Glycine, N-(3-methyl-1-oxo-2-butenyl)-N-(trimethylsilyl)-, trimethylsilyl ester
- Formula: C13H27NO3Si2
- Molecular weight: 301.5294
- IUPAC Standard InChI: InChI=1S/C13H27NO3Si2/c1-11(2)9-12(15)14(18(3,4)5)10-13(16)17-19(6,7)8/h9H,10H2,1-8H3
- IUPAC Standard InChIKey: RJILLMNUANBLCE-UHFFFAOYSA-N
- CAS Registry Number: 55649-86-0
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: β-Methyl crotonyl glycine bis(trimethylsilyl)-
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 1563. | Ramsdell and Tanaka, 1980 | N2, Anakrom, 4. K/min; Column length: 2. m; Tstart: 80. C |
| Packed | OV-1 | 1563. | Tanaka, Hine, et al., 1980 | N2, 100-120 mesh, 70. C @ 0.5 min, 28. K/min; Column length: 1.8 m; Tend: 290. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Ramsdell and Tanaka, 1980
Ramsdell, H.S.; Tanaka, K.,
Gas chromatographic retention indices of twenty metabolically important acylglycines as trimethylsilyl derivatives,
J. Chromatogr., 1980, 181, 1, 90-94, https://doi.org/10.1016/S0378-4347(00)81273-6
. [all data]
Tanaka, Hine, et al., 1980
Tanaka, K.; Hine, D.G.; West-Dull, A.; Lynn, T.B.,
Gas-chromatographic method of analysis for urinary organic acids. I. Retention indices of 155 metabolically important compounds,
Clin. Chem., 1980, 26, 13, 1839-1846. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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