2-Pentenedioic acid, 3-methyl-, bis(trimethylsilyl) ester
- Formula: C12H24O4Si2
- Molecular weight: 288.4876
- IUPAC Standard InChI: InChI=1S/C12H24O4Si2/c1-10(8-11(13)15-17(2,3)4)9-12(14)16-18(5,6)7/h8H,9H2,1-7H3/b10-8+
- IUPAC Standard InChIKey: CWJVRLKZONLMHK-CSKARUKUSA-N
- CAS Registry Number: 55887-63-3
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: 3-Methylglutaconic acid, bis(trimethylsilyl) ester; 3-Methylglutaconic acid, di(trimethylsilyl) ester; 3-Methylglutaconic acid, di-TMS; Bis(trimethylsilyl) 3-methyl-2-pentenedioate; 3-Methylglutaconic acid, di-TMS ester; 3-Methylglutaconic acid, di-TMS, #2; 3-Methylglutaconic acid, di-TMS, #1
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-1 | 1441. | Lefevere, Verhaeghe, et al., 1989 | 10. m/0.22 mm/0.17 μm, He, 5. K/min; Tstart: 70. C; Tend: 270. C |
| Capillary | SE-52 | 1450. | Lefevere, Verhaeghe, et al., 1989 | 25. m/0.32 mm/0.52 μm, He, 5. K/min; Tstart: 70. C; Tend: 270. C |
| Capillary | SE-52 | 1494. | Lefevere, Verhaeghe, et al., 1989 | 25. m/0.32 mm/0.52 μm, He, 5. K/min; Tstart: 70. C; Tend: 270. C |
| Capillary | SE-52 | 1451. | Lefevere, Verhaeghe, et al., 1988 | 25. m/0.20 mm/0.40 μm, He, 5. K/min; Tstart: 50. C; Tend: 270. C |
| Capillary | SE-52 | 1491. | Lefevere, Verhaeghe, et al., 1988 | 25. m/0.20 mm/0.40 μm, He, 5. K/min; Tstart: 50. C; Tend: 270. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Lefevere, Verhaeghe, et al., 1989
Lefevere, M.F.; Verhaeghe, B.J.; Declerck, D.H.; Van Bocxlaer, J.F.; De Leenheer, A.P.; De Sagher, R.M.,
Metabolic Profiling of Urinary Organic Acids by Single and Multicolumn Capillary Gas Chromatography,
J. Chromatogr. Sci., 1989, 27, 1, 23-29, https://doi.org/10.1093/chromsci/27.1.23
. [all data]
Lefevere, Verhaeghe, et al., 1988
Lefevere, M.F.; Verhaeghe, B.J.; Declerck, D.M.; de Leenheer, A.P.,
Automated profiling of urinary organic acids by dual-column gas chromatography and gas chromatography/mass spectrometry,
Biomed. Environ. Mass Spectrom., 1988, 15, 6, 311-322, https://doi.org/10.1002/bms.1200150603
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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