	1570.	1570.	1576.7	1574.	1563.
Reference	Zunino, Novillo-Newton, et al., 1997	Zygadlo, Ariza-Espinar, et al., 1997	Gawdzik, Mardarowicz, et al., 1996	Sohounhloue, Dangou, et al., 1996	Wong and Lai, 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-101	SE-54	DB-1	CP Sil 8 CB	BP-1
Column length (m)	50.	30.	30.	25.	50.
Carrier gas	H2	Hydrogen	N2		H2
Substrate
Column diameter (mm)	0.32	0.25		0.20	0.30
Phase thickness (μm)	0.3	0.25
T_start (C)	65.	60.	80.	60.	40.
T_end (C)	300.	250.	220.	230.	250.
Heat rate (K/min)	2.	2.	4.	3.	10.
Initial hold (min)	5.	5.		10.	1.
Final hold (min)		2.
I	1556.	1569.	1595.	1589.	1573.
Reference	Demarne and van der Walt, 1993	Kollmannsberger, Nitz, et al., 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991	Jantan and Goh, 1990	Brophy, Davies, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary
Active phase	DB-1
Column length (m)	10.
Carrier gas	H2
Substrate
Column diameter (mm)	0.25
Phase thickness (μm)	0.25
T_start (C)	50.
T_end (C)	250.
Heat rate (K/min)	5.
Initial hold (min)
Final hold (min)
I	1555.
Reference	Perry, Baxter, et al., 1986
Comment	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Rahimi-Nasrabadi, Gholivand, et al., 2009
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Scrivanti, Anton, et al., 2009
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Shafaghat and Sadeghi, 2009
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de Souza, Lopes, et al., 2009
de Souza, A.; Lopes, E.M.C.; da Silva, M.C.; Cordeiro, I.; Young, M.C.M.; Sobral, M.E.G.; Moreno, P.R.H., Chemical composition and acetylcholinesterase inhibitory activity of essential oils of Myrceugenia myrcioides (Chambess.) O. Berg and Eugenia riedeliana O. Berg, Myrtaceae, Braz. J. Pharmacognosy, 2009, 20, 2, 175-179. [all data]

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Sefidkon, 2002
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Gupta, Mallavarapu, et al., 2001
Gupta, R.; Mallavarapu, G.R.; Banerjee, S.; Kumar, S., Characteristics of an isomenthone-rich somaclonal mutant isolated in a geraniol-rich rose-scented geranium accession of Pelargonium graveolens, Flavour Fragr. J., 2001, 16, 5, 319-324, https://doi.org/10.1002/ffj.1002 . [all data]

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Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

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Asekun and Ekundayo, 2000
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Ayedoun, Adéoti, et al., 1999
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Kalemba, 1999
Kalemba, D., Constituents of the essential oil of Artemisia asiatica Nakai, Flavour Fragr. J., 1999, 14, 3, 173-176, https://doi.org/10.1002/(SICI)1099-1026(199905/06)14:3<173::AID-FFJ805>3.0.CO;2-Q . [all data]

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Sefidkon and Mirza, 1999
Sefidkon, F.; Mirza, M., Chemical composition of the essential oils of two Salvia species from Iran, Salvia virgata Jacq. and Salvia syriaca L., Flavour Fragr. J., 1999, 14, 1, 45-46, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<45::AID-FFJ774>3.0.CO;2-S . [all data]

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Weyerstahl, P.; Marschall, H.; Thefeld, K.; Rustaiyan, A., Constituents of the essential oil of Tanacetum (syn. Chrysanthemum) fruticulosum Ledeb. from Iran, Flavour Fragr. J., 1999, 14, 2, 112-120, https://doi.org/10.1002/(SICI)1099-1026(199903/04)14:2<112::AID-FFJ786>3.0.CO;2-1 . [all data]

Zoghbi, Andrade, et al., 1999
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Doneanu and Anitescu, 1998
Doneanu, C.; Anitescu, G., Supercritical carbon dioxide extraction of Angelica archangelica L. root oil, J. Supercrit. Fluids, 1998, 12, 1, 59-67, https://doi.org/10.1016/S0896-8446(97)00040-5 . [all data]

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Lamarque, Maestri, et al., 1998
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Maia, Zohhbi, et al., 1998
Maia, J.G.S.; Zohhbi, M.G.B.; Andrade, E.H.A.; Santos, A.S.; da Silva, M.H.L.; Luz, A.I.R.; Bastos, C.N., Constituents of the essential oil of Piper aduncum L. growing wild in the Amazon region, Flavour Fragr. J., 1998, 13, 4, 269-272, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<269::AID-FFJ744>3.0.CO;2-A . [all data]

Santos, Andrade, et al., 1998
Santos, A.S.; Andrade, E.H.A.; Zoghbi, M. das.G.B.; Luz, A.I.R.; Maia, J.G.S., Sesquiterpenes of Amazonian Piper species, Acta Amazomica, 1998, 28, 2, 127-130. [all data]

Zollo, Biyiti, et al., 1998
Zollo, P.H.A.; Biyiti, L.; Tchoumbougnang, F.; Menut, C.; Lamaty, G.; Bouchet, Ph., Aromatic plants of tropical central Africa. Part XXXII. Chemical composition and antifungal activity of thirteen essential oils from aromatic plants of Cameroon, Flavour Fragr. J., 1998, 13, 2, 107-114, https://doi.org/10.1002/(SICI)1099-1026(199803/04)13:2<107::AID-FFJ701>3.0.CO;2-G . [all data]

Abreu and Noronha, 1997
Abreu, P.M.; Noronha, R.G., Volatile constituents of the rhizomes of Aframomum alboviolaceum (Ridley) K. Schum. from Guinea-Bissau, Flavour Fragr. J., 1997, 12, 2, 79-83, https://doi.org/10.1002/(SICI)1099-1026(199703)12:2<79::AID-FFJ617>3.0.CO;2-7 . [all data]

Tellez, Estell, et al., 1997
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Zunino, Novillo-Newton, et al., 1997
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Zygadlo, Ariza-Espinar, et al., 1997
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Wong and Lai, 1996
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Demarne and van der Walt, 1993
Demarne, F.-E.; van der Walt, J.J.A., Composition of the Essential Oil of Pelargonium citronellum (Geraniaceae), J. Essent. Oil Res., 1993, 5, 3, 233-238, https://doi.org/10.1080/10412905.1993.9698214 . [all data]

Kollmannsberger, Nitz, et al., 1992
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Velasco-Negueruela, Pérez Alonso, et al., 1991
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Jantan and Goh, 1990
Jantan, I.; Goh, S.H., The essential oils of Cinnamomum mollissimum as natural sources of safrole and benzyl benzoate, J. Tropical Forest Sci., 1990, 2, 3, 252-259. [all data]

Brophy, Davies, et al., 1989
Brophy, J.J.; Davies, N.W.; Southwell, I.A.; Stiff, I.A.; Williams, L.R., Gas chromatographic quality control for oil of Melaleuca terpinen-4-ol type (Australian tea tree), J. Agric. Food Chem., 1989, 37, 5, 1330-1335, https://doi.org/10.1021/jf00089a027 . [all data]

Perry, Baxter, et al., 1986
Perry, N.B.; Baxter, A.J.; Brennan, N.J.; van Klink, J.W., Dalmatian Sage. PArt 1. Differing oil yields and compositions from flowering and non-flowering accessions, Flavour Fragr. J., 1986, 11, 4, 231-238, https://doi.org/10.1002/(SICI)1099-1026(199607)11:4<231::AID-FFJ572>3.0.CO;2-0 . [all data]

Notes

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Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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