Cyclohexene, 3-methyl-6-(1-methylethylidene)-
- Formula: C10H16
- Molecular weight: 136.2340
- IUPAC Standard InChI: InChI=1S/C10H16/c1-8(2)10-6-4-9(3)5-7-10/h4,6,9H,5,7H2,1-3H3
- IUPAC Standard InChIKey: CIPXOBMYVWRNLL-UHFFFAOYSA-N
- CAS Registry Number: 586-63-0
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: p-Mentha-2,4(8)-diene; Isoterpinolene; 3-Isopropylidene-6-methyl-cyclohexene; 3-Methyl-6-(1-methylethylidene)-cyclohexene; p-2,4(8)-Menthadiene; para-Mentha-2,4(8)-diene; 2,4(8)-p-Menthadiene; 3-Methyl-6-(propan-2-ylidene)cyclohex-1-ene; 3-Methyl-6-(1-methylethylidene)-1-cyclohexene; cis-p-Mentha-2,4(8)-diene
- Permanent link for this species. Use this link for bookmarking this species for future reference.
- Information on this page:
- Other data available:
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Gas Chromatography
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | Apiezon L | 100. | 1106. | Morishita, Okano, et al., 1980 | Column length: 45. m; Column diameter: 0.25 mm |
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1090. | Lucero, Fredrickson, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C |
| Capillary | DB-5MS | 1057. | Marongiu, Porcedda, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 3. K/min, 280. C @ 30. min; Tstart: 60. C |
| Capillary | DB-5 | 1088. | Adams, Morris, et al., 2005 | 30. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C |
| Capillary | HP-5 | 1088. | Lopes, Strobl, et al., 2004 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C |
| Capillary | DB-5 | 1084. | Viña and Murillo, 2003 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 0.5 K/min, 250. C @ 10. min |
| Capillary | DB-5 | 1082. | El-Ghorab, Fadel, et al., 2002 | 25. m/0.22 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1090. | Moreira, Sousa, et al., 2001 | H2, 3. K/min; Column length: 30. m; Column diameter: 0.20 mm; Tstart: 60. C; Tend: 240. C |
| Capillary | SE-54 | 1086. | Adams, 2000 | 30. m/0.26 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 246. C |
| Capillary | DB-5 | 1086. | Adams, 2000, 2 | 30. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C |
Kovats' RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1086. | Moreira, Sousa, et al., 2001 | H2; Column length: 30. m; Column diameter: 0.20 mm; Program: not specified |
Kovats' RI, polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | PEG-20M | 100. | 1296. | Morishita, Okano, et al., 1980 | Column length: 75. m; Column diameter: 0.25 mm |
Kovats' RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-Wax | 1270. | Lopes, Strobl, et al., 2004 | 30. m/0.32 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min; Tend: 220. C |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1081. | Batista-Pereira, Fernandes, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C |
| Capillary | DB-5 | 1081. | Batista-Pereira, Fernandes, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C |
| Capillary | DB-5 | 1088. | Su, Ho, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min; Tend: 250. C |
| Capillary | HP-5 | 1068. | Couladis, Tsortanidou, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 380. C |
| Capillary | Mega 5MS | 1077. | Verzera, Trozzi, et al., 2000 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 3. K/min; Tend: 240. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5MS | 1087.3 | Andriamaharavo, 2014 | 30. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min) |
| Capillary | CBP-5 | 1085. | Oliveira, Campos, et al., 2005 | 30. m/0.25 mm/0.25 μm, He; Program: 60C => 3C/min => 240C => 10C/min => 280C(10min) |
| Capillary | CBP-5 | 1081. | Azevedo, Campos, et al., 2002 | 50. m/0.25 mm/0.25 μm, He; Program: 60C(2min) => 3C/min => 240C => 10C/min => 280C(10min) |
| Capillary | BPX-5 | 1108. | Elmore, Erbahadir, et al., 1997 | 50. m/0.32 mm/0.5 μm, He; Program: 0C (5min) => 40C/min => 40C (2min) => 10C/min => 280C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Optima-5 | 1087. | Al-Qudah, Muhaidat, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium, 60. C @ 1. min, 3. K/min; Tend: 246. C |
| Capillary | HP-5 MS | 1085. | Kotowska, Zalikowski, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium, 35. C @ 5. min, 3. K/min, 300. C @ 15. min |
| Capillary | HP-5 MS | 1088. | Phungpanya, Thongpoon, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium, 2. K/min; Tstart: 50. C; Tend: 180. C |
| Capillary | ZB-5 | 1091. | Vazques, Aimar, et al., 2011 | 30. m/0.25 mm/0.25 μm, Nitrogen, 40. C @ 5. min, 5. K/min; Tend: 200. C |
| Capillary | ZB-5 MS | 1082. | Boix, Victorio, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 5. K/min; Tstart: 60. C; Tend: 290. C |
| Capillary | DB-5 MS | 1081. | Chalchat, Figueredo, et al., 2010 | 25. m/0.30 mm/0.25 μm, Helium, 3. K/min; Tstart: 50. C; Tend: 240. C |
| Capillary | HP-5 | 1086. | Miyazawa, Kawauchi, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C |
| Capillary | HP-5 | 1090. | Miyazawa, Kawauchi, et al., 2010 | 30. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C |
| Capillary | DB-5 MS | 1079. | Noudogbessi, Yedomonhan, et al., 2008 | 30. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 5. K/min, 300. C @ 5. min |
| Capillary | DB-5MS | 1055. | Marongiu B., Piras A., et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 3. K/min, 280. C @ 30. min; Tstart: 60. C |
| Capillary | HP-5 | 1089. | Shafi, Jose, et al., 2006 | 25. m/0.2 mm/0.33 μm, N2, 3. K/min; Tstart: 30. C; Tend: 280. C |
| Capillary | DB-1 | 1073. | Palá-Paúl, Pérez-Alonso, et al., 2005 | 50. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C |
| Capillary | HP-5MS | 1083. | Setzer, Noletto, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C |
| Capillary | DB-5 | 1083. | Maia, da Silva, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1080. | Ruberto, Biondi, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 300. C |
| Capillary | DB-5 | 1086. | Tellez M., Estell R., et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1086. | Zoghbi, Andrade, et al., 1999 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-5 | 1087. | Tellez, Estell, et al., 1997 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 1064. | Albano, Lima, et al., 2012 | 30. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) |
| Capillary | HP-5 MS | 1086. | Kotowska, Zalikowski, et al., 2012 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
| Capillary | ZB-5 | 1091. | Vazques, Aimar, et al., 2011 | 30. m/0.25 mm/0.25 μm, Nitrogen; Program: not specified |
| Capillary | HP-5MS | 1071. | Ning, Zheng, et al., 2008 | 30. m/0.25 mm/0.25 μm, He; Program: 40 0C (2 min) 3 0C/min -> 180 0C (2 min) 15 0C -> 280 0C |
| Capillary | DB-1 | 1064. | Nogueira, Marcelo-Curto, et al., 2008 | 30. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 300C (10min) |
| Capillary | CP Sil 8 CB | 1088. | Mockute, Bernotiene, et al., 2007 | 50. m/0.32 mm/0.25 μm, He; Program: 60 0C (2 min) 5 0C/min -> 160 0C 5 0C/min -> 250 0C (10 min) |
| Capillary | SPB-5 | 1078. | Iriti, Colnaghi, et al., 2006 | 60. m/0.32 mm/1. μm, He; Program: 60C => 1C/min => 130C => 2C/min => 200C => 4C/min => 250C(40min) |
| Capillary | CP Sil 8 CB | 1088. | Mockute, Bernotiene, et al., 2006 | 50. m/0.32 mm/0.25 μm, He; Program: 60 0C (2 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C (5 min) |
| Capillary | SE-52 | 1088. | Tognolini, Barocelli, et al., 2006 | 30. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min) |
| Capillary | CP Sil 8 CB | 1088. | Radudienë, Judpintienë, et al., 2005 | 50. m/0.32 mm/0.25 μm, He; Program: 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min) |
| Capillary | SE-30 | 1068. | Vinogradov, 2004 | Program: not specified |
| Capillary | DB-5 | 1085. | Isidorov, Zenkevich, et al., 1997 | Program: not specified |
| Capillary | Methyl Silicone | 1067. | Zenkevich, 1996 | Program: not specified |
Normal alkane RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-Wax | 1272. | Miyazawa, Kawauchi, et al., 2010 | 15. m/0.25 mm/0.25 μm, Helium, 4. K/min, 260. C @ 5. min; Tstart: 40. C |
| Capillary | DB-Wax | 1331. | Chida, Sone, et al., 2004 | 60. m/0.25 mm/0.5 μm, 35. C @ 5. min, 4. K/min, 240. C @ 10. min |
Normal alkane RI, polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP Innowax FSP | 1286. | Wedge, Klun, et al., 2009 | 60. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C (20 min) |
| Capillary | Carbowax 20M | 1286. | Vinogradov, 2004 | Program: not specified |
| Capillary | Innowax FSC | 1286. | Baser, Demirei, et al., 2002 | 60. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C |
| Capillary | Innowax FSC | 1286. | Kirimer, Tabanca, et al., 1999 | 60. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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. [all data]
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Constituents of stem and flower oils of Helichrysum litoreum Guss.,
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Tellez M., Estell R., et al., 2001
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Chida, M.; Sone, Y.; Tamura, H.,
Aroma characteristics of stored tobacco cut leaves analyzed by a high vacuum distillation and canister system,
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Wedge, Klun, et al., 2009
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. [all data]
Baser, Demirei, et al., 2002
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Micro-distilled volatile compounds from Ferulago species growing in Western Turkey,
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. [all data]
Kirimer, Tabanca, et al., 1999
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. [all data]
Notes
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