16β,17β-Estriol, 3TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-52830.Gerhardt, Ludwig-Köhn, et al., 198925. m/0.32 mm/0.25 μm, H2, 2. K/min; Tstart: 120. C; Tend: 270. C
CapillaryDB-52830.Gerhardt, Ludwig-Köhn, et al., 198925. m/0.32 mm/0.25 μm, H2, 2. K/min; Tstart: 120. C; Tend: 270. C
CapillaryDB-52886.Gerhardt, Ludwig-Köhn, et al., 198925. m/0.32 mm/0.25 μm, H2, 2. K/min; Tstart: 120. C; Tend: 270. C

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1200.2890.Dehennin and Scholler, 1969N2, Gas-Chrom Q; Column length: 1.50 m
PackedOV-1200.2905.Dehennin and Scholler, 1969N2, Gas-Chrom Q; Column length: 1.50 m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-302853.Fels, Dehennin, et al., 197520. m/0.25 mm/0.33 μm, 1.3 K/min; Tstart: 200. C; Tend: 250. C
CapillarySE-302861.Fels, Dehennin, et al., 197520. m/0.25 mm/0.33 μm, 200. C @ 10. min, 2.2 K/min; Tend: 250. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Gerhardt, Ludwig-Köhn, et al., 1989
Gerhardt, K.; Ludwig-Köhn, H.; Henning, H.V.; Remberg, G.; Zeeck, A., Identification of oestrogen metabolites in human urine by capillary gas chromatography and mass spectrometry, Biomed. Environ. Mass Spectrom., 1989, 18, 2, 87-95, https://doi.org/10.1002/bms.1200180202 . [all data]

Dehennin and Scholler, 1969
Dehennin, L.; Scholler, R., Correlation entre la structure moleculaire de quelques steroides en C18 et leurs grandeurs de retention en chromatographie en phase gazeuse, J. Steroid Biochem., 1969, 1, 1, 57-76, https://doi.org/10.1016/0022-4731(69)90009-0 . [all data]

Fels, Dehennin, et al., 1975
Fels, J.P.; Dehennin, L.; Scholler, R., Determination of estrogenes by gas-liquid chromatography with an open tubular column, J. Steroid Biochem., 1975, 6, 7, 1201-1203, https://doi.org/10.1016/0022-4731(75)90103-X . [all data]


Notes

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