3-Cyclohexen-1-ol, 1-methyl-4-(1-methylethyl)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51147.Baranauskiene, Venskutonis, et al., 200350. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min, 280. C @ 10. min
CapillaryMethyl Silicone1134.Adegoke, Rao, et al., 199830. m/0.32 mm/0.25 μm, He, 60. C @ 2. min, 2. K/min, 250. C @ 5. min

Kovats' RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-51137.Sibanda, Chigwada, et al., 200430. m/0.25 mm/0.25 μm, He; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C
CapillaryAT-51135.Khouri, Usubillaga, et al., 200060. m/0.25 mm/0.25 μm, He; Program: 60 C 4K/min -> 200 C 10 K/min -> 280 C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1134.Saroglou, Marin, et al., 200730. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-51120.Dob, Dahmane, et al., 200630. m/0.32 mm/0.25 μm, N2, 60. C @ 3. min, 3. K/min, 240. C @ 5. min
CapillaryHP-5MS1133.Saroglou, Dorizas, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-51134.Su, Ho, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryHP-51138.Mahattanatawee, Goodner, et al., 200530. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 4. K/min, 250. C @ 15. min
CapillaryHP-5MS1131.Chorianopoulos, Kalpoutzakis, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51136.Javidnia, Miri, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C
CapillaryHP-5MS1134.Karioti, Hadjipavlou-Litina, et al., 200430. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryOptima 51137.Vérité, Nacer, et al., 200425. m/0.25 mm/0.25 μm, He, 3. K/min, 280. C @ 20. min; Tstart: 60. C
CapillaryDB-5MS1140.Yu, Kim, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 4. K/min, 200. C @ 20. min
CapillarySPB-11120.Chisholm, Wilson, et al., 200325. m/0.25 mm/0.25 μm, 35. C @ 10. min, 4. K/min; Tend: 225. C
CapillaryHP-51139.Fokialakis, Melliou, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51130.Karioti, Skaltsa, et al., 200330. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryHP-51136.Aligiannis, Kalpoutzakis, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillarySPB-11120.Chisholm, Wilson, et al., 200115. m/0.25 mm/0.25 μm, 35. C @ 3. min, 6. K/min, 225. C @ 10. min
CapillaryHP-5MS1134.Giamakis, Kretsi, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1141.4Andriamaharavo, 201430. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryBPX-51142.Dharmawan, Kasapis, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C => 4C/min => 200C => 30C/min => 300C (3min)
CapillaryBPX-51162.Elmore, Erbahadir, et al., 199750. m/0.32 mm/0.5 μm, He; Program: 0C (5min) => 40C/min => 40C (2min) => 10C/min => 280C
CapillaryBPX-51167.Elmore, Erbahadir, et al., 199750. m/0.32 mm/0.5 μm, He; Program: 0C (5min) => 40C/min => 40C (2min) => 10C/min => 280C

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryCarbowax 20M1562.Verzera, Campisi, et al., 200560. m/0.25 mm/0.25 μm, He, 45. C @ 0.17 min, 2. K/min; Tend: 250. C
CapillaryZB-Wax1571.Ledauphin, Saint-Clair, et al., 200430. m/0.25 mm/0.15 μm, He, 35. C @ 5. min, 5. K/min, 220. C @ 10. min
CapillarySupelcowax1589.Chisholm, Wilson, et al., 200325. m/0.25 mm/0.25 μm, 35. C @ 5. min, 4. K/min, 225. C @ 10. min
CapillaryCP-Wax 52CB1562.Verzera, Campisi, et al., 200160. m/0.25 mm/0.25 μm, He, 45. C @ 0.17 min, 2. K/min; Tend: 250. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5 MS1099.Sardashti, Valizadeh, et al., 201360. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 20. min
CapillaryHP-5 MS1136.Hammami, Kamoun, et al., 201130. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 50. C; Tend: 180. C
CapillaryDB-51141.de Souza, Lopes, et al., 201030. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 3. K/min; Tend: 240. C
CapillaryDB-51134.Shafaghat and Sadeghi, 200950. m/0.20 mm/0.32 μm, Nitrogen, 60. C @ 3. min, 5. K/min, 220. C @ 5. min
CapillaryDB-51141.de Souza, Lopes, et al., 200930. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 3. K/min; Tend: 240. C
CapillaryDBP-51096.Sereshti and Samadi, 200725. m/0.25 mm/0.22 μm, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 10. min
CapillaryHP-51140.Coronel, Cerda-Garcia-Rojas, et al., 200630. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryHP-5MS1134.Farah, Afifi, et al., 200630. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5MS1127.Kim, Abd El-Aty, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 4. min, 5. K/min, 280. C @ 10. min
CapillaryHP-51140.Shafi, Jose, et al., 200625. m/0.2 mm/0.33 μm, N2, 3. K/min; Tstart: 30. C; Tend: 280. C
CapillaryHP-51142.Wang, Yang, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 10. K/min, 250. C @ 10. min
CapillaryDB-11130.Palá-Paúl, Pérez-Alonso, et al., 200550. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryDB-51133.Tellez, Khan, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryRTX-5Sil1146.Dudai, Larkov, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min, 200. C @ 10. min; Tstart: 70. C
CapillaryDB-11141.Norouzi-Arasi, Yavari, et al., 200230. m/0.25 mm/0.25 μm, He, 60. C @ 10. min, 4. K/min; Tend: 250. C
CapillaryCBP-11145.Ly, Yamauchi, et al., 200125. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 2. min, 3. K/min; Tend: 210. C
CapillaryOV-1011133.Zenkevich, Kosman, et al., 1999He, 6. K/min; Column length: 25. m; Column diameter: 0.20 mm; Tstart: 80. C; Tend: 240. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-51136.Zhao, Li, et al., 200830. m/0.25 mm/0.25 μm; Program: 40 0C (2 min) 5 0C/min -> 80 0C 7 oC/min -> 160 0C 9 0C/min -> 200 0C 20 0C/min -> 280 0C (10 min)
CapillaryHP-51139.Zhao, Li, et al., 200830. m/0.25 mm/0.25 μm; Program: not specified
CapillaryHP-5MS1138.Cole, Haber, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(10min) => 3C/min => 200C => 2C/min => 220C
CapillaryHP-5MS1139.Singh, Marimuthu, et al., 200430. m/0.25 mm/0.25 μm; Program: 60C(1min) => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)
CapillarySE-301147.Vinogradov, 2004Program: not specified
CapillaryPolydimethyl siloxanes1147.Zenkevich, 1997Program: not specified

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP Wax 52 CB1586.Chen, Chyau, et al., 200760. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryCP Wax 52 CB1586.Chen, Chyau, et al., 200760. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryCP-Wax 52CB1565.Chyau, Tsai, et al., 200760. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 220. C
CapillaryDB-Wax Etr1582.Ibarz, Ferreira, et al., 200660. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 230. C @ 100. min
CapillaryDB-Wax1621.Lee, Umano, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 180. C @ 40. min; Tstart: 50. C
CapillaryDB-Wax1628.Jiang and Kubota, 2004He, 60. C @ 4. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 220. C
CapillaryDB-Wax1628.Jiang and Kubota, 2004He, 60. C @ 4. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 220. C
CapillaryCarbowax 20M1576.Kasali, Oyedeji, et al., 200130. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 215. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M1562.Editorial paper, 2005Program: not specified
CapillaryCarbowax 20M1576.Editorial paper, 2005Program: not specified
CapillaryCarbowax 20M1576.Vinogradov, 2004Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Shafi, P.M.; Jose, B.; Radhamani, K.T.; Clery, R.A., Influence of pH on essential oil composition of Zanthoxylum rhetsa seeds obtained by steam distillation, Flavour Fragr. J., 2006, 21, 2, 317-318, https://doi.org/10.1002/ffj.1598 . [all data]

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Editorial paper, 2005
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Notes

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