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D-Glucose, 5TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51926.Fu, Iga, et al., 200030. m/0.25 mm/0.25 «mu»m, He, 100. C @ 1. min, 10. K/min, 290. C @ 8. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11930.Yang and Cashman, 199230. m/0.32 mm/1.0 «mu»m, He; Program: 3 min at 100 0C; 100 - 200 0C at 8 deg/min; 1 min at 200 0C; 200 - 280 0C at 5 deg/min; 30 min at 280 0C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-1011937.Binder and Haddon, 1984Helium; Column length: 42. m; Column diameter: 0.50 mm; Program: 60 0C (0.5 min) 30 0C/min -> 170 0C 3 0C/min -> 220 0C
CapillaryOV-1011934.Binder and Haddon, 1984Helium; Column length: 42. m; Column diameter: 0.50 mm; Program: 80 0C (0.5 min) 30 0C/min -> 170 0C 3 0C/min -> 220 0C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Fu, Iga, et al., 2000
Fu, X.; Iga, M.; Kimura, M.; Yamaguchi, S., Simplified screening for organic acidemia using GC/MS and dried urine filter paper: a study on neonatal mass screening, Early Hum. Dev., 2000, 58, 1, 41-55, https://doi.org/10.1016/S0378-3782(00)00053-0 . [all data]

Yang and Cashman, 1992
Yang, Z.C.; Cashman, J.R., Structure-retention index relationships for derivatized monosaccharides on non-polar gas chromatography columns, J. Chromatogr., 1992, 596, 1, 79-84, https://doi.org/10.1016/0021-9673(92)80205-9 . [all data]

Binder and Haddon, 1984
Binder, R.B.; Haddon, W.F., Analysis of O-methylinositols by gas-liquid chromatography-mass spectrometry, Carbohydrate Research, 1984, 129, 21-32, https://doi.org/10.1016/0008-6215(84)85295-7 . [all data]


Notes

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