Indoleacrylic acid, 2TMS derivative
- Formula: C17H25NO2Si2
- Molecular weight: 331.5569
- IUPAC Standard InChI: InChI=1S/C17H25NO2Si2/c1-21(2,3)18-13-14(15-9-7-8-10-16(15)18)11-12-17(19)20-22(4,5)6/h7-13H,1-6H3/b12-11+
- IUPAC Standard InChIKey: QGUSJWZJGZJSGS-VAWYXSNFSA-N
- CAS Registry Number: 55124-88-4
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 2-Propenoic acid, 3-[1-(trimethylsilyl)-1H-indol-3-yl]-, trimethylsilyl ester; Trimethylsilyl 3-[1-(trimethylsilyl)-1H-indol-3-yl]-2-propenoate; Indole-3-acrylic acid, N,O-bis-TMS; Indole-3-acrylic acid, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 2357. | Butts, 1972 | He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 2402.2 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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