2,6-Nonadienal, (E,Z)-


Van Den Dool and Kratz RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-FFAPFFAPFFAPFFAPDB-Wax
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.50.250.250.250.5
Tstart (C) 35.35.35.35.40.
Tend (C) 225.225.225.225.240.
Heat rate (K/min) 4.10.10.10.7.
Initial hold (min) 5.5.5.5. 
Final hold (min) 30.25.25.25.5.
I 1596.1581.1589.1596.1595.
ReferenceJarunrattanasri, Theerakulkait, et al., 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Miracle E.R., et al., 2007Mahattanatawee K., Perez-Cacho P.R., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FFAPDB-WaxHP-WaxCP-Wax 52CBDB-Wax
Column length (m) 30.30.30.60.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm)  0.250.250.250.5
Tstart (C) 40.50.60.40.50.
Tend (C) 240.230.220.250.260.
Heat rate (K/min) 8.10.5.4.4.
Initial hold (min) 2.5.10.  
Final hold (min) 5.25.  5.
I 1570.1590.1573.1598.1587.
ReferenceSchlutt B., Moran N., et al., 2007Fernandez-Segovia, Escriche, et al., 2006Flamini, Tebano, et al., 2006Kourkoutas, Elmore, et al., 2006Selli, Rannou, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-FFAPStabilwaxStabilwaxSupelcowax-10
Column length (m) 30.30.60.60.30.
Carrier gas  N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.30.40.40.60.
Tend (C) 200.250.240.240.240.
Heat rate (K/min) 10.3.3.3.3.
Initial hold (min) 3.2.5.5.5.
Final hold (min) 20.2.10.10.10.
I 1555.1577.1598.1585.1577.
ReferenceCarunchia Whetstine, Croissant, et al., 2005Colahan-Sederstrom and Peterson, 2005Cros S., Lignot B., et al., 2005Cros, Lignot, et al., 2005Riu-Aumatell, Lopez-Tamames, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-FFAPDB-WaxDB-Wax
Column length (m) 30.30.15.30.30.
Carrier gas   HeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.250.250.500.5
Tstart (C) 40.40.35.40.40.
Tend (C) 200.200.225.240.230.
Heat rate (K/min) 10.10.10.7.5.
Initial hold (min) 3.5.5. 2.
Final hold (min) 20.15.15.5.10.
I 1573.1583.1589.1596.1604.
ReferenceWhetstine, Cadwallader, et al., 2005Avsar, Karagul-Yuceer, et al., 2004Avsar, Karagul-Yuceer, et al., 2004Bell, 2004Mahajan, Goddik, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxInnowax
Column length (m) 30.30.30.30.15.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.35.
Tend (C) 200.200.200.200.225.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 5.5.5.5.5.
Final hold (min) 20.20.20.20.20.
I 1553.1555.1563.1556.1593.
ReferenceYu, Kim, et al., 2004Yu, Kim, et al., 2004, 2Zheng, Kim, et al., 2004Zheng, Kim, et al., 2004Chisholm, Jell, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase StabilwaxDB-WaxDB-FFAPZB-WaxZB-Wax
Column length (m) 60.60.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.40.35.40.40.
Tend (C) 240.220.200.220.220.
Heat rate (K/min) 3.3.10.3.3.
Initial hold (min) 5.10.5.  
Final hold (min) 10.30.30.  
I 1585.1582.1578.1573.1573.
ReferenceCros, Vandanjon, et al., 2003Hayata, Sakamoto, et al., 2003Karagül-Yüceer, Vlahovich, et al., 2003Brunton, Cronin, et al., 2002Brunton, Cronin, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10DB-WaxDB-WaxDB-WaxSupelcowax-10
Column length (m) 60.30.30.30.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.530.25
Phase thickness (μm) 0.250.251.1.0.25
Tstart (C) 35.35.40.40.35.
Tend (C) 195.200.200.200.195.
Heat rate (K/min) 2.10.10.10.2.
Initial hold (min) 5.5.5.5.5.
Final hold (min) 90.30.30.30.90.
I 1591.1568.1579.1579.1591.
ReferenceChung, Yung, et al., 2002Karagül-Yüceer, Cadwallader, et al., 2002Wu and Cadwallader, 2002Wu and Cadwallader, 2002Chung, Yung, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 30.30.60.60.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 35.40.40.40.40.
Tend (C) 200.200.200.200.250.
Heat rate (K/min) 10.2.2.2.4.
Initial hold (min) 5.5.  2.
Final hold (min) 30.20.  10.
I 1583.1593.1593.1593.1594.
ReferenceKaragül-Yüceer, Drake, et al., 2001Kim, Shin, et al., 2001Lee, Suriyaphan, et al., 2001Lee, Suriyaphan, et al., 2001Le Guen, Prost, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10FFAPDB-WaxDB-WaxDB-Wax
Column length (m) 60.60.30.60.30.
Carrier gas He   He
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.250.50.250.250.25
Tstart (C) 35.50.40.40.40.
Tend (C) 195.230.200.200.200.
Heat rate (K/min) 2.5.6.3.6.
Initial hold (min) 5.3.5.5.5.
Final hold (min) 90.15.30.60.30.
I 1593.1629.1574.1580.1570.
ReferenceChung, 1999Stephan and Steinhart, 1999Cha and Cadwallader, 1998Cha, Kim, et al., 1998Cha, Kim, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10DB-WaxDB-WaxDB-WaxSupelcowax-10
Column length (m) 60.60.60.60.60.
Carrier gas He  He 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.50.50.40.
Tend (C) 200.230.230.230.175.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 5.   5.
Final hold (min) 30. 60.60.20.
I 1583.1576.1590.1590.1592.
ReferenceCadwallader, Tan, et al., 1995Shimoda, Shigematsu, et al., 1995Shiratsuchi, Shimoda, et al., 1994Shiratsuchi, Shimoda, et al., 1994, 2Tanchotikul and Hsieh, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase Supelcowax-10Carbowax 20M
Column length (m) 60.50.
Carrier gas  H2
Substrate   
Column diameter (mm) 0.250.2
Phase thickness (μm) 0.25 
Tstart (C) 40.50.
Tend (C) 175.200.
Heat rate (K/min) 2.2.
Initial hold (min) 5. 
Final hold (min) 20.55.
I 1596.1548.
ReferenceTanchotikul and Hsieh, 1989Wu and Liou, 1986
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jarunrattanasri, Theerakulkait, et al., 2007
Jarunrattanasri, A.; Theerakulkait, C.; Cadwallader, K.R., Aroma Components of Acid-Hydrolyzed Vegetable Protein Made by Partial Hydrolysis of Rice Bran Protein, J. Agric. Food Chem., 2007, 55, 8, 3044-3050, https://doi.org/10.1021/jf0631474 . [all data]

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Carunchia Whetstine, Croissant, et al., 2005
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Whetstine, Cadwallader, et al., 2005
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Avsar, Karagul-Yuceer, et al., 2004
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Bell, 2004
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Yu, Kim, et al., 2004, 2
Yu, E.J.; Kim, T.H.; Kim, K.H.; Lee, H.J., Characterization of aroma-active compounds of Abies nephrolepis (Khingan fir) needles using aroma extract dilution analysis, Flavour Fragr. J., 2004, 19, 1, 74-79, https://doi.org/10.1002/ffj.1314 . [all data]

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Cros, Vandanjon, et al., 2003
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Lee, Suriyaphan, et al., 2001
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Chung, 1999
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Cha and Cadwallader, 1998
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Cha, Kim, et al., 1998
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Cadwallader, Tan, et al., 1995
Cadwallader, K.R.; Tan, Q.; Chen, F.; Meyers, S.P., Evaluation of the aroma of cooked spiny lobster tail meat by aroma extract dilution analysis, J. Agric. Food Chem., 1995, 43, 9, 2432-2437, https://doi.org/10.1021/jf00057a022 . [all data]

Shimoda, Shigematsu, et al., 1995
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Shiratsuchi, Shimoda, et al., 1994
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Shiratsuchi, Shimoda, et al., 1994, 2
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Tanchotikul and Hsieh, 1989
Tanchotikul, U.; Hsieh, T.C.-Y., Volatile Flavor Components in Crayfish Waste, J. Food Sci., 1989, 54, 6, 1515-1520, https://doi.org/10.1111/j.1365-2621.1989.tb05149.x . [all data]

Wu and Liou, 1986
Wu, C.-M.; Liou, S.-E., Effect of tissue disruption of volatile constituents of bell peppers, J. Agric. Food Chem., 1986, 34, 4, 770-772, https://doi.org/10.1021/jf00070a044 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References