Guaiacol, TMS derivative
- Formula: C10H16O2Si
- Molecular weight: 196.3183
- IUPAC Standard InChI: InChI=1S/C10H16O2Si/c1-11-9-7-5-6-8-10(9)12-13(2,3)4/h5-8H,1-4H3
- IUPAC Standard InChIKey: XUSIKNZBGJLXTJ-UHFFFAOYSA-N
- CAS Registry Number: 6689-37-8
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 2-Methoxyphenol trimethylsilyl ether; Guaicol-TMS; 2-Methoxyphenol, TMS ether; Guaiacol, trimethylsilyl ether; 2-Methoxyphenol, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 1210. | Mattsson and Petersson, 1977 | N2, Supelcoport, 4. K/min; Column length: 2. m; Tstart: 80. C; Tend: 240. C |
| Packed | SE-30 | 1184. | Lhuguenot, Maume, et al., 1971 | N2, Gas Chrom P (120-140 mesh), 1. K/min; Column length: 3. m; Tstart: 100. C; Tend: 180. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 1233.3 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-30 | 1224. | Zimmermann, Lauterbach, et al., 1985 | Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G.,
Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives,
J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546
. [all data]
Lhuguenot, Maume, et al., 1971
Lhuguenot, J.C.; Maume, B.F.; Baron, C.,
Gas Chromatographic and Mass Spectrometric Study of Vanillin Related Compounds,
Chromatographia, 1971, 4, 5, 204-208, https://doi.org/10.1007/BF02281053
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Zimmermann, Lauterbach, et al., 1985
Zimmermann, V.; Lauterbach, M.; Jaeger, G.,
Analytical characterization phenolic compounds obtained from phenosolvan-extracts by use of gas-chromatography with capillary columns,
Chem. Tech. (Leipzig), 1985, 37, 11, 476-478. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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