Glycine, N-(1-oxopentyl)-N-(trimethylsilyl)-, trimethylsilyl ester
- Formula: C13H29NO3Si2
- Molecular weight: 303.5453
- IUPAC Standard InChI: InChI=1S/C13H29NO3Si2/c1-8-9-10-12(15)14(18(2,3)4)11-13(16)17-19(5,6)7/h8-11H2,1-7H3
- IUPAC Standard InChIKey: NPOYZFNGZIGKET-UHFFFAOYSA-N
- CAS Registry Number: 55530-59-1
- Chemical structure:
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Gas Chromatography
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 1559. | Ramsdell and Tanaka, 1980 | N2, Anakrom, 4. K/min; Column length: 2. m; Tstart: 80. C |
| Packed | OV-1 | 1559. | Tanaka, Hine, et al., 1980 | N2, 100-120 mesh, 70. C @ 0.5 min, 28. K/min; Column length: 1.8 m; Tend: 290. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-101 | 1559. | Tanaka and Hine, 1982 | Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Ramsdell and Tanaka, 1980
Ramsdell, H.S.; Tanaka, K.,
Gas chromatographic retention indices of twenty metabolically important acylglycines as trimethylsilyl derivatives,
J. Chromatogr., 1980, 181, 1, 90-94, https://doi.org/10.1016/S0378-4347(00)81273-6
. [all data]
Tanaka, Hine, et al., 1980
Tanaka, K.; Hine, D.G.; West-Dull, A.; Lynn, T.B.,
Gas-chromatographic method of analysis for urinary organic acids. I. Retention indices of 155 metabolically important compounds,
Clin. Chem., 1980, 26, 13, 1839-1846. [all data]
Tanaka and Hine, 1982
Tanaka, K.; Hine, D.G.,
Compilation of Gas Chromatographic Retention Indices of 163 Metabolically Important Organic Acids, and Their Use in Detection of Patients with Organic Acidurias,
J. Chromatogr., 1982, 239, 301-322, https://doi.org/10.1016/S0021-9673(00)81990-1
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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