Bicyclo[3.1.1]hept-2-ene-2-methanol, 6,6-dimethyl-

Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1Polydimethyl siloxane with 5 % PhDB-5 MSCP-Sil 5 CBMethylsiloxane + 5 % Ph-groups
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.22 0.250.250.25
Phase thickness (μm) 0.25 0.250.260.25
Tstart (C) 60.80.60.45.60.
Tend (C) 230.200.270.280.230.
Heat rate (K/min) 2.5.3.3.7.
Initial hold (min)     2.
Final hold (min) 5.25. 22.20.
I 1178.1194.1207.1182.1191.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Priya, Prathapan, et al., 2012Cui, Yang, et al., 2011Mothana, Hasson, et al., 2011Nadim, Malik, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5 MSSE-54DB-5
Column length (m)  30.30.30.30.
Carrier gas  HeliumHeliumHeliumHelium
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.50.70.60.70.
Tend (C) 220.240.290.260.240.
Heat rate (K/min) 10.3.5.2.5.
Initial hold (min) 5.5. 5. 
Final hold (min) 8. 10.999. 
I 1209.1200.1202.1192.1201.
ReferenceHohaus, Trimborn, et al., 2010Monsef-Esfahani, Miri, et al., 2010Radulovic, Blagojevic, et al., 2010Dayisoylu and Alma, 2009Lawal and Oyedelji, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1DB-5 MS5 % Phenyl methyl siloxaneHP-5MS
Column length (m) 60.60.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.90.50.
Tend (C) 230.230.330.225.240.
Heat rate (K/min) 2.2.2.3.5.
Initial hold (min)   12.  
Final hold (min) 30.30.30.3. 
I 1176.1178.1206.1195.1194.
ReferenceMuseli, Pau, et al., 2009Museli, Pau, et al., 2009Patil, Jayaprakasha, et al., 2009Retta, Gattuso, et al., 2009Wannes, Mhamdi, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra 2HP-5HP-5 MSDB-5MSHP-5MS
Column length (m) 50.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (μm) 0.110.320.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 230.250.230.240.280.
Heat rate (K/min) 2.5.3.3.3.
Initial hold (min) 5.30.10.  
Final hold (min) 30. 10.  
I 1194.1196.1191.1194.1196.
ReferenceByun and Shin, 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Andrade, Oliveira, et al., 2007Bozin B., Mlmica-Dukic N., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Col-Elite 5MSDBP-5AT-5SPB-1
Column length (m) 30.30.25.60.30.
Carrier gas HeHeHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.220.250.2
Tstart (C) 60.30.40.60.70.
Tend (C) 210.246.250.260.220.
Heat rate (K/min) 30.3.3.4.3.
Initial hold (min) 3. 1.  
Final hold (min)   10. 15.
I 1190.1197.1170.1198.1176.
ReferenceGhasemi, Yamini, et al., 2007Gudaityte and Venskutonis R.P., 2007Heravi and Sereshti, 2007Meccia, Rojas, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5 MSDBP-5HP-5 MSHP-5MS
Column length (m) 30.60.25.30.30.
Carrier gas HeHydrogenHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.220.250.25
Tstart (C) 50.60.40.60.40.
Tend (C) 250.260.250.280.250.
Heat rate (K/min) 2.4.3.3.3.
Initial hold (min)   1. 5.
Final hold (min)  20.10. 10.
I 1200.1197.1170.1196.1192.
ReferenceRaal, Orav, et al., 2007Rojas, Velasco, et al., 2007Sereshti and Samadi, 2007Vagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5HP-5SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2N2Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.320.250.250.250.20
Tstart (C) 60.40.50.50.70.
Tend (C) 250.260.280.280.220.
Heat rate (K/min) 5.4.9.9.3.
Initial hold (min) 30. 3.3. 
Final hold (min)   3.3.15.
I 1196.1195.11169.1170.1176.
ReferenceYassa and Akhani, 2007Zizovic, Stamenic, et al., 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Cavaleiro, Pinto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-1CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.30.50.30.30.
Carrier gas  HeHe N2
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 60.50.60.40.50.
Tend (C) 280.250.250.220.200.
Heat rate (K/min) 4.2.2.3.5.
Initial hold (min)      
Final hold (min)   40.3. 
I 1198.1194.1177.1200.1188.
ReferenceEbrahim Sajjadi and Mehregan, 2006Farah, Afifi, et al., 2006Filippi, Lanfranchi, et al., 2006Hymete, Rohloff, et al., 2006Martin, Joseph, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5NB-30HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenN2HeHeHydrogen
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.520.250.250.25
Tstart (C) 50.50.50.60.70.
Tend (C) 280.280.250.220.280.
Heat rate (K/min) 5.5.2.5.4.
Initial hold (min)    10.4.
Final hold (min) 5.5.   
I 1181.1181.1180.1198.1194.
ReferenceMarzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Orav, Raal, et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-1SPB-5HP-5
Column length (m) 25.30.60. 25.
Carrier gas H2 HeHeHe
Substrate      
Column diameter (mm) 0.320.250.25 0.2
Phase thickness (μm) 0.250.25  0.33
Tstart (C) 60.50.40.50.60.
Tend (C) 240.250.250.250.240.
Heat rate (K/min) 3.10.4.5.3.
Initial hold (min)  5. 3. 
Final hold (min)    15.7.
I 1198.1198.1175.1194.1194.
ReferencePotzernheim, Bizzo, et al., 2006Robinson, 2006Sefidkon, Jamzad, et al., 2006Stojanovic, Palic, et al., 2006Duarte, Figueira, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5HP-5MSRSL-200DB-1
Column length (m) 50.30.25.30.30.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.50.40.50.
Tend (C) 250.30.250.280.265.
Heat rate (K/min) 2.4.3.6.2.5
Initial hold (min) 60.3.3.2.1.
Final hold (min)  15.10.10.30.
I 1182.1195.1197.1195.1172.
ReferenceFernandez, Lizzani-Cuvelier, et al., 2005Ferretti, Maggi, et al., 2005Ghasemi Y., Faridi P., et al., 2005Jirovetz, Buchbauer, et al., 2005Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas  HeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.35.60.70.60.
Tend (C) 280.280.220.240.280.
Heat rate (K/min) 4.4.4.5.4.
Initial hold (min) 2.2.5.  
Final hold (min)      
I 1202.1202.1196.1200.1195.
ReferenceKowalski and Wolski, 2005Kowalski, 2005Morteza-Semnani, Akbarzadeh, et al., 2005Oyedeji, Yani, et al., 2005Sajjadi S.E. and Eskandari B., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSPE-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 275.260.280.230.280.
Heat rate (K/min) 4.2.3.5.3.
Initial hold (min)  5.5.2. 
Final hold (min)  20. 4. 
I 1200.1194.1193.1216.1197.
ReferenceSajjadi and Ghannadi, 2005Senatore, Apostolides Arnold, et al., 2005Setzer, Noletto, et al., 2005Singh, Raina, et al., 2005Slavkovska, Couladis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5MSCP Sil 5 CBSPB-5
Column length (m) 60.30.30.30.60.
Carrier gas HeHe N2He
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (μm) 0.250.250.250.251.
Tstart (C) 60.60.40.50.60.
Tend (C) 250.280.220.200.200.
Heat rate (K/min) 5.3.3.5.4.
Initial hold (min)   5.  
Final hold (min) 10. 10. 30.
I 1182.1165.1192.1181.1203.
ReferenceSonboli, Salehi, et al., 2005Tzakou and Constantinidis, 2005Vichi, Riu-Aumatell, et al., 2005Agnaniet, Menut, et al., 2004Gauvin, Ravaomanarivo, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-5RTX-1HP-5MSHP-5MS
Column length (m) 25.60.30.30.30.
Carrier gas NitrogenHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.50.60.
Tend (C) 240.260.300.230.275.
Heat rate (K/min) 3.6.4.5.4.
Initial hold (min)  4.6 2. 
Final hold (min)  1. 10. 
I 1195.1212.1180.1176.1199.
ReferenceJAvidnia, Mojab, et al., 2004Jürgens and Dötterl, 2004Kalemba and Thiem, 2004Li and Jiang, 2004Mehrabani, Asadipour, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30NB-30DB-1NB-30HP-5MS
Column length (m) 50.50.50.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.220.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.70.50.60.
Tend (C) 250.250.220.250.280.
Heat rate (K/min) 2.2.4.2.4.
Initial hold (min)      
Final hold (min)      
I 1185.1185.1179.1187.1191.
ReferenceOrav, Stulova, et al., 2004Orav, Stulova, et al., 2004Palá-Paúl, García-Jiménez, et al., 2004Raal, Arak, et al., 2004Sadeghpour, Asghari, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5BPX-5HP-5MSDB-5
Column length (m) 30.25.25.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.20.220.250.25
Phase thickness (μm) 0.250.51.0.250.25
Tstart (C) 60.30.60.60.60.
Tend (C) 280.280.250.275.240.
Heat rate (K/min) 4.3.3.4.4.
Initial hold (min)   5.  
Final hold (min)   10.  
I 1195.1203.1224.1194.1179.
ReferenceSajjadi and Shahpiri, 2004Shafi, Nambiar, et al., 2004Vilaseca, Guy, et al., 2004Afsharypuor and Jahromy, 2003Cabanillas, Lopez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-1HP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 280.220.200.275.275.
Heat rate (K/min) 3.5.5.4.4.
Initial hold (min)  20.   
Final hold (min)  20.   
I 1194.1197.1181.1194.1195.
ReferenceCouladis, Özcan, et al., 2003Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Ngouana, et al., 2003Ghannadi, Aghazari, et al., 2003Ghannadi and Zolfaghari, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5DB-5OV-101
Column length (m) 30.30.30.30.25.
Carrier gas H2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.60.60.50.
Tend (C) 280.280.280.240.200.
Heat rate (K/min) 4.3.3.3.5.
Initial hold (min) 10.    
Final hold (min) 40.    
I 1194.1178.1179.1194.1183.
ReferencePino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Pitarokili, Tzakou, et al., 2003da Silva, Luz, et al., 2003Boyom, Keumedjio, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5PTE-5DB-5
Column length (m) 60.30.30.60.30.
Carrier gas HeN2HeH2He
Substrate      
Column diameter (mm) 0.320.250.250.320.25
Phase thickness (μm) 0.250.250.250.300.25
Tstart (C) 50.50.60.60.60.
Tend (C) 200.250.275.285.240.
Heat rate (K/min) 3.4.4.4.33.
Initial hold (min) 6.    
Final hold (min)      
I 1216.1194.1193.1194.1194.
ReferenceCimanga, Apers, et al., 2002Farah, Fechtal, et al., 2002Ghannadi, Sajjadi, et al., 2002Gudzic, Djokovic, et al., 2002Kobaisy, Tellez, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-1DB-1
Column length (m) 30.25.25.60.50.
Carrier gas HeN2HeHeN2
Substrate      
Column diameter (mm) 0.250.230.20.250.25
Phase thickness (μm) 0.250.15  0.25
Tstart (C) 35.50.60.40.60.
Tend (C) 280.250.220.250.240.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min) 2.    
Final hold (min) 15.    
I 1201.1189.1198.1171.1171.
ReferenceKrauze-Baranowska, Mardarowicz, et al., 2002Mahmout, Bessière, et al., 2002Schwob, Bessière, et al., 2002Sefidkon, Dabiri, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSDB-5RTX-1PTE-5
Column length (m) 30.30.30.30.60.
Carrier gas H2HeHeN2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.3
Tstart (C) 40.60.60.60.60.
Tend (C) 280.270.240.300.285.
Heat rate (K/min) 4.3.3.4.4.3
Initial hold (min)      
Final hold (min)      
I 1194.1196.1195.1184.1194.
ReferenceVelickovic, Randjelovic, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Kalemba, Marschall, et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1DB-5CP Sil 5 CBDB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeN2HeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.390.25
Tstart (C) 60.60.40.60.60.
Tend (C) 240.300.250.220.240.
Heat rate (K/min) 3.4.2.5.3.
Initial hold (min)   5.  
Final hold (min)   60.  
I 1195.1185.1150.1184.1194.
ReferenceTellez, Dayan, et al., 2000Kalemba, 1999Porta, Porcedda, et al., 1999Rustaiyan and Nadji, 1999Tellez, Canel, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30HP-101CP Sil 5 CBOV-1SPB-Sulfur
Column length (m) 25.25.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.20.250.320.32
Phase thickness (μm)  0.20.250.254.
Tstart (C) 60.70.60.40.45.
Tend (C) 180.200.300.270.240.
Heat rate (K/min) 3.3.6.2.5.
Initial hold (min) 10.2. 4.13.
Final hold (min)  10.  5.
I 1183.1193.1171.1191.1206.
ReferenceJantan, Ahmad, et al., 1998Milso, Mastelic, et al., 1998Bos, Woerdenbag, et al., 1997Kökdil, Kurucu, et al., 1997Mariaca, Berger, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-SulfurDB-5HP-1SE-54RSL-150
Column length (m) 30.30.23.30.30.
Carrier gas HeHeliumHeHydrogen 
Substrate      
Column diameter (mm) 0.320.250.320.250.32
Phase thickness (μm) 4.0.250.170.250.20
Tstart (C) 45.60.60.60.30.
Tend (C) 240.240.250.250.200.
Heat rate (K/min) 5.3.5.2.3.
Initial hold (min) 13. 3.5. 
Final hold (min) 5. 30.2. 
I 1207.1194.1176.1191.1180.
ReferenceMariaca, Berger, et al., 1997Tellez, Estell, et al., 1997Ayedoun, Adeoti, et al., 1996Kollmannsberger, Nitz, et al., 1992Ronse and De Pooter, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-1SE-30DB-1
Column length (m) 60.40.60.
Carrier gas  He 
Substrate    
Column diameter (mm) 0.320.500.32
Phase thickness (μm)  0.75 
Tstart (C) 50.30.50.
Tend (C) 250.220.250.
Heat rate (K/min) 4.3.4.
Initial hold (min)   0.1
Final hold (min) 5. 5.
I 1177.1189.1176.
ReferenceBinder, Flath, et al., 1989de Pooter, de Buyck, et al., 1989Flath, Mon, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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