Borneol

Formula: C₁₀H₁₈O
Molecular weight: 154.2493
IUPAC Standard InChI: InChI=1S/C10H18O/c1-9(2)7-4-5-10(9,3)8(11)6-7/h7-8,11H,4-6H2,1-3H3/t7?,8-,10?/m1/s1
IUPAC Standard InChIKey: DTGKSKDOIYIVQL-CCNFQMFXSA-N
CAS Registry Number: 507-70-0
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Species with the same structure:
- Isoborneol
- Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, (1S-endo)-
Stereoisomers:
Other names: Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-; endo-Borneol; endo-2-Hydroxy-1,7,7-trimethylnorbornane; Camphol; Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, endo-; 2-Bornanol, endo-; Baros camphor; Bhimsaim camphor; Borneo camphor; trans-Borneol; Bornyl alcohol; Camphane, 2-hydroxy-; 2-Camphanol; Dryobalanops camphor; 2-Hydroxycamphane; Malayan camphor; Sumatra camphor; 1,7,7-Trimethyl-bicyclo(2.2.1)heptan-2-ol, endo-; UN 1312; Bhimsiam camphor; dl-Borneol; Endo-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ol; Endo-2-bornanol; Endo-2-camphanol; Endo-2-hydroxycamphane; Malay camphor; 1,7,7-Trimethylbicyclo[2.2.1]heptan-2-ol; 2-endo-Bornyl alcohol; Camphor
Information on this page:
Other data available:
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-1	RTX-1	RTX-1	Mega-5
Column length (m)	60.	30.	60.	60.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	50.
T_end (C)	250.	240.	230.	230.	220.
Heat rate (K/min)	3.	3.	2.	2.	3.
Initial hold (min)	1.				1.
Final hold (min)	20.		5.	5.	5.
I	1161.	1155.	1150.	1150.	1165.
Reference	Sardashti, Valizadeh, et al., 2013	Alizadeh and Shaabani, 2012	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Dell'Agli, Sanna, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-5	HP-5	HP-5 MS
Column length (m)	30.	25.	25.	25.	30.
Carrier gas	Helium	Hydrogen	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.52	0.52	0.52	0.25
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	250.	280.	280.	280.	300.
Heat rate (K/min)	3.	4.	4.	4.	15.
Initial hold (min)	1.				2.
Final hold (min)	3.	10.	10.	10.	10.
I	1168.	1181.	1182.	1182.	1171.
Reference	Jian-Yu, Zhu, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Xu, Han, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	HP-5 MS	CP-Sil 5 CB	DB-5	DB-5 MS
Column length (m)	60.	30.	25.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.25	0.25
T_start (C)	60.	50.	50.	40.	60.
T_end (C)	230.	250.	220.	250.	270.
Heat rate (K/min)	2.	7.		3.	3.
Initial hold (min)		1.		5.
Final hold (min)	45.	5.		20.
I	1149.	1164.	1162.	1173.	1178.
Reference	Yapi, Boti, et al., 2012	Zouari, Ayadi, et al., 2012	Ameen, Usman, et al., 2011	Cao, Li, et al., 2011	Cui, Yang, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5 MS	HP-5 MS	HP-5	VF-5 MS
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	35.	60.	30.
T_end (C)	210.	220.	250.	240.	260.
Heat rate (K/min)	5.	4.	5.	3.	2.
Initial hold (min)		20.	3.	2.
Final hold (min)		20.	10.		28.
I	1167.	1155.	1205.	1169.	1174.
Reference	Fathi, Sahari, et al., 2011	Feizbakhsh and Naeemy, 2011	Kadri, Zarai, et al., 2011	Kahriman, Tosun, et al., 2011	Leffingwell and Alford, 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5 MS	CP-Sil 5 CB	Methylsiloxane + 5 % Ph-groups	HP-5 MS	ZB-5 MS
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.26	0.25	0.25	0.25
T_start (C)	30.	45.	60.	30.	60.
T_end (C)	260.	280.	230.	250.	290.
Heat rate (K/min)	2.	3.	7.	5.	5.
Initial hold (min)			2.	3.
Final hold (min)	28.	22.	20.	10.
I	1176.	1154.	1165.	1199.	1177.
Reference	Leffingwell and Alford, 2011	Mothana, Hasson, et al., 2011	Nadim, Malik, et al., 2011	Zarai, Kadri, et al., 2011	Boix, Victorio, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5 MS	BP-1	HP-5
Column length (m)	30.	30.	60.		30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25		0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	50.	40.	60.	50.
T_end (C)	280.	250.	250.	220.	240.
Heat rate (K/min)	3.	2.	5.	5.	3.
Initial hold (min)			15.	10.	5.
Final hold (min)			15.	30.
I	1164.	1169.	1186.	1154.	1169.
Reference	Georgiou, Koutsaviti, et al., 2010	Ho, Wang, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Mishra, Chaudhary, et al., 2010	Monsef-Esfahani, Miri, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5 MS	HP-5 MS	HP-5 MS	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.20	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	100.	70.	70.
T_end (C)	220.	220.	220.	290.	290.
Heat rate (K/min)	3.	5.	2.	5.	5.
Initial hold (min)		10.
Final hold (min)	15.			10.	10.
I	1145.	1167.	1172.	1172.	1177.
Reference	Neves, Rosa, et al., 2010	Ogunwande, Flamini, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Blagojevic, et al., 2010	Radulovic, Dordevic, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-1-MS	CP Sil 5 CB	DB-5	HP-5MS
Column length (m)	30.	60.	25.	30.	30.
Carrier gas	Helium	Helium		Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.25	0.25
T_start (C)	60.	30.	50.	40.	50.
T_end (C)	220.	200.	230.	250.	250.
Heat rate (K/min)	6.	2.	3.	10.	7.
Initial hold (min)	3.	4.		1.	1.
Final hold (min)		35.		3.	5.
I	1155.	1144.	1162.	1169.	1176.
Reference	Safaei-Ghomi and Batooli, 2010	Takeoka, Hobbs, et al., 2010	Usman, Zubair, et al., 2010	Yang, Zhang, et al., 2010	Zouari, Zouari, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	HP-5 MS	DB-5	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.33
T_start (C)	60.	60.	50.	70.	60.
T_end (C)	260.	250.	250.	240.	240.
Heat rate (K/min)	2.	2.	5.	5.	3.
Initial hold (min)	5.	8.	2.
Final hold (min)	999.	15.			7.
I	1162.	1184.	1169.	1167.	1169.
Reference	Dayisoylu and Alma, 2009	Farhat, Ginies, et al., 2009	Ho, Wang, et al., 2009	Lawal and Oyedelji, 2009	Maridass, 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	OV-1	BP-1	DB-5
Column length (m)	60.	60.	30.	50.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	60.	45.
T_end (C)	230.	230.	300.	220.	250.
Heat rate (K/min)	2.	2.	4.	2.	3.
Initial hold (min)			2.		3.
Final hold (min)	30.	30.	10.	20.	5.
I	1150.	1153.	1145.	1142.	1167.
Reference	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009	Nibret and Wink, 2009	Ottavioli, Bighelli, et al., 2009	Porto, Decorti, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	5 % Phenyl methyl siloxane	DB-5	DB-5	HP-5MS
Column length (m)	30.	60.	30.	50.	30.
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.32	0.25
T_start (C)	70.	90.	40.	60.	50.
T_end (C)	290.	225.	230.	220.	240.
Heat rate (K/min)	5.	3.	2.	5.	5.
Initial hold (min)				3.
Final hold (min)	10.	3.		5.
I	1172.	1167.	1170.	1165.	1165.
Reference	Radulovic, Blagojevic, et al., 2009	Retta, Gattuso, et al., 2009	Scrivanti, Anton, et al., 2009	Shafaghat and Sadeghi, 2009	Wannes, Mhamdi, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5 MS	HP-5 MS	Ultra 2	ZB-1
Column length (m)	30.	30.	30.	50.	30.
Carrier gas	Helium	Helium		Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25		0.11	0.25
T_start (C)	60.	50.	60.	60.	45.
T_end (C)	300.	280.	280.	230.	230.
Heat rate (K/min)	15.	4.	3.	2.	3.
Initial hold (min)	2.			5.
Final hold (min)	10.			30.
I	1171.	1183.	1163.	1163.	1143.
Reference	Xu, Han, et al., 2009	Zhao, Zeng, et al., 2009	Baziou, Couladis, et al., 2008	Byun and Shin, 2008	Mierendorff, Stahl-Biskup, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	Elite-1	HP-5 MS	RTX-5	HP-5
Column length (m)	60.	30.	30.	20.	25.
Carrier gas	Nitrogen	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.18	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	250.	246.	250.	280.	240.
Heat rate (K/min)	5.	3.	2.	4.	4.
Initial hold (min)			8.	1.	2.
Final hold (min)	10.		15.
I	1179.	1168.	1176.	1168.	1167.
Reference	Mosayebi, Amin, et al., 2008	Raj, Baby, et al., 2008	Sahraoui, Vian, et al., 2008	Skalicka-Wozniak, Los, et al., 2008	Verdian-rizi, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	DB-5	CP Sil 5 CB	SE-52
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	Helium	Helium	Nitrogen	N2
Substrate
Column diameter (mm)	0.25	0.25	0.20	0.32	0.25
Phase thickness (μm)	0.32	0.25	0.32	0.25	0.25
T_start (C)	60.	50.	60.	60.	50.
T_end (C)	250.	230.	220.	300.	220.
Heat rate (K/min)	5.	3.	5.	4.	3.
Initial hold (min)	30.	10.	3.		1.
Final hold (min)		10.	5.		5.
I	1166.	1165.	1166.	1149.	1147.
Reference	Yassa and Akhani, 2008	Adams, Beauchamp, et al., 2007	Amiri, 2007	Baran, von Reuss, et al., 2007	Bicchi, Cordero, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	Helium	He	He
Substrate
Column diameter (mm)	0.26	0.25	0.26	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	280.	290.	250.	250.
Heat rate (K/min)	3.	3.	3.	2.	2.
Initial hold (min)				8.	8.
Final hold (min)				15.	15.
I	1162.	1167.	1162.	1176.	1161.
Reference	Bos, Woerdenbag, et al., 2007	Bozin B., Mlmica-Dukic N., et al., 2007	Elfami, Bos, et al., 2007	Ferhat, Meklati, et al., 2007	Ferhat, Tigrine-Kordjani, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	Col-Elite 5MS	DBP-5	RTX-5 MS	DB-5MS
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	He	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	60.	30.	40.	45.	60.
T_end (C)	210.	246.	250.	210.	280.
Heat rate (K/min)	30.	3.	3.	3.	3.
Initial hold (min)	3.		1.
Final hold (min)			10.		30.
I	1165.	1169.	1142.	1169.	1136.
Reference	Ghasemi, Yamini, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Heravi and Sereshti, 2007	Hudaib and Aburjai, 2007	Marongiu B., Piras A., et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	SPB-1	SPB-5	BPX-5
Column length (m)	25.	25.	30.	30.	50.
Carrier gas	H2	Helium	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.2	0.25	0.22
Phase thickness (μm)	0.33	0.25	0.2	0.25
T_start (C)	60.	100.	70.	50.	50.
T_end (C)	240.	280.	220.	250.	300.
Heat rate (K/min)	3.	4.	3.	2.	4.
Initial hold (min)		3.			1.
Final hold (min)		5.	15.		10.
I	1168.	1176.	1146.	1160.	1210.
Reference	Oliveira, Leitão, et al., 2007	Phutdhawong, Kawaree, et al., 2007	Pinto, Salgueiro, et al., 2007	Raal, Orav, et al., 2007	Rali, Wossa, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DBP-5	HP-5 MS	HP-5 MS
Column length (m)	60.	30.	25.	30.	30.
Carrier gas	He	He	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	60.	50.	40.	60.	60.
T_end (C)	250.	240.	250.	280.	280.
Heat rate (K/min)	5.	4.	3.	3.	3.
Initial hold (min)			1.
Final hold (min)			10.
I	1155.	1164.	1142.	1168.	1169.
Reference	Salehi, Fakhari, et al., 2007	Sefidkon, Abbasi, et al., 2007	Sereshti and Samadi, 2007	Tsokou, Georgopoulos, et al., 2007	Vagionas, Graikou, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5	DB-5	ZB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	50.	50.	40.
T_end (C)	260.	280.	280.	265.	300.
Heat rate (K/min)	4.	9.	9.	2.5	2.
Initial hold (min)		3.	3.	1.
Final hold (min)		3.	3.	20.
I	1163.3	1149.	1151.	1172.	1165.
Reference	Zizovic, Stamenic, et al., 2007	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Bazargani, Almasirad, et al., 2006	Biondi, Sari, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	SPB-1	HP-5	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	He		Helium
Substrate
Column diameter (mm)	0.25	0.20	0.32	0.25	0.26
Phase thickness (μm)	0.25	0.20	0.25	0.25	0.25
T_start (C)	60.	70.	60.	60.	60.
T_end (C)	280.	220.	246.	280.	290.
Heat rate (K/min)	3.	3.	3.	4.	3.
Initial hold (min)
Final hold (min)		15.
I	1167.	1144.	1168.	1168.	1162.
Reference	Bozin, Mimicá-Dukic, et al., 2006	Cavaleiro, Pinto, et al., 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-1	DB-1	DB-5	DB-1
Column length (m)	30.	50.	60.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	300.	250.	240.	240.	240.
Heat rate (K/min)	5.	2.	5.	5.	5.
Initial hold (min)	5.		2.	2.	2.
Final hold (min)	5.	40.
I	1177.	1149.	1164.	1165.	1164.
Reference	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari, Hadjiakhoondi, et al., 2006	Gohari A.R., Hadjiakhoondi A., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	Methyl Silicone	RTX-1
Column length (m)	30.	60.	30.	25.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	90.	60.
T_end (C)	240.	250.	250.	220.	300.
Heat rate (K/min)	5.	5.	3.	7.	4.
Initial hold (min)	2.			2.
Final hold (min)		10.	10.
I	1165.	1155.	1167.	1162.	1150.
Reference	Gohari A.R., Hadjiakhoondi A., et al., 2006	Hadian, Sonboli, et al., 2006	Havlik, Kokoska, et al., 2006	Kitchlu, Bakshi, et al., 2006	Kula, Izydorczyk, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	HP-101	HP-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	Nitrogen	N2	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.32	0.25
Phase thickness (μm)	0.25	0.52	0.2	0.25	0.25
T_start (C)	50.	50.	70.	40.	60.
T_end (C)	280.	280.	200.	240.	220.
Heat rate (K/min)	5.	5.	3.	4.	4.
Initial hold (min)			2.
Final hold (min)	5.	5.	15.	5.
I	1149.	1149.	1166.	1168.	1172.
Reference	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Mastelic, Jerkovic, et al., 2006	Miyazawa and Kawata, 2006	Morteza-Semnani, Akbarzadeh, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	CP-Sil 5 CB
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.15
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	220.	260.	220.	250.	230.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)	5.	4.	5.
Final hold (min)
I	1171.	1172.	1171.	1167.	1153.
Reference	Morteza-Semnani K., Akbarzadeh M., et al., 2006	Morteza-Semnani, Saeedi, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Najafpour Navaei, Mirza, et al., 2006	Olawore, Usman, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	HP-5MS	DB-5	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	N2	He	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.15	0.25	0.25	0.25
T_start (C)	50.	50.	40.	70.	70.
T_end (C)	250.	200.	260.	280.	280.
Heat rate (K/min)	2.	4.	4.	4.	4.
Initial hold (min)		3.		4.	4.
Final hold (min)
I	1157.	1173.	1168.	1165.	1163.
Reference	Orav, Raal, et al., 2006	Ouamba, Ouabonzi, et al., 2006	Petrovic, Ristic, et al., 2006	Pino, Marbot, et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	ZB-5	DB-5
Column length (m)	30.	30.	30.	30.	15.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	280.	200.	260.	300.	305.
Heat rate (K/min)	3.	2.	5.	2.	15.
Initial hold (min)					2.
Final hold (min)		60.
I	1134.	1168.	1172.	1165.	1175.
Reference	Pitarokili, Tzakou, et al., 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006	Sari M., Biondi D.M., et al., 2006	Sebastián, Urzúa, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5MS	DB-1	SPB-5
Column length (m)	30.	60.	30.	60.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	240.	250.	280.	250.	250.
Heat rate (K/min)	4.	4.	3.	5.	5.
Initial hold (min)			5.		3.
Final hold (min)				10.	15.
I	1164.	1146.	1165.	1154.	1165.
Reference	Sefidkon and Jamzad, 2006	Sefidkon, Jamzad, et al., 2006	Setzer, Noletto, et al., 2006	Sonboli, Mirjalili, et al., 2006	Stojanovic, Palic, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	BPX-5	SPB-1	SE-30
Column length (m)	50.	25.	50.	30.	30.
Carrier gas	N2	H2		He	He
Substrate
Column diameter (mm)	0.25	0.32	0.22	0.25
Phase thickness (μm)	0.25	0.52	1.	0.25
T_start (C)	90.	50.	70.	50.	90.
T_end (C)	240.	280.	280.	250.	220.
Heat rate (K/min)	4.	2.5	4.	4.	7.
Initial hold (min)		5.		1.	2.
Final hold (min)			4.	10.
I	1150.	1170.	1213.	1142.	1148.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2006	Wang, Kong, et al., 2006	Wohlmuth, Smith, et al., 2006	Wong, Sivasothy, et al., 2006	Ahuja, Bakshi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-1	DB-5MS	Methyl Silicone	DB-1
Column length (m)	30.	50.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.3	0.25
Phase thickness (μm)	0.25	0.5	0.25		0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	280.	250.	240.	240.	250.
Heat rate (K/min)	3.	2.	3.	3.	5.
Initial hold (min)					5.
Final hold (min)		60.			15.
I	1151.	1150.	1166.	1168.	1170.
Reference	Basta, Tzakou, et al., 2005	Bendimerad and Bendiab, 2005	Busman, Zoghbi, et al., 2005	Chalchat and Özcan, 2005	Facundo, Pinto, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	HP-5	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	60.	50.	30.	30.	30.
Carrier gas	He		He	N2	N2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	250.	250.	300.	250.	250.
Heat rate (K/min)	5.	2.	5.	5.	5.
Initial hold (min)		60.	5.
Final hold (min)			5.	10.	10.
I	1158.	1148.	1177.	1159.	1160.
Reference	Fakhari, Salehi, et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005	Figuérédo, Cabassu, et al., 2005	Jassbi, Mehrdad, et al., 2005	Jassbi, Mehrdad, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	SPB-5	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.53	0.25	0.25
Phase thickness (μm)	0.52			0.25	0.25
T_start (C)	40.	60.	100.	60.	60.
T_end (C)	240.	240.	250.	220.	220.
Heat rate (K/min)	4.	3.	5.	4.	4.
Initial hold (min)				5.	5.
Final hold (min)
I	1163.	1168.	1190.	1169.	1169.
Reference	Jovanovic, Kitic, et al., 2005	Khayyat and Karimi, 2005	Kilic, Kollmannsberger, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	RTX-5 MS	HP-5MS	HP-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas		He	He		He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.2	0.25
Phase thickness (μm)	0.15	0.25	0.25
T_start (C)	50.	40.	50.	60.	60.
T_end (C)	230.	250.	280.	280.	240.
Heat rate (K/min)	3.	5.	8.	3.	5.
Initial hold (min)		0.5	2.
Final hold (min)		2.	2.
I	1151.	1162.	1175.	1169.	1163.
Reference	Ogunwande, Olawore, et al., 2005	Özel, Gögüs, et al., 2005	Pellati, Benvenuti, et al., 2005	Petrakis, Roussis, et al., 2005	Saeidnia, Gohari, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5	HP-5MS	RTX-1
Column length (m)	30.	30.	30.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	240.	275.	230.	280.	250.
Heat rate (K/min)	4.	15.	3.	3.	5.
Initial hold (min)
Final hold (min)			20.		10.
I	1165.	1177.	1169.	1165.	1157.
Reference	Sefidkon and Jamzad, 2005	Shams-Ardakani, Ghannadi, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005	Sonboli A., Fakhari A.R., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5 MS	DB-5	DB-1	SPB-1
Column length (m)	30.	30.	30.	50.	50.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.2
Phase thickness (μm)	0.25	0.50	0.25	0.25	0.33
T_start (C)	50.	60.	60.	60.	50.
T_end (C)	240.	260.	280.	240.	220.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)	3.				3.
Final hold (min)		20.			30.
I	1193.	1168.	1144.	1142.	1156.
Reference	Tepe B., Sokmen M., et al., 2005	Topçu, Barla, et al., 2005	Tzakou and Constantinidis, 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Wong, Lee, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	BP-1	SPB-5	DB-1
Column length (m)	30.	30.	50.	60.	25.
Carrier gas	N2	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	1.	0.25
T_start (C)	50.	90.	60.	60.	60.
T_end (C)	200.	220.	220.	200.	180.
Heat rate (K/min)	5.	7.	2.	4.	3.
Initial hold (min)		2.			10.
Final hold (min)		5.	20.	30.	10.
I	1159.	1152.	1149.	1174.	1167.
Reference	Agnaniet, Menut, et al., 2004	Agnihotri, Thappa, et al., 2004	Blanc, Muselli, et al., 2004	Gauvin, Ravaomanarivo, et al., 2004	bin Jantan, Ayop, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-5	DB-5	RTX-1	SE-54
Column length (m)	25.	60.	60.	30.	30.
Carrier gas	Nitrogen	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	40.	60.	60.
T_end (C)	240.	260.	280.	300.	260.
Heat rate (K/min)	3.	6.	4.	4.	2.
Initial hold (min)		4.6	4.		5.
Final hold (min)		1.
I	1165.	1187.	1164.	1155.	1162.
Reference	JAvidnia, Mojab, et al., 2004	Jürgens and Dötterl, 2004	Kalvandi, Sefidkon, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-1	DB-1	DB-1	NB-30
Column length (m)	30.	60.	60.	60.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.053	0.32	0.32	0.32	0.2
Phase thickness (μm)	1.5	0.25	0.25	0.25	0.25
T_start (C)	100.	35.	35.	35.	50.
T_end (C)	250.	230.	230.	230.	250.
Heat rate (K/min)	5.	2.	2.	2.	2.
Initial hold (min)		4.	4.	4.
Final hold (min)		25.	25.	25.
I	1195.	1142.	1142.	1147.	1156.
Reference	Kilic, Hafizoglu, et al., 2004	Park, Lee, et al., 2004	Park, Lee, et al., 2004	Park, Lee, et al., 2004	Raal, Arak, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-5	HP-5MS	DB-1	DB-1
Column length (m)	50.	30.	30.	30.	60.
Carrier gas	He	He	He	He	Nitrogen
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	35.	60.	50.	70.
T_end (C)	250.	220.	280.	265.	230.
Heat rate (K/min)	2.	2.5	4.	2.5	2.
Initial hold (min)				1.	2.
Final hold (min)		6.		20.
I	1156.	1169.	1166.	1140.	1135.
Reference	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004	Sajjadi and Shahpiri, 2004	Sarkhail, Amin, et al., 2004	Sawamura, Sou, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-1	DB-5	HP-5
Column length (m)	30.	60.	30.	30.	25.
Carrier gas		He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.5
T_start (C)	50.	40.	40.	40.	30.
T_end (C)	250.	280.	260.	250.	280.
Heat rate (K/min)	3.	4.	2.	2.	3.
Initial hold (min)	5.	5.	5.	5.
Final hold (min)			20.	20.
I	1165.	1147.	1136.	1164.	1176.
Reference	Sefidkon, Jamzad, et al., 2004	Sefidkon and Shaabani, 2004	Senatore, Napolitano, et al., 2004	Senatore, Rigano, et al., 2004	Shafi, Nambiar, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5	DB-1	HP-5MS
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.249	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	70.	60.
T_end (C)	300.	275.	240.	230.	280.
Heat rate (K/min)	3.	4.	4.	2.	3.
Initial hold (min)				2.
Final hold (min)				20.
I	1162.	1165.	1152.	1131.	1160.
Reference	Woerdenbag, Windono, et al., 2004	Afsharypuor and Jahromy, 2003	Cabanillas, Lopez, et al., 2003	Choi, 2003	Couladis, Özcan, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5Sil	DB-1	HP-1	HP-5MS	HP-5MS
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	50.	70.	60.	60.
T_end (C)	200.	250.	200.	275.	275.
Heat rate (K/min)	4.	4.	10.	4.	4.
Initial hold (min)
Final hold (min)	10.
I	1177.	1161.	1156.	1165.	1162.
Reference	Dudai, Larkov, et al., 2003	Ebrahimzadeh, Yamini, et al., 2003	Fekam Boyom, Amvam Zollo, et al., 2003	Ghannadi, Aghazari, et al., 2003	Hajhashemi, Ghannadi, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RSL-200	CP Sil 5 CB	DB-1	ZB-1
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	H2	H2	He	N2	N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	40.	35.	80.	45.
T_end (C)	280.	280.	280.	250.	230.
Heat rate (K/min)	6.	6.	5.	4.	3.
Initial hold (min)	5.	5.	2.5
Final hold (min)	5.	5.
I	1163.	1154.	1144.	1149.	1143.
Reference	Jirovetz, Buchbauer, et al., 2003	Jirovetz, Buchbauer, et al., 2003, 2	Kanjilal, Kotoky, et al., 2003	Mahalwal and Ali, 2003	Mierendorff, Stahl-Biskup, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	DB-1	DB-5
Column length (m)	50.	30.	30.	60.	30.
Carrier gas	N2	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	60.	60.	50.	75.
T_end (C)	240.	280.	280.	250.	220.
Heat rate (K/min)	4.	4.	3.	4.	3.
Initial hold (min)		10.			4.
Final hold (min)		40.
I	1157.	1165.	1152.	1144.	1170.
Reference	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Priestap, van Baren, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	NB-30	DB-1	DB-1	DB-5	Methyl Silicone
Column length (m)	50.	60.	60.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25
T_start (C)	50.	40.	40.	40.	35.
T_end (C)	250.	220.	220.	230.	180.
Heat rate (K/min)	2.	4.	4.	2.	4.
Initial hold (min)
Final hold (min)
I	1156.	1150.	1154.	1152.	1133.
Reference	Raal, Arak, et al., 2003	Rasooli and Mirmostafa, 2003	Rasooli and Mirmostafa, 2003	Rotman, Ahumada, et al., 2003	Santos and Cordeiro, 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5	HP-5	HP-5
Column length (m)	30.	50.	25.	25.	25.
Carrier gas	He	N2	H2	H2	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.53	0.53	0.53
T_start (C)	60.	90.	40.	40.	40.
T_end (C)	240.	240.	280.	280.	280.
Heat rate (K/min)	3.	4.	4.	4.	4.
Initial hold (min)
Final hold (min)
I	1168.	1130.	1163.	1169.	1162.
Reference	da Silva, Luz, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-5	CP Sil 5 CB	OV-101
Column length (m)	25.	25.	30.	25.	25.
Carrier gas	Helium	Helium	He	N2
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.32
Phase thickness (μm)	0.53	0.53	0.25	0.4
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	280.	280.	240.	260.	200.
Heat rate (K/min)	4.	4.	3.	5.	5.
Initial hold (min)
Final hold (min)				40.
I	1162.	1169.	1163.	1151.	1156.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Zoghbi, Andrade, et al., 2003	Azaz. D., Demirci, et al., 2002	Boyom, Keumedjio, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5MS	BP-1	DB-5
Column length (m)	30.	60.	30.	25.	30.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.50	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	50.	50.	60.	50.
T_end (C)	280.	200.	280.	220.	250.
Heat rate (K/min)	3.	3.	15.	5.	4.
Initial hold (min)		6.	2.
Final hold (min)	30.		10.	10.
I	1159.	1160.	1159.	1153.	1165.
Reference	Caredda, Marongiu, et al., 2002	Cimanga, Apers, et al., 2002	Damon, Hernández, et al., 2002	Das, Ram, et al., 2002	Farah, Fechtal, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	SE-30	RSL-200	RSL-200	CP Sil 8 CB
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	H2	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	40.	50.	50.
T_end (C)	275.	240.	280.	280.	220.
Heat rate (K/min)	4.	4.	6.	6.	3.
Initial hold (min)			5.	5.	2.
Final hold (min)			5.	5.
I	1164.	1161.	1162.	1152.	1174.
Reference	Ghannadi, Sajjadi, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Jirovetz, Buchbauer, et al., 2002	Jirovetz, Ngassoum, et al., 2002	Juteau, Masotti, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-5	DB-5	OV-101	DB-1
Column length (m)	60.	30.	30.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	50.	60.	35.	50.	60.
T_end (C)	240.	240.	280.	200.	250.
Heat rate (K/min)	5.	3.	3.	5.	4.
Initial hold (min)	3.		2.		10.
Final hold (min)	10.		15.
I	1182.	1167.	1170.	1155.	1172.
Reference	Kim and Lee, 2002	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002	Menut, Bessière, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	OV-101	DB-1	HP-1	DB-5
Column length (m)	30.	50.	50.	50.	30.
Carrier gas		He	N2	N2	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.5	0.25	0.25	0.25
T_start (C)	60.	50.	80.	90.	60.
T_end (C)	240.	250.	225.	220.	300.
Heat rate (K/min)	3.	2.	4.	3.	2.
Initial hold (min)
Final hold (min)
I	1173.	1150.	1147.	1163.	1166.
Reference	Novak, Langbehn, et al., 2002	Orav, Kailas, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002	Priestap, van Baren, et al., 2002	Ruberto, Biondi, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	OV-101	DB-5MS	DB-5
Column length (m)	60.	50.	25.	30.	30.
Carrier gas	He	N2	Nitrogen	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	280.	240.	240.	270.	240.
Heat rate (K/min)	4.	3.	4.	3.	3.
Initial hold (min)	5.		0.
Final hold (min)			0.
I	1146.	1142.	1154.	1164.	1164.
Reference	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Zenkevich and Rodin, 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	DB-1	HP-5	HP-5
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	40.	40.	40.	60.	60.
T_end (C)	220.	280.	280.	220.	220.
Heat rate (K/min)	3.	4.	4.	5.	5.
Initial hold (min)	5.	5.	5.	10.	10.
Final hold (min)	15.
I	1166.	1142.	1145.	1167.	1167.
Reference	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Flamini, Cioni, et al., 2001	Gallori, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	RTX-1	SPB-1	SPB-5	DB-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	N2	N2	N2	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	70.	50.	50.
T_end (C)	220.	300.	180.	240.	270.
Heat rate (K/min)	5.	4.	2.	3.	4.
Initial hold (min)			2.	3.
Final hold (min)			1.	10.
I	1154.	1156.	1158.	1183.	1145.
Reference	Gupta, Mallavarapu, et al., 2001	Kalemba, Marschall, et al., 2001	Kamath, Asha, et al., 2001	Kim and Lee, 2001	Mirza, Ahmadi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	PTE-5	DB-5	RSL-200
Column length (m)	30.	30.	60.	30.	60.
Carrier gas	N2	H2	H2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.3	0.25	0.25
T_start (C)	80.	60.	60.	60.	40.
T_end (C)	225.	285.	285.	240.	250.
Heat rate (K/min)	4.	3.	4.3	3.	6.
Initial hold (min)
Final hold (min)
I	1147.	1165.	1165.	1166.	1163.
Reference	Palá-Paúl, Pérez-Alonso, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Stojanovic, Palic, et al., 2001	Tellez M., Estell R., et al., 2001	Jirovetz, Puschmann, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	HP-5	DB-5	DB-5	SE-30
Column length (m)	60.	30.	60.	30.	25.
Carrier gas	He	He	Hydrogen or helium (He2 wrote in original paper)	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.30	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	200.	275.	285.	240.	230.
Heat rate (K/min)	4.	4.	4.3	3.	3.
Initial hold (min)	5.
Final hold (min)	25.
I	1157.	1165.	1165.	1167.	1148.
Reference	Meccia, Rojas, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Simic, Andjelkovic, et al., 2000	Tellez, Dayan, et al., 2000	Ali N.A.M. and Jantan, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	SPB-1	SE-30	RTX-1	OV-101
Column length (m)	25.	50.	30.	30.	50.
Carrier gas	Hydrogen		N2	N2	N2
Substrate
Column diameter (mm)	0.32	0.2	0.25	0.25	0.2
Phase thickness (μm)	0.30	0.33	0.25	0.25
T_start (C)	50.	60.	60.	60.	80.
T_end (C)	200.	260.	220.	300.	200.
Heat rate (K/min)	3.	4.	4.	4.	1.
Initial hold (min)	1.		10.
Final hold (min)	10.				20.
I	1136.	1170.	1155.	1158.	1164.
Reference	Bicchi, Binello, et al., 1999	Choo, Wong, et al., 1999	Jassbi, Ahmad, et al., 1999	Kalemba, 1999	Menon, Chacko, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	OV-1	CP Sil 5 CB	DB-1	DB-5
Column length (m)	25.	25.	25.	50.	30.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25		0.25	0.25
T_start (C)	60.	40.	50.	70.	40.
T_end (C)	230.	220.	230.	240.	250.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)	10.	5.			5.
Final hold (min)		5.			60.
I	1148.	1142.	1146.	1147.	1130.
Reference	Mohd and Jantan, 1999	Oberhofer, Nikiforov, et al., 1999	Oyedeji, Olawore, et al., 1999	Palá-Paúl, Pérez-Alonso, et al., 1999	Porta, Porcedda, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	PONA	CP Sil 5 CB	DB-1	DB-5
Column length (m)	30.	50.	25.	60.	30.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.20	0.5	0.39	0.25	0.25
T_start (C)	60.	40.	60.	40.	40.
T_end (C)	200.	250.	220.	280.	220.
Heat rate (K/min)	3.	6.	5.	4.	4.
Initial hold (min)	4.	5.	5.	5.	5.
Final hold (min)			20.
I	1163.	1169.	1155.	1153.	1165.
Reference	Prikhod'ko, Klyuev, et al., 1999	Ramalho, de Freitas, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Sefidkon, Dabiri, et al., 1999	Sefidkon and Khajavi, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5	CP Sil 5 CB	DB-5MS
Column length (m)	60.	60.	30.	25.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.32	0.25		0.25
Phase thickness (μm)	0.25		0.25	0.39	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	220.	230.	240.	220.	240.
Heat rate (K/min)	4.	3.	3.	5.	3.
Initial hold (min)
Final hold (min)		5.
I	1155.	1155.	1166.	1157.	1163.
Reference	Sefidkon and Mirza, 1999	Shafiee, Javidnia, et al., 1999	Tellez, Canel, et al., 1999	Weyerstahl, Marschall, et al., 1999	Zoghbi, Andrade, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	HP-1	CP Sil 5 CB	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	25.	60.	25.	25.	25.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.32	0.32	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	50.	60.
T_end (C)	180.	280.	290.	290.	300.
Heat rate (K/min)	3.	4.	4.	4.	6.
Initial hold (min)	10.	5.
Final hold (min)
I	1154.	1169.	1140.	1140.	1140.
Reference	Jantan, Ahmad, et al., 1998	Stashenko, Cervantes, et al., 1998	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-Sulfur	SPB-Sulfur	DB-1	DB-5	OV-101
Column length (m)	30.	30.		30.	50.
Carrier gas	He	He		Helium	He
Substrate
Column diameter (mm)	0.32	0.32		0.25	0.25
Phase thickness (μm)	4.	4.		0.25
T_start (C)	45.	45.	80.	60.	50.
T_end (C)	240.	240.	220.	240.	250.
Heat rate (K/min)	5.	5.	6.	3.	2.
Initial hold (min)	13.	13.
Final hold (min)	5.	5.
I	1182.	1183.	1134.	1166.	1150.
Reference	Mariaca, Berger, et al., 1997	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Orav, Kailas, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	DB-1	HP-1	HP-5
Column length (m)	25.	25.	60.	25.
Carrier gas	N2	N2	He	Helium
Substrate
Column diameter (mm)	0.50	0.50	0.32	0.32
Phase thickness (μm)			0.50	0.25
T_start (C)	60.	60.	50.	60.	35.
T_end (C)	220.	220.	250.	220.	200.
Heat rate (K/min)	5.	5.	8.	4.	6.
Initial hold (min)			1.	2.	2.
Final hold (min)			6.	20.
I	1156.	1164.	1168.	1144.	1193.
Reference	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Sagrero-Nieves and Bartley, 1996	Thanh, Dung, et al., 1996	Larsen and Frisvad, 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	HP-5	HP-5	Methyl Silicone	Methyl Silicone
Column length (m)	50.			50.	50.
Carrier gas	He			N2	N2
Substrate
Column diameter (mm)	0.2			0.25	0.25
Phase thickness (μm)	0.5			0.17	0.17
T_start (C)	70.	40.	40.	80.	80.
T_end (C)	180.	210.	210.	200.	200.
Heat rate (K/min)	1.	2.	2.	2.	3.
Initial hold (min)
Final hold (min)
I	1152.	1166.	1167.	1164.	1159.
Reference	Orav, Kuningas, et al., 1995	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Gopalakrishnan, Menon, et al., 1993	Gopalakrishnan, Menon, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	Methyl Silicone	OV-101	OV-101	OV-101
Column length (m)	25.	25.	50.	50.	52.
Carrier gas					Helium
Substrate
Column diameter (mm)	0.25	0.50	0.25	0.25	0.26
Phase thickness (μm)
T_start (C)	60.	60.	80.	80.	40.
T_end (C)	280.	220.	200.	200.	200.
Heat rate (K/min)	5.	5.	2.	2.	3.
Initial hold (min)					0.
Final hold (min)					0.
I	1155.	1162.	1153.	1155.	1158.
Reference	Kaul, Singh, et al., 1993	Mallavarapu, Ramesh, et al., 1993	Tamura, Yang, et al., 1993	Tamura, Yang, et al., 1993	Tkachenko and Zenkevich, 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	DB-1	RSL-150	BP-1	OV-101
Column length (m)	30.	30.	30.	25.	50.
Carrier gas	Hydrogen	N2			N2
Substrate
Column diameter (mm)	0.25		0.32	0.33	0.25
Phase thickness (μm)	0.25		0.20
T_start (C)	60.	80.	30.	45.	80.
T_end (C)	250.	220.	200.	180.	200.
Heat rate (K/min)	2.	4.	3.	3.	2.
Initial hold (min)	5.			3.
Final hold (min)	2.
I	1162.	1144.	1152.	1147.	1156.
Reference	Kollmannsberger, Nitz, et al., 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991	Ronse and De Pooter, 1990	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-1	DB-1	SE-30
Column length (m)	50.	10.	50.	50.	50.
Carrier gas	N2	H2			He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.5
Phase thickness (μm)		0.25
T_start (C)	80.	50.	0.	50.	40.
T_end (C)	200.	250.	250.	250.	170.
Heat rate (K/min)	2.	5.	3.	3.	3.
Initial hold (min)					3.
Final hold (min)
I	1156.	1146.	1147.	1146.	1156.
Reference	Yang and Sugisawa, 1990	Perry, Baxter, et al., 1986	Habu, Flath, et al., 1985	Habu, Flath, et al., 1985	Heydanek and McGorrin, 1981
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

Alizadeh and Shaabani, 2012
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Wyllie, Brophy, et al., 1990
Wyllie, S.G.; Brophy, J.J.; Sarafis, V.; Hobbs, M., Volatile Components of the Fruit of Pistacia Lentiscus, J. Food. Sci., 1990, 55, 5, 1325-1326, https://doi.org/10.1111/j.1365-2621.1990.tb03926.x . [all data]

Yang and Sugisawa, 1990
Yang, R.; Sugisawa, H., Citrus Suachi Hort. ex Shirai. Volatile components in Sudachi (Citrus Sudachi Hort. ex Shirai) juice, Nippon Shokuhin Kogyo Gakkaishi, 1990, 37, 12, 946-952, https://doi.org/10.3136/nskkk1962.37.12_946 . [all data]

Perry, Baxter, et al., 1986
Perry, N.B.; Baxter, A.J.; Brennan, N.J.; van Klink, J.W., Dalmatian Sage. PArt 1. Differing oil yields and compositions from flowering and non-flowering accessions, Flavour Fragr. J., 1986, 11, 4, 231-238, https://doi.org/10.1002/(SICI)1099-1026(199607)11:4<231::AID-FFJ572>3.0.CO;2-0 . [all data]

Habu, Flath, et al., 1985
Habu, T.; Flath, R.A.; Mon, T.R.; Morton, J.F., Volatile components of Rooibos tea (Aspalathus linearis), J. Agric. Food Chem., 1985, 33, 2, 249-254, https://doi.org/10.1021/jf00062a024 . [all data]

Heydanek and McGorrin, 1981
Heydanek, M.G.; McGorrin, R.J., Gas chromatography-mass spectroscopy investigations on the flavor chemistry of oat groats, J. Agric. Food Chem., 1981, 29, 5, 950-954, https://doi.org/10.1021/jf00107a016 . [all data]

Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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