(E)-1-Methyl-4-(6-methylhept-5-en-2-ylidene)cyclohex-1-ene
- Formula: C15H24
- Molecular weight: 204.3511
- IUPAC Standard InChI: InChI=1S/C15H24/c1-12(2)6-5-7-14(4)15-10-8-13(3)9-11-15/h6,8H,5,7,9-11H2,1-4H3/b15-14-
- IUPAC Standard InChIKey: XBGUIVFBMBVUEG-PFONDFGASA-N
- CAS Registry Number: 53585-13-0
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: Cyclohexene, 4-(1,5-dimethyl-4-hexen-1-ylidene)-1-methyl-, (E)-; Cyclohexene, 4-(1,5-dimethyl-4-hexenylidene)-1-methyl-, (E)-; (E)-γ-Bisabolene; trans-γ-Bisabolene; γ-Bisabolene; γ-E-Bisabolene; (E)-iso-γ-Bisabolene
- Permanent link for this species. Use this link for bookmarking this species for future reference.
- Information on this page:
- Other data available:
- Options:
Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-5 MS | DB-5 | HP-5 | DB-5 | SLB-5 MS |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | Helium | Helium | Hydrogen | Helium | Helium |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. | 70. | 35. | 50. |
| Tend (C) | 230. | 240. | 290. | 220. | 250. |
| Heat rate (K/min) | 3. | 3. | 5. | 3. | 3. |
| Initial hold (min) | 2. | ||||
| Final hold (min) | 40. | 10. | |||
| I | 1538. | 1525. | 1538. | 1531. | 1528. |
| Reference | Pripdeevech and Saansoomchai, 2013 | Magalhaes, Lima, et al., 2010 | Radulovic, Dordevic, et al., 2010 | El-Massry, El-Ghorab, et al., 2009 | Lo Presti, Sciarrone, et al., 2008 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-5 | CP Sil 5 CB | DB-5 | DB-5 | HP-5MS |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | Helium | N2 | He | Helium | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.26 | 0.26 | 0.25 |
| Phase thickness (μm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. | 60. | 60. | 60. |
| Tend (C) | 250. | 300. | 240. | 290. | 250. |
| Heat rate (K/min) | 5. | 4. | 3. | 3. | 2. |
| Initial hold (min) | 30. | 8. | |||
| Final hold (min) | 15. | ||||
| I | 1535. | 1524. | 1527. | 1527. | 1527. |
| Reference | Yassa and Akhani, 2008 | Baran, von Reuss, et al., 2007 | Bos, Woerdenbag, et al., 2007 | Elfami, Bos, et al., 2007 | Ferhat, Meklati, et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-5MS | DB-5 | DB-5 | HP-5 | HP-5 |
| Column length (m) | 30. | 30. | 30. | 25. | 30. |
| Carrier gas | He | He | Helium | H2 | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.2 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.33 | 0.32 |
| Tstart (C) | 60. | 60. | 60. | 60. | 60. |
| Tend (C) | 250. | 240. | 220. | 240. | 250. |
| Heat rate (K/min) | 2. | 2. | 4. | 3. | 5. |
| Initial hold (min) | 8. | 30. | |||
| Final hold (min) | 15. | ||||
| I | 1531. | 1520. | 1533. | 1533. | 1535. |
| Reference | Ferhat, Tigrine-Kordjani, et al., 2007 | Miyazawa and Tamura, 2007 | Morteza-Semnani, Saeedi, et al., 2007 | Oliveira, Leitão, et al., 2007 | Yassa and Akhani, 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-5 | DB-1 | DB-5 | RTX-1 | DB-5 |
| Column length (m) | 30. | 60. | 30. | 30. | 30. |
| Carrier gas | He | Nitrogen | Helium | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.26 | 0.32 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 60. | 40. | 60. | 60. | 50. |
| Tend (C) | 300. | 200. | 290. | 300. | 250. |
| Heat rate (K/min) | 3. | 2. | 3. | 4. | 3. |
| Initial hold (min) | 1. | 5. | |||
| Final hold (min) | 9. | ||||
| I | 1523. | 1518. | 1527. | 1531. | 1538. |
| Reference | Apel, Sobral, et al., 2006 | Chen, Sheu, et al., 2006 | Elfami, Komar, et al., 2006 | Kula, Izydorczyk, et al., 2006 | Navaei and Mirza, 2006 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | SPB-5 | HP-5 MS | DB-5MS | DB-5 | DB-1 |
| Column length (m) | 30. | 30. | 50. | 60. | |
| Carrier gas | He | Helium | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.3 | 0.25 | |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 50. | 60. | 60. | 60. | 50. |
| Tend (C) | 250. | 250. | 240. | 240. | 250. |
| Heat rate (K/min) | 5. | 2. | 3. | 2. | 4. |
| Initial hold (min) | 3. | 8. | 5. | ||
| Final hold (min) | 15. | 15. | |||
| I | 1515. | 1531. | 1534. | 1531. | 1532. |
| Reference | Stojanovic, Palic, et al., 2006 | Tigrine-Kordiani, Meklati, et al., 2006 | Busman, Zoghbi, et al., 2005 | Chagonda and Chalchat, 2005 | Khajeh, Yamini, et al., 2005 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-5 | HP-5MS | HP-5 | DB-5 | HP-5 |
| Column length (m) | 30. | 30. | 30. | 30. | 60. |
| Carrier gas | He | He | Helium | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 60. | 60. | 70. | 60. | 40. |
| Tend (C) | 300. | 220. | 210. | 240. | 250. |
| Heat rate (K/min) | 3. | 5. | 2. | 3. | 5. |
| Initial hold (min) | 20. | 15. | |||
| Final hold (min) | 20. | 60. | |||
| I | 1531. | 1541. | 1533. | 1535. | 1530. |
| Reference | Tirillini, Pellegrino, et al., 2004 | Feizbaksh, Saber Tehrani, et al., 2003 | Mookdasanit, Tamura, et al., 2003 | da Silva, Luz, et al., 2003 | Stashenko, Jaramillo, et al., 2003 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | HP-5 | HP-5 | HP-5 | DB-5 | DB-5 |
| Column length (m) | 60. | 25. | 25. | 30. | 30. |
| Carrier gas | H2 | H2 | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.249 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.53 | 0.53 | 0.25 | 0.25 |
| Tstart (C) | 40. | 40. | 40. | 60. | 35. |
| Tend (C) | 250. | 280. | 280. | 300. | 280. |
| Heat rate (K/min) | 5. | 4. | 4. | 3. | 4. |
| Initial hold (min) | 15. | 2. | |||
| Final hold (min) | 5. | 15. | |||
| I | 1515. | 1531. | 1532. | 1527. | 1539. |
| Reference | Stashenko, Jaramillo, et al., 2003 | Velickovic, Randjelovic, et al., 2003 | Velickovic, Randjelovic, et al., 2003 | Bos, Koulman, et al., 2002 | Krauze-Baranowska, Mardarowicz, et al., 2002 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-5MS | HP-5 | DB-1 | DB-1 | DB-1 |
| Column length (m) | 30. | 30. | 33. | 30. | 25. |
| Carrier gas | He | N2 | N2 | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.50 | 0.25 | 0.25 |
| Tstart (C) | 60. | 60. | 50. | 45. | 50. |
| Tend (C) | 240. | 220. | 135. | 300. | 290. |
| Heat rate (K/min) | 3. | 5. | 20. | 15. | 4. |
| Initial hold (min) | 10. | 2. | 2. | ||
| Final hold (min) | 5. | ||||
| I | 1535. | 1535. | 1529. | 1515. | 1527. |
| Reference | Maia, Zoghbi, et al., 2002 | Gallori, Flamini, et al., 2001 | Feger, Brandauer, et al., 2000 | Hedin, McKibben, et al., 2000 | Koulman, 1999 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | CP Sil 5 CB | CBP-1 |
| Column length (m) | 25. | 30. |
| Carrier gas | He | He |
| Substrate | ||
| Column diameter (mm) | 0.25 | 0.25 |
| Phase thickness (μm) | ||
| Tstart (C) | 50. | 60. |
| Tend (C) | 230. | 240. |
| Heat rate (K/min) | 3. | 4. |
| Initial hold (min) | ||
| Final hold (min) | ||
| I | 1531. | 1510. |
| Reference | Oyedeji, Olawore, et al., 1999 | Lamarque, Maestri, et al., 1998 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Pripdeevech and Saansoomchai, 2013
Pripdeevech, P.; Saansoomchai, J.,
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Chagonda and Chalchat, 2005
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The essential oil of wild and cultivated Hoslundia opposita Vahl. from Zimbabwe,
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Tirillini, Pellegrino, et al., 2004
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Feizbaksh, Saber Tehrani, et al., 2003
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Essential oils composition of Eupatorium species growing wild in the Amazon,
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Gallori, Flamini, et al., 2001
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Chemical composition of some traditional herbal drug preparations: essential oil and aromatic water of costmary (Balsamita suaveolens Pers.),
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Feger, Brandauer, et al., 2000
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Sesquiterpene hydrocarbons of cold-pressed lime oils,
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Hedin, McKibben, et al., 2000
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Oyedeji, Olawore, et al., 1999
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Volatile leaf oil constituents of three Eucalyptus species from Nigeria,
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. [all data]
Lamarque, Maestri, et al., 1998
Lamarque, A.L.; Maestri, D.M.; Zygadlo, J.A.; Grosso, N.R.,
Volatile constituents from flowers of Acacia caven (Mol.) Mol. var. caven, Acacia aroma Gill. ex Hook., Erythrina crista-galli L. and Calliandra tweedii Benth.,
Flavour Fragr. J., 1998, 13, 4, 266-268, https://doi.org/10.1002/(SICI)1099-1026(1998070)13:4<266::AID-FFJ739>3.0.CO;2-5
. [all data]
Notes
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- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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