1,3,7-Octatriene, 3,7-dimethyl-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1050.Jalali-Heravi, Zekavat, et al., 200660. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 3. K/min, 250. C @ 20. min
CapillaryPTE-51050.Gudzic, Dordevic, et al., 200160. m/0.32 mm/0.39 μm, H2, 4.3 K/min; Tstart: 60. C; Tend: 285. C
CapillaryDB-51052.Rao, Rout, et al., 2000He, 2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 180. C
CapillaryOV-1011038.Padrayuttawat, Tamura, et al., 199650. m/0.25 mm/0.2 μm, N2, 2. K/min, 200. C @ 60. min; Tstart: 80. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51050.Rao, Rout, et al., 2000He; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51052.Liu J.M., Nan P., et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 10. K/min, 250. C @ 10. min
CapillaryDB-11057.Rezazadeh, Hamedani, et al., 200630. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51049.Rezazadeh, Hamedani, et al., 200625. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryPetrocol DH1050.Alonzo, Saiano, et al., 2001100. m/0.25 mm/0.5 μm, He, 60. C @ 8. min, 4. K/min, 180. C @ 2. min
CapillaryDB-51042.Tzakou, Roussis, et al., 1997He, 50. C @ 3. min, 5. K/min; Column length: 60. m; Column diameter: 0.24 mm; Tend: 280. C
CapillaryOV-1011038.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011039.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBPX-51039.Dharmawan, Kasapis, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C => 4C/min => 200C => 30C/min => 300C (3min)
CapillaryVF-5MS1041.Carasek and Pawliszyn, 200630. m/0.25 mm/0.25 μm, He; Program: 40C(2min) => 5C/min => 200C (2min) => 30C/min => 260C
CapillaryVF-5MS1041.Carasek and Pawliszyn, 200630. m/0.25 mm/0.25 μm, He; Program: 40C(2min) => 5C/min => 200C (2min) => 30C/min => 260C
CapillaryVF-5MS1041.Carasek and Pawliszyn, 200630. m/0.25 mm/0.25 μm, He; Program: 40C(2min) => 5C/min => 200C (2min) => 30C/min => 260C
CapillaryDB-5MS1052.Eom S.H., Yang H.S., et al., 200630. m/0.25 mm/0.25 μm, He; Program: 50C(3min) => 200C(2min) => 15C/min => 300C(5min)
CapillaryDB-51052.Özel, Gögüs, et al., 2006Program: not specified

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M1232.Chen, Kuo, et al., 1986He, 50. C @ 5. min, 2. K/min, 200. C @ 40. min; Column length: 50. m; Column diameter: 0.32 mm

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySupelcowax-101237.Bianchi, Careri, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C(8min) => 4C/min => 60C => 6C/min => 160C => 20C/min => 200C(1min)
CapillarySupelcowax-101239.Bianchi, Careri, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C(8min) => 4C/min => 60C => 6C/min => 160C => 20C/min => 200C(1min)

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP Sil 5 CB1040.Usman, Zubair, et al., 201025. m/0.25 mm/0.15 μm, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillarySPB-51047.Gauvin-Bialecki and Marodon, 200960. m/0.35 mm/0.25 μm, Nitrogen, 4. K/min, 230. C @ 40. min; Tstart: 60. C
CapillaryHP-5MS1018.Kim, El-Aty, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 4. min, 5. K/min, 280. C @ 10. min
CapillaryBP-11032.Moody, Gundidza, et al., 2006He, 70. C @ 2. min, 4. K/min, 220. C @ 10. min; Column length: 25. m; Column diameter: 0.3 mm
CapillaryDB-51052.Ozel, Gogus, et al., 200630. m/0.32 mm/0.25 μm, He, 60. C @ 0.5 min, 5. K/min, 280. C @ 2. min
CapillaryHP-5MS1046.Petrakis, Roussis, et al., 20053. K/min; Column length: 30. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 280. C
CapillaryDB-5MS1046.Congiu, Falconieri, et al., 200230. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryOV-1011039.Yang, 2001N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011039.Yang, 2001, 2N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryHP-51043.Lis-Balchin and Roth, 2000He, 9. K/min, 200. C @ 10. min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 80. C
CapillaryHP-11039.Meccia, Rojas, et al., 200060. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min, 200. C @ 25. min
CapillaryMethyl Silicone1039.50Baraldi, Rapparini, et al., 199960. m/0.25 mm/0.25 μm, 40. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51051.Sun and Petracek, 1999H2, 32. C @ 5. min, 7. K/min, 260. C @ 5. min; Column length: 30. m; Column diameter: 0.32 mm
CapillarySPB-51050.Viallon C., Verdier-Metz I., et al., 199960. m/0.32 mm/1. μm, He, 40. C @ 5. min, 3. K/min, 200. C @ 2. min
CapillaryOV-1011038.Yang and Sugisawa, 1990N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011040.Yang and Sugisawa, 1990N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011038.Sugisawa, Yang, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011040.Sugisawa, Yang, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillarySE-301040.Alves and Jennings, 1979Helium, 2. K/min; Tstart: 70. C; Tend: 170. C
CapillarySE-30+Igepal1051.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillarySE-30+Igepal1055.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51049.Courtois, Paine, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C
CapillaryHP-5MS1044.Ning, Zheng, et al., 200830. m/0.25 mm/0.25 μm, He; Program: 40 0C (2 min) 3 0C/min -> 180 0C (2 min) 15 0C -> 280 0C
CapillaryCBP-51029.Cheriti, Saad, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 60C(2min) => 3C/min => 240C => 10C/min => 300C
CapillaryHP-5MS1050.Liu, Song, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)
CapillaryHP-5MS1041.Mu, Wang, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 8C/min => 160C => 15C/min => 300C
CapillaryHP-51043.Splivallo, Bossi, et al., 2007He; Program: 50C => 3C/min => 200C(10min) => 10C/min => 290C(10min)
CapillaryDB-11026.de Lima, Maia, et al., 2006He; Column length: 30. m; Column diameter: 0.25 mm; Program: 35C => 4C/min => 180C => 10C/min => 250C
CapillaryHP-5MS1051.Deng, Yao, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 50C => 8C/min => 200C => 10C/min => 270C (5min)
CapillaryCP-Sil5 CB MS1031.Iraqi, Vermeulen, et al., 200550. m/0.32 mm/1.2 μm; Program: 36C(2min) => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)
CapillaryHP-5MS1041.Deng, Li, et al., 200430. m/0.25 mm/0.25 μm, He; Program: 60C => 10C/min => 160C => 12C/min => 300C (5min)
CapillaryMDN-51050.Moretti, Madonia, et al., 200430. m/0.25 mm/0.25 μm, Helium; Program: 30 0C (1 min) ballistically -> 60 0C 2 0C/min -> 120 0C 5 0C/min -> 280 0C (5 min)
CapillaryHP-51056.Jordán, Margaría, et al., 200330. m/0.25 mm/0.25 μm; Program: 40C(6min) => 2.5C/min => 150C => 90C/min => 250C
CapillaryHP-51043.Jordán, Goodner, et al., 200230. m/0.25 mm/0.25 μm; Program: not specified
CapillaryDB-51042.Petrakis, Tsitsimpikou, et al., 2001Program: not specified
CapillaryOV-1011038.Yang, 2001N2; Column length: 50. m; Column diameter: 0.25 mm; Program: not specified
CapillaryDB-51033.Storer, Elmore, et al., 199330. m/0.32 mm/1. μm; Program: 0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)
CapillaryDB-51037.Storer, Elmore, et al., 199330. m/0.32 mm/1. μm; Program: 0C(5min) => 60C/min => 60C (5min) => 4C/min => 250C (5min)
CapillarySF96+Igepal1044.Flath, Altieri, et al., 1984Column length: 152. m; Column diameter: 0.76 mm; Program: 25C(1min) => 5C/min => 50C (4min) => 1.25C/min => 180C

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySupelcowax1250.Gauvin-Bialecki and Marodon, 200960. m/0.35 mm/0.25 μm, Nitrogen, 4. K/min, 230. C @ 40. min; Tstart: 60. C
CapillarySupelcowax-101245.Korány, Mednyánszky, et al., 200060. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 280. C
CapillaryCarbowax 20M1254.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillaryCarbowax 20M1259.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jalali-Heravi, Zekavat, et al., 2006
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Cheriti, Saad, et al., 2007
Cheriti, A.; Saad, A.; Belboukhari, N.; Ghezali, S., The essential oil composition of Bubonium graveolens (Forssk.) Maire from the algerian Sahara, Flavour Fragr. J., 2007, 22, 4, 286-288, https://doi.org/10.1002/ffj.1794 . [all data]

Liu, Song, et al., 2007
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Mu, Wang, et al., 2007
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Splivallo, Bossi, et al., 2007
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Notes

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