Stanolone


Phase change data

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: Eugene S. Domalski and Elizabeth D. Hearing

Enthalpy of phase transition

ΔHtrs (kcal/mol) Temperature (K) Initial Phase Final Phase Reference Comment
4.7299453.0crystaline, IIIliquidMasse, de Maury, et al., 1989Monotropic.
5.5139454.2crystaline, IIliquidMasse, de Maury, et al., 1989Monotropic.
6.4890455.5crystaline, IliquidMasse, de Maury, et al., 1989Monotropic.

Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1230.2536.Quilliam and Westmore, 1978Gas Chrom Q; Column length: 1. m
PackedOV-1210.2495.Brooks, Thawley, et al., 1971 

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryVF-5MS2653.3Tretyakov, 201430. m/0.25 mm/0.25 μm, He; Tstart: 60. C; Tend: 270. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Masse, de Maury, et al., 1989
Masse, J.; de Maury, G.; Chauvet, A.; Terol, A., Thermoanalytical study of some steroids. V. Adrostanolone, Thermochim. Acta, 1989, 149, 1-14. [all data]

Quilliam and Westmore, 1978
Quilliam, M.A.; Westmore, J.B., Sterically crowded trialkylsilyl derivatives for chromatography and mass spectrometry of biologically-important compounds, Anal. Chem., 1978, 50, 1, 59-68, https://doi.org/10.1021/ac50023a020 . [all data]

Brooks, Thawley, et al., 1971
Brooks, C.J.W.; Thawley, A.R.; Rocher, P.; Middleditch, B.S.; Anthony, G.M.; Stillwell, W.G., Characterization of Steroidal Drug Metabolites by Combined Gas Chromatography-Mass Spectrometry, J. Chromatogr. Sci., 1971, 9, 1, 35-43, https://doi.org/10.1093/chromsci/9.1.35 . [all data]

Tretyakov, 2014
Tretyakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]


Notes

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