n-Hexadecanoic acid

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5RTX-1BP-1DP-5SE-54
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.80.80.
Tend (C) 246.230.275.300.250.
Heat rate (K/min) 3.2.4.4.10.
Initial hold (min) 1.  1.2.
Final hold (min)  5. 40.10.
I 1965.1951.1973.1968.1969.
ReferenceAl-Qudah, Muhaidat, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dehshahri, Afsharypuor, et al., 2012Vijayakumar, Duraipandiyan, et al., 2012Buono-Core, Nunez, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5VF-5 MSVF-5 MSVF-5 MSHP-5 MS
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.30.30.40.40.
Tend (C) 240.260.260.250.260.
Heat rate (K/min) 3.2.2.5.4.
Initial hold (min) 2.  3. 
Final hold (min)  28.28.3.5.
I 1981.1962.1963.1963.1960.
ReferenceKahriman, Tosun, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011Liu, Lu, et al., 2011Miyazawa, Marumoto, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBDB-5 MSHP-5HP-5OV-1
Column length (m) 30.30.30.30.50.
Carrier gas NitrogenHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.250.250.2520.32
Phase thickness (μm) 0.260.250.250.250.50
Tstart (C) 45.70.50.60.40.
Tend (C) 280.290.300.240.270.
Heat rate (K/min) 3.5.50.3.2.
Initial hold (min)   5.  
Final hold (min) 22.10.5. 10.
I 1951.1958.1945.1963.1943.
ReferenceMothana, Hasson, et al., 2011Stojanovic, RAdulovic, et al., 2011Bi Kouame, Bedi, et al., 2010Cavar, Maksimovic, et al., 2010Da Costa, Yang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1SPB-1SPB-1OV-1HP-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.30.30.50.70.
Tend (C) 230.250.250.250.200.
Heat rate (K/min) 2.4.4.5.3.
Initial hold (min)  3.3.3.2.
Final hold (min) 30.10.10.2.18.
I 1951.1968.1968.1963.1953.
ReferenceDib, Djabou, et al., 2010Escalona-Arranz, Perez-Roses, et al., 2010Escalona-Arranz, Perez-Roses, et al., 2010Hu, Liang, et al., 2010Jerkovic, Hegic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSHP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.70.70.60.
Tend (C) 200.200.200.200.240.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 2.2.2.2.2.
Final hold (min) 18.18.18.18. 
I 1963.1963.1963.1963.1981.
ReferenceJerkovic, Hegic, et al., 2010Jerkovic and Marijanovic, 2010Jerkovic and Marijanovic, 2010Jerkovic, Tuberso, et al., 2010Kahriman, Tosun, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5 MSHP-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.70.70.70.70.
Tend (C) 250.290.290.290.290.
Heat rate (K/min) 5.5.5.5.5.
Initial hold (min) 3.    
Final hold (min) 15. 10. 10.
I 1968.1963.1968.1962.1968.
ReferenceLazarevic, Palic, et al., 2010Lazarevic, Radulovic, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSDB-5OV-1HP-5 MS
Column length (m) 60.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.35.70.40.70.
Tend (C) 250.195.240.300.290.
Heat rate (K/min) 4.2.5.4.5.
Initial hold (min) 1.5. 2. 
Final hold (min) 10.30. 10.10.
I 1943.1976.1942.1951.1963.
ReferenceSafaei-Ghomi, Meshkatalsadat, et al., 2010Kim and Chung, 2009Lawal and Oyedelji, 2009Nibret and Wink, 2009Radulovic, Blagojevic, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5 MSRTX-1HP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeliumNitrogenHeliumHeNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.50.60.50.
Tend (C) 280.280.230.230.280.
Heat rate (K/min) 4.5.4.2.5.
Initial hold (min)  1.4. 1.
Final hold (min)  1.10.35.1.
I 1984.1945.1991.1944.1978.
ReferenceZhao, Zeng, et al., 2009Bousaada, Ammar, et al., 2008Forero, Quijano, et al., 2008Paolini, Tomi, et al., 2008Saidana, Mahjoub, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5MSHP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.70.50.60.60.
Tend (C) 280.240.200.250.250.
Heat rate (K/min) 10.5.1.2.2.
Initial hold (min) 1. 1.8.8.
Final hold (min) 7.  15.15.
I 1960.1971.1976.1981.1974.
ReferenceSzarka, Hethelyi, et al., 2008Asekun, Olusegun, et al., 2007Calyecac-cortero, Cibrian-Tovar, et al., 2007Ferhat, Meklati, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5MSHP-101SE-30HP-5DB-5MS
Column length (m) 30.25.30.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 40.70.40.40.60.
Tend (C) 250.200.250.250.280.
Heat rate (K/min) 7.3.5.5.3.
Initial hold (min)  2.5.5. 
Final hold (min)   10.10.30.
I 2001.1968.1967.1963.1933.
ReferenceGhiasvand, Setkova, et al., 2007Jerkovic, Mastelic, et al., 2007Loizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Marongiu B., Piras A., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5SPB-5HP-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeliumHeliumHeHeliumHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.520.250.250.25
Tstart (C) 60.40.50.40.60.
Tend (C) 220.280.250.260.320.
Heat rate (K/min) 4.4.2.4.10.
Initial hold (min)      
Final hold (min)     4.
I 1984.1965.1954.1960.1968.
ReferenceMorteza-Semnani, Saeedi, et al., 2007Pavlovic, Petrovic, et al., 2007Raal, Orav, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Smelcerovic, Spiteller, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5MSHP-5HP-5MSHP-1HP-1
Column length (m) 30.30.30.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.20.2
Phase thickness (μm) 0.50.320.250.50.33
Tstart (C) 40.60.40.60.60.
Tend (C) 280.250.260.250.250.
Heat rate (K/min) 4.5.4.2.2.
Initial hold (min) 5.30.   
Final hold (min) 10.  120.60.
I 1968.1978.1959.61937.1937.
ReferenceTava, Pecetti, et al., 2007Yassa and Akhani, 2007Zizovic, Stamenic, et al., 2007Castel, Fernandez, et al., 2006Fernandez, Pintaric, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-5DB-1
Column length (m) 30.30.60.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 240.240.250.250.265.
Heat rate (K/min) 5.5.5.3.2.5
Initial hold (min) 2.2.  1.
Final hold (min)   10.10.20.
I 1936.1936.1949.1940.1935.
ReferenceGohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Hadian, Sonboli, et al., 2006Havlik, Kokoska, et al., 2006Iranshahi, Amin, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSDB-5DB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.95.
Tend (C) 260.280.280.220.240.
Heat rate (K/min) 3.5.5.4.4.
Initial hold (min)  4.4.  
Final hold (min)  10.10.  
I 1970.1931.1931.1973.1955.
ReferenceJavidnia, Miri, et al., 2006Kim, Abd El-Aty, et al., 2006Kim, El-Aty, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PE-5HP-5MSSPB-5HP-5HP-5MS
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeliumH2He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 100.40.60.50.60.
Tend (C) 280.260.250.280.280.
Heat rate (K/min) 3.4.4.4.3.
Initial hold (min) 1. 2.2. 
Final hold (min)   20.10. 
I 1974.1993.1970.1983.1959.
ReferencePandey-Rai S., Mallavarapu G.R., et al., 2006Petrovic, Ristic, et al., 2006Pino, Marquez, et al., 2006Pino, Sauri-Duch, et al., 2006Pitarokili, Tzakou, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.100.60.60.
Tend (C) 260.250.280.230.280.
Heat rate (K/min) 2.4.5.3.3.
Initial hold (min) 5.2. 3. 
Final hold (min) 20.10.20.10. 
I 1967.2009.1981.1997.1981.
ReferenceSenatore, Landolfi, et al., 2006Shen X., Gao Y., et al., 2006Singh G., Maurya S., et al., 2006Tohar, Mohd, et al., 2006Tzakou, Said, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-1DB-5DB-5HP-5
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.50.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.250.240.240.30.
Heat rate (K/min) 10.2.3.3.4.
Initial hold (min) 2.   3.
Final hold (min) 10.60.  15.
I 1969.1940.1968.1967.1939.
ReferenceWang, Yang, et al., 2006Bendimerad and Bendiab, 2005Chaverri and Cicció, 2005Chaverri and Cicció, 2005Ferretti, Maggi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-5HP-5DB-5
Column length (m) 25.30.30.60.30.
Carrier gas H2HeHeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 0.520.250.250.250.25
Tstart (C) 40.50.35.30.60.
Tend (C) 240.265.280.260.240.
Heat rate (K/min) 4.2.54.2.3.
Initial hold (min)  1.2.2. 
Final hold (min)  20. 28. 
I 1959.1978.1970.1972.21959.
ReferenceJovanovic, Kitic, et al., 2005Khanavi, Ghasemian, et al., 2005Kowalski, 2005Leffingwell and Alford, 2005Miyazawa, Nishiguchi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-5HP-5DB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.60.40.60.
Tend (C) 220.250.240.260.285.
Heat rate (K/min) 4.4.5.2.4.3
Initial hold (min) 4.2. 5. 
Final hold (min)  20. 20. 
I 1978.1981.1936.1967.1968.
ReferenceMorteza-Semnani and Saeedi, 2005Pino, Marbot, et al., 2005Saeidnia, Gohari, et al., 2005Senatore, Apostolides Arnold, et al., 2005Tesevic, Nikicevic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1HP-5HP-5HP-5
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.20.320.320.32
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 40.50.40.40.40.
Tend (C) 300.220.250.250.250.
Heat rate (K/min) 4.4.5.5.5.
Initial hold (min)  3.2.2.2.
Final hold (min) 5.30.5.5.5.
I 1968.1949.1958.1962.1965.
ReferenceUtsunomia, Kawata, et al., 2005Wong and Tan, 2005N/AN/AN/A
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5DB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeliumHeliumHeliumHe 
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.60.
Tend (C) 250.250.250.250.180.
Heat rate (K/min) 5.5.5.5.3.
Initial hold (min) 2.2.2.2.10.
Final hold (min) 5.5.5.10.10.
I 1971.1976.1977.1965.1970.
ReferenceN/AN/AN/AWu, Krings, et al., 2005bin Jantan, Ayop, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5BP-5DB-1
Column length (m) 25.30.30.25.30.
Carrier gas NitrogenHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.330.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.40.60.50.80.
Tend (C) 240.250.300.275.250.
Heat rate (K/min) 3.2.3.3.4.
Initial hold (min)  5.   
Final hold (min)  20.   
I 1975.1968.1937.1955.1950.
ReferenceJAvidnia, Mojab, et al., 2004Senatore, Rigano, et al., 2004Tirillini, Pellegrino, et al., 2004Ardakani, Mosaddegh, et al., 2003Mahalwal and Ali, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5SE-30DB-5
Column length (m) 30.30.30.50.25.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.75.40.70.40.
Tend (C) 280.220.260.240.280.
Heat rate (K/min) 4.3.2.4.3.
Initial hold (min) 10.4.5. 5.
Final hold (min) 40.   5.
I 1973.1984.1960.1946.1946.
ReferencePino, Marbot, et al., 2003Priestap, van Baren, et al., 2003Senatore and Bruno, 2003Iñigo, Palá-Paúl, et al., 2002Merle, Blázquez, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101SPB-5DB-5MSDB-5MS
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.50.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 220.250.250.270.270.
Heat rate (K/min) 4.2.4.3.3.
Initial hold (min) 5. 2.  
Final hold (min)   20.  
I 1977.1945.1980.1962.1958.
ReferenceMorteza-Semnani, Saeedi, et al., 2002Orav, Kailas, et al., 2002Pino, Marbot, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-1DB-5DB-5SPB-1CP Sil 5 CB
Column length (m) 25.30.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.200.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.4
Tstart (C) 50.60.60.50.60.
Tend (C) 250.270.270.250.260.
Heat rate (K/min) 3.3.3.2.5.
Initial hold (min) 3.   40.
Final hold (min)      
I 1976.1963.1965.1970.1937.
ReferenceBrun, Bessière, et al., 2001Palmeira, Conserva, et al., 2001Palmeira, Conserva, et al., 2001Vijayanand, Rao, et al., 2001Baser, Özek, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBOptima-1HP-5DB-1OV-101
Column length (m) 25.25.30.25.50.
Carrier gas HeHeH2HeNitrogen
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (μm) 0.40.250.250.13 
Tstart (C) 60.50.40.60.40.
Tend (C) 260.250.280.200.200.
Heat rate (K/min) 5.3.3.4.2.
Initial hold (min) 40.3.10.2.10.
Final hold (min)   10.  
I 1937.1965.1986.1983.1956.
ReferenceBaser, Özek, et al., 2000de Beck, Bessière, et al., 2000Bicalho, Pereira, et al., 2000Rapior, Konska, et al., 2000Tamura, Boonbumrung, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSMethyl SiliconeSE-30HP-1CP Sil 5 CB
Column length (m) 30.50.30.25.25.
Carrier gas HeH2 H2N2
Substrate      
Column diameter (mm) 0.250.250.250.32 
Phase thickness (μm) 0.250.5 0.170.39
Tstart (C) 40.40.50.40.60.
Tend (C) 280.260.300.260.220.
Heat rate (K/min) 10.4.10.3.5.
Initial hold (min) 1.0.5 5. 
Final hold (min) 20. 4.  
I 1974.1944.1953.1946.1936.
ReferenceTkachev, Dobrotvorsky, et al., 2000Vendramini and Trugo, 2000Zhou, Robards, et al., 2000Lopes, Koketsu, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSE-54CP Sil 5 CBDB-1Cross-Linked Methylsilicone
Column length (m) 30.25.25.60.25.
Carrier gas He He He
Substrate      
Column diameter (mm) 0.250.310.250.320.32
Phase thickness (μm) 0.25 0.25  
Tstart (C) 60.35.60.50.35.
Tend (C) 240.250.300.230.225.
Heat rate (K/min) 3.4.6.4.4.
Initial hold (min)  3.  3.
Final hold (min)    10. 
I 1967.1963.1946.1941.1944.
ReferenceZoghbi, Andrade, et al., 1999Ding, Deng, et al., 1998Bos, Woerdenbag, et al., 1997Binder and French, 1994Bravo and Hotchkiss, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-2DB-5DB-5Ultra-1DB-1
Column length (m) 50.60.60.25.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.320.250.320.25
Phase thickness (μm) 0.521.00.250.250.25
Tstart (C) 40.40.40.80.50.
Tend (C) 250.240.250.260.240.
Heat rate (K/min) 4.3.2.3.3.
Initial hold (min) 3. 5.  
Final hold (min) 30.    
I 1969.1957.1961.1964.1947.
ReferenceKing, Hamilton, et al., 1993Berdague, Denoyer, et al., 1991Lee, Macku, et al., 1991Okumura, 1991Shiota, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101OV-101SE-54
Column length (m) 60.50.50.25.
Carrier gas HeNitrogenNitrogenN2
Substrate     
Column diameter (mm) 0.250.250.250.25
Phase thickness (μm) 0.25   
Tstart (C) 50.70.80.60.
Tend (C) 240.200.200.260.
Heat rate (K/min) 3.2.2.6.
Initial hold (min)    2.
Final hold (min)     
I 1957.1944.1950.1973.
ReferenceShiota, 1991Sugisawa, Nakamura, et al., 1990Sugisawa, Nakamura, et al., 1990Bestmann, Classen, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Lawal and Oyedelji, 2009
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Paolini, Tomi, et al., 2008
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Ferhat, Meklati, et al., 2007
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Morteza-Semnani, Saeedi, et al., 2007
Morteza-Semnani, K.; Saeedi, M.; Akbarzadeh, M., Essential oil composition of Teucrium scordium L., Acta Pharm., 2007, 57, 4, 499-504, https://doi.org/10.2478/v10007-007-0040-6 . [all data]

Pavlovic, Petrovic, et al., 2007
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Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M., Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia, Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]

Ristic, Krivokuca-Dokic, et al., 2007
Ristic, M.; Krivokuca-Dokic, D.; Radanovic, D.; Nastovski, T., Etarsko ulje Arnica montata i Arnica chamissonis, Hem. Ind., 2007, 61, 5, 272-277, https://doi.org/10.2298/HEMIND0704272R . [all data]

Smelcerovic, Spiteller, et al., 2007
Smelcerovic, A.; Spiteller, M.; Ligon, A.P.; Smelcerovic, Z.; Raabe, N., Essential oil composition of Hypericum L. species from Southeastern Serbia and their chemotaxonomy, Biochem. Syst. Ecol., 2007, 35, 2, 99-113, https://doi.org/10.1016/j.bse.2006.09.012 . [all data]

Tava, Pecetti, et al., 2007
Tava, A.; Pecetti, L.; Ricci, M.; Pagnotta, M.A.; Russi, L., Volatile compounds from leaves and flowers of Bituminaria bituminosa (L.) Stirt. (Fabaceae) from Italy, Flavour Fragr. J., 2007, 22, 5, 363-370, https://doi.org/10.1002/ffj.1806 . [all data]

Yassa and Akhani, 2007
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2007, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Zizovic, Stamenic, et al., 2007
Zizovic, I.; Stamenic, M.; Ivanovic, J.; Orlovic, A.; Ristic, M.; Djordjevic, S.; Petrovic, S.D.; Skala, D., Supercritical carbon dioxide extraction of sesquiterpenes from valerian root, J. Supercrit. Fluids, 2007, 43, 2, 249-258, https://doi.org/10.1016/j.supflu.2007.05.007 . [all data]

Castel, Fernandez, et al., 2006
Castel, C.; Fernandez, X.; Lizzani-Cuvelier, L.; Perichet, C.; Lavoine, S., Characterization of the Chemical Composition of a Byproduct from Siam Benzoin Gum, J. Agric. Food Chem., 2006, 54, 23, 8848-8854, https://doi.org/10.1021/jf061193y . [all data]

Fernandez, Pintaric, et al., 2006
Fernandez, X.; Pintaric, C.; Lizzani-Cuvelier, L.; Loiseau, A.-M.; Morello, A.; Pellerin, P., Chemical composition of absolute and supercritical carbon dioxide extract of Aframomum melegueta, Flavour Fragr. J., 2006, 21, 1, 162-165, https://doi.org/10.1002/ffj.1554 . [all data]

Gohari, Hadjiakhoondi, et al., 2006
Gohari, A.R.; Hadjiakhoondi, A.; Sadat-Ebrahimi, E.; Saeidnia, S.; Shafiee, A., Composition of the volatile oils of Satureja spicigera C. Koch Boiss. and S. macrantha C. A. Mey from Iran, Flavour Fragr. J., 2006, 21, 2, 348-350, https://doi.org/10.1002/ffj.1642 . [all data]

Gohari A.R., Hadjiakhoondi A., et al., 2006
Gohari A.R.; Hadjiakhoondi A.; Sadat-Ebrahimi E.; Saeidnia S.; Shafiee A., Composition of the volatile oils of Satureja spicigera C. Koch Boiss. and S-macrantha C. A. Mey from Iran, Flavour Fragr. J., 2006, 21, 3, 510-512, https://doi.org/10.1002/ffj.1613 . [all data]

Hadian, Sonboli, et al., 2006
Hadian, J.; Sonboli, A.; Ebrahimi, S.N.; Mirjalili, M.H., Essential oil composition of Nepeta satureioides from Iran, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 2, 175-177, https://doi.org/10.1007/s10600-006-0071-0 . [all data]

Havlik, Kokoska, et al., 2006
Havlik, J.; Kokoska, L.; Vasickova, S.; Valterova, I., Chemical composition of essential oil from the seeds of Nigella arvensis L. and assessment of its actimicrobial activity, Flavour Fragr. J., 2006, 21, 4, 713-717, https://doi.org/10.1002/ffj.1713 . [all data]

Iranshahi, Amin, et al., 2006
Iranshahi, M.; Amin, G.; Sourmaghi, M.S.; Shafiee, A.; Hadjiakhoondi, A., Sulphur-containing compounds in the essential oil of the root of Ferula persica Willd. var. persica, Flavour Fragr. J., 2006, 21, 2, 260-261, https://doi.org/10.1002/ffj.1574 . [all data]

Javidnia, Miri, et al., 2006
Javidnia, K.; Miri, R.; Kamalinejad, M.; Mehdipour, A.R., Composition of the essential oil of Diplotaenia cachrydifolia Boiss. from Iran, J. Ess. Oil Res., 2006, 18, 1, 86-87, https://doi.org/10.1080/10412905.2006.9699393 . [all data]

Kim, Abd El-Aty, et al., 2006
Kim, M.R.; Abd El-Aty, A.M.; Kim, I.S.; Shim, J.H., Determination of volatile flavor components in danggui cultivars by solvent free injection and hydrodistillation followed by gas chromatographic-mass spectrometric analysis, J. Chromatogr. A, 2006, 1116, 1-2, 259-264, https://doi.org/10.1016/j.chroma.2006.03.060 . [all data]

Kim, El-Aty, et al., 2006
Kim, M.R.; El-Aty, A.M.A.; Choi, J.-H.; Lee, K.B.; Shim, J.H., Identification of volatile components in Angelica species using supercritical-CO2 fluid extraction and solid phase microextraction coupled to gas chromatography-mass spectrometry, Biomedical Chromatography, 2006, 20, 11, 1267-1273, https://doi.org/10.1002/bmc.696 . [all data]

Morteza-Semnani, Akbarzadeh, et al., 2006
Morteza-Semnani, K.; Akbarzadeh, M.; Changizi, S., Essential oils composition of Stachys byzantina, S. inflata, S. lavandulifolia and S. laxa from Iran, Flavour Fragr. J., 2006, 21, 2, 300-303, https://doi.org/10.1002/ffj.1594 . [all data]

Pala-Paul J., Perez-Alonso M.J., et al., 2006
Pala-Paul J.; Perez-Alonso M.J.; Velasco-Negueruela A.; Ballesteros M.T.; Sanz J., Essential oil composition of Sideritis hirsuta L. from Guadalajara Province, Spain, Flavour Fragr. J., 2006, 21, 3, 410-415, https://doi.org/10.1002/ffj.1727 . [all data]

Pandey-Rai S., Mallavarapu G.R., et al., 2006
Pandey-Rai S.; Mallavarapu G.R.; Naqvi A.A.; Yadav A.; Rai S.K.; Srivastava S.; Singh D.; Mishra R.; Kumar S., Volatile components of leaves and flowers of periwinkle Catharanthus roseus (L.) G. Don from New Delhi, Flavour Fragr. J., 2006, 21, 3, 427-430, https://doi.org/10.1002/ffj.1606 . [all data]

Petrovic, Ristic, et al., 2006
Petrovic, S.; Ristic, M.; Milenkovic, M.; Kukic, J.; Antic-Stankovic, J.; Niketic, M., Composition and antimicrobial activity of essential oil of Stachys plumosa Griseb., Flavour Fragr. J., 2006, 21, 2, 250-252, https://doi.org/10.1002/ffj.1570 . [all data]

Pino, Marquez, et al., 2006
Pino, J.A.; Marquez, E.; Marbot, R., Volatile constituents from tea of roselle (Hibiscus sabdariffa L.), Rev. CENIC Ciencias Quimicas, 2006, 37, 3, 127-129. [all data]

Pino, Sauri-Duch, et al., 2006
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Notes

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