Naphthalene, 1,2,3,5,6,8a-hexahydro-4,7-dimethyl-1-(1-methylethyl)-, (1S-cis)-

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Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxBP-20HP-InnowaxHP-InnowaxDB-FFAP
Column length (m) 60.50.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.220.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 230.220.220.250.250.
Heat rate (K/min) 2.2.5.5.4.
Initial hold (min)   1.5.4.
Final hold (min) 5.20.5.10.5.
I 1715.1752.1764.1772.1765.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Yapi, Boti, et al., 2012Feng, Cui, et al., 2011Menichini, Tundis, et al., 2011Osorio, Carriazo, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52 CBRTX-WaxBP-20DB-WaxDB-Wax
Column length (m) 60.60. 15.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.22 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 40.60.60.40.80.
Tend (C) 220.230.200.260.240.
Heat rate (K/min) 3.2.5.4.3.
Initial hold (min)      
Final hold (min)  30. 5.2.
I 1768.1736.1753.1756.1754.
ReferenceTsai, Huang, et al., 2011Dib, Djabou, et al., 2010Mishra, Chaudhary, et al., 2010Miyazawa, Kawauchi, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxRTX-WaxBP-20DB-WaxRTX-Wax
Column length (m) 30.60.50.60.60.
Carrier gas HydrogenHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.220.220.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 30.60.60.50.60.
Tend (C) 230.230.220.220.230.
Heat rate (K/min) 8.2.2.3.2.
Initial hold (min) 5.  2. 
Final hold (min) 10.30.20.70.35.
I 1759.1729.1756.1764.1748.
ReferenceKarlsson, Birgersson, et al., 2009Museli, Pau, et al., 2009Ottavioli, Bighelli, et al., 2009Shimizu, Imayoshi, et al., 2009Paolini, Tomi, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP InnowaxHP-InnowaxCarbowaxCarbowaxHP-Innowax
Column length (m) 30.30.60.60.30.
Carrier gas HeliumN2HeHeHe
Substrate      
Column diameter (mm) 0.320.250.20.20.25
Phase thickness (μm) 0.500.250.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 260.240.250.250.240.
Heat rate (K/min) 3.5.2.2.2.
Initial hold (min)  1.8.8. 
Final hold (min)  4.15.15.20.
I 1755.1772.1746.1760.1753.
ReferenceCapetanos, Saroglou, et al., 2007Cheraif, Ben Jannet, et al., 2007Ferhat, Meklati, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Hachicha, Skanji, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBTC-FFAPTC-FFAPCarbowax 20MTC-Wax
Column length (m) 30.  30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 220.220.220.230.240.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min) 1.    
Final hold (min) 2.30.30.  
I 1759.1791.1756.1740.1752.
ReferenceHymete, Rohloff, et al., 2007Kurose, Okamura, et al., 2007Kurose, Okamura, et al., 2007Limberger, Scopel, et al., 2007Miyazawa and Tamura, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10CP-Wax 52CBSupelcowax-10Supelcowax-10Supelcowax-10
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.20.320.250.250.25
Phase thickness (μm) 0.20.50.250.250.25
Tstart (C) 70.40.50.40.40.
Tend (C) 220.220.250.210.250.
Heat rate (K/min) 3.4.2.2.3.
Initial hold (min)  8.  5.
Final hold (min) 15.20. 33.10.
I 1751.1765.1750.1758.1767.
ReferencePinto, Salgueiro, et al., 2007Povolo, Contarini, et al., 2007Raal, Orav, et al., 2007Sylvestre, Longtin, et al., 2007Vichi, Riu-Aumatell, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-WaxBP-20BP-20DB-WaxSupelcowax 10
Column length (m) 60.50.50.60.30.
Carrier gas HeHe HeHelium
Substrate      
Column diameter (mm) 0.250.220.220.250.20
Phase thickness (μm) 0.250.250.250.50.20
Tstart (C) 60.60.60.50.70.
Tend (C) 200.220.220.230.220.
Heat rate (K/min) 4.2.2.3.3.
Initial hold (min)    2. 
Final hold (min) 20.20.20.20.15.
I 1760.1746.1754.1748.1751.
ReferenceBorges, Rojas, et al., 2006Boti, Muselli, et al., 2006Boti, Yao, et al., 2006Cai, Lin, et al., 2006Cavaleiro, Pinto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-20MSupelcowax-10DB-WaxBP-20Supelcowax
Column length (m) 50.30.60.50.30.
Carrier gas He  HeN2
Substrate      
Column diameter (mm) 0.20.250.250.220.32
Phase thickness (μm) 0.10.250.250.250.25
Tstart (C) 60.40.70.60.50.
Tend (C) 220.210.230.220.200.
Heat rate (K/min) 2.2.2.2.5.
Initial hold (min)  2.2.  
Final hold (min) 30.33.20.20. 
I 1718.1758.1758.1757.1762.
ReferenceFilippi, Lanfranchi, et al., 2006Garneau F.X., Collin G., et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lesueur, Ban, et al., 2006Martin, Joseph, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-WaxHP-20MDB-InnowaxNB-20MSupelcowax-10
Column length (m) 30.30.60.30.30.
Carrier gas NitrogenN2HeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.50.50.
Tend (C) 280.250.240.250.220.
Heat rate (K/min) 5.5.3.2.4.
Initial hold (min)     1.
Final hold (min) 5.10.20. 10.
I 1720.1720.1761.1745.1753.
ReferenceMarzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Mendivil, Rodrigues, et al., 2006Orav, Raal, et al., 2006Wong, Lim, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxHP-20MSupelcowaxCP-WaxHP-20M
Column length (m) 50.50.60.30.50.
Carrier gas HeHeliumHeHeHelium
Substrate      
Column diameter (mm) 0.20.200.20.320.20
Phase thickness (μm) 0.50.200.20.250.20
Tstart (C) 60.70.60.40.70.
Tend (C) 250.250.230.180.180.
Heat rate (K/min) 2.4.4.5.4.
Initial hold (min)  4.30.2.4.
Final hold (min) 60.10.  10.
I 1755.1729.1733.1739.1729.
ReferenceBendimerad and Bendiab, 2005Bezic, Skocibusic, et al., 2005Gauvin and Smadja, 2005Ka, Choi, et al., 2005Kulisic, Radonic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-20MDB-WaxCP-Wax 52CBSupelcowax-10Carbowax
Column length (m) 50.30.30.30.30.
Carrier gas HeliumHeHe  
Substrate      
Column diameter (mm) 0.200.250.320.250.25
Phase thickness (μm) 0.200.250.250.250.25
Tstart (C) 70.50.40.40.40.
Tend (C) 180.180.220.210.200.
Heat rate (K/min) 4.3.4.2.4.
Initial hold (min) 4. 1.2. 
Final hold (min) 10.40. 33. 
I 1729.1745.1755.1733.1761.
ReferenceKulisic, Radonic, et al., 2005Lee, Umano, et al., 2005Rohloff and Bones, 2005Stevanovic, Garneau, et al., 2005Szafranek, Chrapkowska, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10BP-20Supelcowax-10Supelcowax-10Carbowax 20M
Column length (m) 30.50.60.30.30.
Carrier gas   HeN2He
Substrate      
Column diameter (mm) 0.250.220.20.250.25
Phase thickness (μm) 0.250.250.20.250.25
Tstart (C) 40.60.60.40.60.
Tend (C) 220.220.200.230.250.
Heat rate (K/min) 3.2.4.2.3.
Initial hold (min) 5.    
Final hold (min) 10.20.40.  
I 1767.1747.1732.1744.1778.
ReferenceVichi, Riu-Aumatell, et al., 2005Blanc, Muselli, et al., 2004Gauvin, Ravaomanarivo, et al., 2004González, Guerra, et al., 2004Lago, de Ávila, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Innowax FSCInnowax FSCSupelcowax-10Supelcowax-10
Column length (m) 30.60.60.50.50.
Carrier gas  HeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.2
Phase thickness (μm) 0.25  0.250.25
Tstart (C) 40.60.60.70.70.
Tend (C) 210.220.220.230.230.
Heat rate (K/min) 2.4.4.2.2.
Initial hold (min) 2.10.10.  
Final hold (min) 33.    
I 1758.1741.1773.1749.1748.
ReferenceLopez Arze, Collin, et al., 2004Lourens, Reddy, et al., 2004Lourens, Reddy, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSW-10HP-WaxHP-20MTC-Wax
Column length (m) 60.50.30.50.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.320.200.250.20.25
Phase thickness (μm) 0.250.250.250.2 
Tstart (C) 35.50.60.70.80.
Tend (C) 220.230.220.180.240.
Heat rate (K/min) 3.2.5.4.3.
Initial hold (min)   10.4. 
Final hold (min)    10. 
I 1760.1748.1785.1732.1756.
ReferencePalá-Paúl, Brophy, et al., 2004Raal, Paaver, et al., 2004Bertoli, Menichini, et al., 2003Juteau, Jerkovic, et al., 2003Miyazawa, Teranishi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10SW-10Supelcowax-10HP-Innowax
Column length (m) 60.50.50.30.50.
Carrier gas HeliumHeHeN2 
Substrate      
Column diameter (mm) 0.250.20.200.250.2
Phase thickness (μm)  0.250.250.250.2
Tstart (C) 70.70.50.40.50.
Tend (C) 210.230.250.230.220.
Heat rate (K/min) 2.2.2.2.4.
Initial hold (min)     5.
Final hold (min) 60.    
I 1762.1749.1740.1744.1785.
ReferenceMookdasanit, Tamura, et al., 2003Orav, Kailas, et al., 2003Raal, Arak, et al., 2003Rotman, Ahumada, et al., 2003Stashenko, Jaramillo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxInnowaxCarbowax 20MDB-WaxSupelcowax-10
Column length (m) 50.60.25.60.30.
Carrier gas  HeN2H2 
Substrate      
Column diameter (mm) 0.20.250.250.320.25
Phase thickness (μm) 0.2 0.250.250.25
Tstart (C) 50.60.50.40.40.
Tend (C) 220.220.250.245.210.
Heat rate (K/min) 4.4.4.1.52.
Initial hold (min) 5.10.  2.
Final hold (min)  10.10.20.33.
I 1785.1773.1766.1743.1733.
ReferenceStashenko, Jaramillo, et al., 2003Suleimenov, Atazharova, et al., 2003Zrira, Elamrani, et al., 2003Gancel, Ollé, et al., 2002Kabouss, Charrouf, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MSupelcowax-10DB-WaxDB-WaxDB-Wax
Column length (m) 30.60.60.60.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.3250.50.250.250.25
Tstart (C) 50.70.70.40.45.
Tend (C) 215.220.230.200.240.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min)   2.2. 
Final hold (min) 20. 20.  
I 1761.1749.1749.1739.1756.
ReferenceKasali, Winterhalter, et al., 2002Orav, Kailas, et al., 2002Tu, Onishi, et al., 2002Umano, Hagi, et al., 2002Christoph, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-WaxPEG-20MPEG-20MCarbowax 20MCP-Wax 52CB
Column length (m) 60.50.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.20.220.30
Phase thickness (μm)    0.250.25
Tstart (C) 80.70.70.60.40.
Tend (C) 250.220.220.220.220.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min)     5.
Final hold (min) 47.    
I 1745.1749.1749.1760.1761.
ReferenceMiyazawa, Kurose, et al., 2001Orav and Kann, 2001Orav and Kann, 2001Vernin, Lageot, et al., 2001Chagonda, Makanda, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxBP-20HP-20MDB-WaxDB-Wax
Column length (m) 30.25.50.60.60.
Carrier gas HeNitrogenHeHeliumNitrogen
Substrate      
Column diameter (mm) 0.20.500.200.320.25
Phase thickness (μm)  0.250.200.25 
Tstart (C) 50.60.70.50.40.
Tend (C) 180.200.180.230.200.
Heat rate (K/min) 3.5.4.5.2.
Initial hold (min) 8. 4.2.10.
Final hold (min)      
I 1725.1737.1729.1755.1768.
ReferenceFranco and Shibamoto, 2000Mallavarapu, Rao, et al., 2000Mastelic, Milos, et al., 2000Paniandy, Chane-Ming, et al., 2000Tamura, Boonbumrung, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxFFAPBP-20HP Innowax FSPInnowax
Column length (m) 60.25.25.60.60.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.250.330.250.25
Phase thickness (μm) 0.25 0.50.250.25
Tstart (C) 40.70.80.60.60.
Tend (C) 200.210.220.220.220.
Heat rate (K/min) 2.3.5.  
Initial hold (min) 2.5. 10.10.
Final hold (min)    10. 
I 1755.1759.1774.1772.1772.
ReferenceUmano, Hagi, et al., 2000Ajaiyeoba and Ekundayo, 1999Dunlop, Bignell, et al., 1999Kaya, Baser, et al., 1999Kaya, Baser, et al., 1999, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-InnowaxSupelcowax-10DB-WaxNB-351
Column length (m) 60.60.30.60.25.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.3
Phase thickness (μm) 0.250.25 0.250.5
Tstart (C) 60.60.60.60.70.
Tend (C) 220.220.240.240.250.
Heat rate (K/min)   4.4.5.
Initial hold (min) 10.10.  2.
Final hold (min)      
I 1772.1772.1760.1765.1754.
ReferenceKaya, Baser, et al., 1999, 3Kaya, Baser, et al., 1999, 3Labuckas, Zygadlo, et al., 1999Ngassoum, Yonkeu, et al., 1999Onocha, Ekundayo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20HP-20MDB-WaxDB-WaxHP-Innowax
Column length (m) 25.50.30.30.60.
Carrier gas H2HeN2N2He
Substrate      
Column diameter (mm) 0.330.20.250.250.25
Phase thickness (μm) 0.50.20.250.250.25
Tstart (C) 80.70.45.45.50.
Tend (C) 220.180.220.220.220.
Heat rate (K/min) 5.4.3.3.5.
Initial hold (min)  4.  5.
Final hold (min)  10.   
I 1774.1716.1788.1769.1768.
ReferenceBignell, Dunlop, et al., 1998Milso, Mastelic, et al., 1998Molleken U., Sinnwell V., et al., 1998Mölleken, Sinnwell, et al., 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-Innowax FSCBP-20BP-20BP-20
Column length (m) 60.60.25.25.25.
Carrier gas HeHeH2H2H2
Substrate      
Column diameter (mm) 0.250.250.330.330.33
Phase thickness (μm) 0.25 0.50.50.5
Tstart (C) 60.60.80.80.80.
Tend (C) 220.240.220.220.220.
Heat rate (K/min) 4.4.5.5.5.
Initial hold (min) 10.10.   
Final hold (min) 10.10.   
I 1772.1772.1774.1774.1774.
ReferenceTümen, Baser, et al., 1998Baser, Kirimer, et al., 1997Bignell, Dunlop, et al., 1997Bignell, Dunlop, et al., 1997, 2Bignell, Dunlop, et al., 1997, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20BP-20Supelcowax-10Supelcowax-10
Column length (m) 25.25.25.30.0.
Carrier gas H2 H2 He
Substrate      
Column diameter (mm) 0.330.330.330.250.25
Phase thickness (μm) 0.50.50.5  
Tstart (C) 80.80.80.60.40.
Tend (C) 220.220.220.240.240.
Heat rate (K/min) 5.5.5.4.3.
Initial hold (min)      
Final hold (min)      
I 1774.1774.1774.1757.1757.
ReferenceBignell, Dunlop, et al., 1997, 4Bignell, Dunlop, et al., 1997, 5Bignell, Dunlop, et al., 1997, 6Zunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SP-1000PEG-20MDB-WaxDB-WaxTC-Wax
Column length (m) 85.50.30.60.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.500.250.320.320.25
Phase thickness (μm)   0.50.50 
Tstart (C) 65.70.40.50.80.
Tend (C) 225.250.210.250.240.
Heat rate (K/min) 3.2.3.8.3.
Initial hold (min)   1.1.5.
Final hold (min)   25.6. 
I 1758.1749.1745.1769.1759.
ReferenceBrophy, Goldsack, et al., 1996Orav, Kailas, et al., 1996Pollak and Berger, 1996Sagrero-Nieves and Bartley, 1996Shuichi, Masazumi, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10DB-WaxCarbowax 20MCP-Wax 52CB
Column length (m) 60.60.60.60.50.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.22
Tstart (C) 50.40.50.50.50.
Tend (C) 180.200.180.150.200.
Heat rate (K/min) 2.53.2.52.2.
Initial hold (min) 5.3.5.10.5.
Final hold (min)  30. 20. 
I 1780.1757.1759.1766.1731.2
ReferenceStashenko, Puertas, et al., 1996Wong and Lai, 1996Stashenko, Torres, et al., 1995Tirado, Stashenko, et al., 1995Chyau, Chen, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 45.60.60.30.60.
Carrier gas Hydrogen    
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 1.0    
Tstart (C) 60.50.50.70.50.
Tend (C) 200.230.230.200.250.
Heat rate (K/min) 2.4.4.4.4.
Initial hold (min) 5.  2.0.1
Final hold (min)  10.10. 5.
I 1740.1752.1752.1767.1752.
ReferenceKollmannsberger, Nitz, et al., 1992Binder, Benson, et al., 1990Binder, Turner, et al., 1990Wyllie, Brophy, et al., 1990Binder and Flath, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase FFAPCarbowax 20MDB-WaxDB-WaxSupelcowax-10
Column length (m) 50.50.60.60.30.
Carrier gas  H2HeHe 
Substrate      
Column diameter (mm)  0.320.320.32 
Phase thickness (μm)  0.150.250.25 
Tstart (C) 50.70.30.30.50.
Tend (C) 180.210.180.180.240.
Heat rate (K/min) 10.2.2.2.4.
Initial hold (min) 1. 4.4.2.
Final hold (min)     10.
I 1777.1740.1732.1734.1763.
ReferenceBrophy, Davies, et al., 1989Gaydou, Faure, et al., 1989Takeoka and Butter, 1989Takeoka and Butter, 1989Ramaswami, Briscese, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MSupelcowax-10Carbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 25.30.150.150.150.
Carrier gas  He   
Substrate      
Column diameter (mm) 0.30 0.660.660.64
Phase thickness (μm)      
Tstart (C) 40.50.60.60.50.
Tend (C) 220.240.170.170.170.
Heat rate (K/min) 2.4.1.1.1.
Initial hold (min) 5.2.40.40.30.
Final hold (min)  10.   
I 1752.1763.1730.1730.1730.
ReferenceNykanen, 1986Ramaswami, Briscese, et al., 1986Buttery, Xu, et al., 1985Buttery and Ling, 1984Buttery, Parker, et al., 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase Carbowax 20MCarbowax 20M
Column length (m) 100.100.
Carrier gas   
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (μm)   
Tstart (C) 70.70.
Tend (C) 170.170.
Heat rate (K/min) 1.1.
Initial hold (min)   
Final hold (min)   
I 1766.1768.
ReferenceShibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Ottavioli, Bighelli, et al., 2009
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Shimizu, Imayoshi, et al., 2009
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Paolini, Tomi, et al., 2008
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Capetanos, Saroglou, et al., 2007
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Ferhat, Meklati, et al., 2007
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Hachicha, Skanji, et al., 2007
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Hymete, Rohloff, et al., 2007
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Kurose, Okamura, et al., 2007
Kurose, K.; Okamura, D.; Yatagai, M., Composition of the essential oils from the leaves of nine Pinus species and the cones of three of Pinus species, Flavour Fragr. J., 2007, 22, 1, 10-20, https://doi.org/10.1002/ffj.1609 . [all data]

Limberger, Scopel, et al., 2007
Limberger, R.P.; Scopel, M.; Sobral, M.; Henriques, A.T., Comparative analysis of volatiles from Drimys brasiliensis Miers and D. angustifolia Miers (Winteraceae) from Southern Brazil, Biochem. Syst. Ecol., 2007, 35, 3, 130-137, https://doi.org/10.1016/j.bse.2006.09.007 . [all data]

Miyazawa and Tamura, 2007
Miyazawa, M.; Tamura, N., Components of the essential oil from sprouts of Polygonum hydropiper L. ('Benitade'), Flavour Fragr. J., 2007, 22, 3, 188-190, https://doi.org/10.1002/ffj.1779 . [all data]

Pinto, Salgueiro, et al., 2007
Pinto, E.; Salgueiro, L.R.; Cavaleiro, C.; Palmeira, A.; Goncalves, M.J., In vitro susceptibility of some species of yeasts and filamentous fungi to essential oils of Salvia of?cinalis, Ind. Crops Prod., 2007, 26, 2, 135-141, https://doi.org/10.1016/j.indcrop.2007.02.004 . [all data]

Povolo, Contarini, et al., 2007
Povolo, M.; Contarini, G.; Mele, M.; Secchiari, P., Study on the influence of pasture on volatile fraction of Ewes' dairy products by solid-phase microextraction and gas chromatography-mass spectrometry, J. Dairy Sci., 2007, 90, 2, 556-569, https://doi.org/10.3168/jds.S0022-0302(07)71539-4 . [all data]

Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M., Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia, Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]

Sylvestre, Longtin, et al., 2007
Sylvestre, M.; Longtin, A.P.A.; Legault, J., Volatile leaf condtituents and anticancer activity of Bursera simaruba (L.) Sarg. essential oil, Natural Product Communications, 2007, 2, 12, 1273-1276. [all data]

Vichi, Riu-Aumatell, et al., 2007
Vichi, S.; Riu-Aumatell, M.; Mora-Pons, M.; Guadayol, J.M.; Buxaderas, S.; López-Tamames, E., Analytical, Nutritional and Clinical Methods. HS-SPME coupled to GC/MS for quality control of Juniperus communis L. berries used for gin aromatization, Food Chem., 2007, 105, 4, 1748-1754, https://doi.org/10.1016/j.foodchem.2007.03.026 . [all data]

Borges, Rojas, et al., 2006
Borges, R.; Rojas, L.B.; Cegarra, J.A.; Usubillaga, A., Study of the essential oils from the leaves and flowers of Lepechinia conferta (Benth) Epl., Flavour Fragr. J., 2006, 21, 1, 155-157, https://doi.org/10.1002/ffj.1550 . [all data]

Boti, Muselli, et al., 2006
Boti, J.B.; Muselli, A.; Tomi, F.; Koukoua, G.; N'Guessan, T.Y.; Costa, J.; Casanova, J., Combined analysis of Cymbopogon giganteus Chiov. leaf oil from Ivory Coast by GC/RI, GC/MS and 13C-NMR, C.R. Chim., 2006, 9, 1, 164-168, https://doi.org/10.1016/j.crci.2005.10.003 . [all data]

Boti, Yao, et al., 2006
Boti, J.B.; Yao, P.A.; Koukoua, G.; N'Guessan, T.Y.; Casanova, J., Components and chemical variability of Isolona campanulata Engler Diels leaf oil, Flavour Fragr. J., 2006, 21, 1, 166-170, https://doi.org/10.1002/ffj.1555 . [all data]

Cai, Lin, et al., 2006
Cai, J.; Lin, P.; Zhu, X.; Su, Q., Comparative analysis of clary sage (S. sclarea L.) oil volatiles by GC-FTIR and GC-MS, Food Chem., 2006, 99, 2, 401-407, https://doi.org/10.1016/j.foodchem.2005.07.041 . [all data]

Cavaleiro, Pinto, et al., 2006
Cavaleiro, C.; Pinto, E.; Gonsales, M.J.; Salguero, L., Antifungal activity of Juniperus essential oils agains dermatophyte, Asrgillus and Candida strains, J. Appl. Microbiol., 2006, 100, 6, 1333-1338, https://doi.org/10.1111/j.1365-2672.2006.02862.x . [all data]

Filippi, Lanfranchi, et al., 2006
Filippi, J.-J.; Lanfranchi, D.-A.; Prado, S.; Baldovini, N.; Meierhenrich, U.J., Composition, Enantiomeric Distribution, and Antibacterial Activity of the Essential Oil of Achillea ligustica All. from Corsica, J. Agric. Food Chem., 2006, 54, 17, 6308-6313, https://doi.org/10.1021/jf060752y . [all data]

Garneau F.X., Collin G., et al., 2006
Garneau F.X.; Collin G.; Gagnon H.; Jean F.I.; Strobl H.; Pichette A., The essential oil composition of Devil's Club, Oplopanax horridus J. E. Smith Miq., Flavour Fragr. J., 2006, 21, 5, 792-794, https://doi.org/10.1002/ffj.1716 . [all data]

Lan Phi N.T., Nishiyama C., et al., 2006
Lan Phi N.T.; Nishiyama C.; Choi H.-S.; Sawamura M., Evaluation of aroma characteristic compounds of Citrus natsudaidai Hayata (Natsudaidai) cold-pressed peel oil, Biosci. Biotechnol. Biochem., 2006, 70, 8, 1832-1838, https://doi.org/10.1271/bbb.50705 . [all data]

Lesueur, Ban, et al., 2006
Lesueur, D.; Ban, N.K.; Bighelli, A.; Muselli, A.; Casanova, J., Analysis of the root oil of Fokienia hodginsii (Dunn) Henry et Thomas (Cupressaceae) by GC, GC-MS and 13C-NMR, Flavour Fragr. J., 2006, 21, 1, 171-174, https://doi.org/10.1002/ffj.1557 . [all data]

Martin, Joseph, et al., 2006
Martin, M.A.C.K.; Joseph, H.; Bercion, S.; Menut, C., Chemical composition of essential oils from aerial parts of Aframomum exscapum (Sims) Hepper collected in Guadeloupe, French West Indies, Flavour Fragr. J., 2006, 21, 6, 902-905, https://doi.org/10.1002/ffj.1741 . [all data]

Marzouk, Mansour, et al., 2006
Marzouk, Z.; Mansour, H.B.; Chraief, I.; Mosrati, R.; Cheriaa, J.; Neffati, A.; Marzouk, B.; Sfari, M.; Boukef, K.; Barillies, D.; Ghedira, L.C., Chemical composition, antibacterial and antimutagenic activities of four populations of Rosmarinus officinalis L. oils from Tunisia, J. Food Agriculture Environment, 2006, 4, 2, 89-94. [all data]

Marzouk, Neffati, et al., 2006
Marzouk, Z.; Neffati, A.; Marzouk, B.; Chraief, I.; Fathia, K.; Ghedira, L.C.; Boukef, K., Chemical composition and antibacterial and antimutagenic activity of Tunisian Rosmarinus officinalis L. oil from Kasrine, Journal of Food, Agriculture Environment, 2006, 4, 34, 61-65. [all data]

Mendivil, Rodrigues, et al., 2006
Mendivil, E.A.S.; Rodrigues, J.F.; Espinosa, M.E.; Fajardo, J.A.G.; Vosques, E.N.O., Chemical Composition and Fungicidal Activity of the Essential Oil of Thymus vulgaris against Alternaria citri, e-Gnosis, 2006, 4, 1-7, retrieved from http://www.e-gnosis.udg.mx. [all data]

Orav, Raal, et al., 2006
Orav, A.; Raal, A.; Arak, E.; Müürisepp, M.; Kailas, T., Composition of the essential oil of Artemisia absinthium L. of different geographical origin, Proc. Est. Acad. Sci. Chem., 2006, 55, 3, 155-165. [all data]

Wong, Lim, et al., 2006
Wong, K.C.; Lim, T.B.; Ali, D.M.H., Essential oil of Homalomena sagittifolia Jungh., Flavour Fragr. J., 2006, 21, 5, 786-788, https://doi.org/10.1002/ffj.1714 . [all data]

Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

Bezic, Skocibusic, et al., 2005
Bezic, N.; Skocibusic, M.; Dunkic, V., Phytochemical Composition and Antimicrobial Activityof Satureja montana L. and Satureja cunefolia Ten. Essential Oils, Acta Bot. Croat., 2005, 64, 2, 313-322. [all data]

Gauvin and Smadja, 2005
Gauvin, A.; Smadja, J., Essential oil composition of four Psiadia species from Reunion Island: A chemotaxonomic study, Biochem. Syst. Ecol., 2005, 33, 7, 705-714, https://doi.org/10.1016/j.bse.2004.12.013 . [all data]

Ka, Choi, et al., 2005
Ka, M.-H.; Choi, E.H.; Chun, H.-S.; Lee, K.-G., Antioxidative Activity of Volatile Extracts Isolated from Angelica tenuissimae Roots, Peppermint Leaves, Pine Needles, and Sweet Flag Leaves, J. Agric. Food Chem., 2005, 53, 10, 4124-4129, https://doi.org/10.1021/jf047932x . [all data]

Kulisic, Radonic, et al., 2005
Kulisic, T.; Radonic, A.; Milos, M., Inhibition of Lard Oxidation by Fractions of Different Essential Oil, Grasas y Aceites, 2005, 56, 4, 284-291, https://doi.org/10.3989/gya.2005.v56.i4.94 . [all data]

Lee, Umano, et al., 2005
Lee, S.-J.; Umano, K.; Shibamoto, T.; Lee, K.-G., Identification of volatile components in basil (Ocimum basilicum L.) and thyme leaves (Thymus vulgaris L.) and their antioxidant properties, Food Chem., 2005, 91, 1, 131-137, https://doi.org/10.1016/j.foodchem.2004.05.056 . [all data]

Rohloff and Bones, 2005
Rohloff, J.; Bones, A.M., Volatile profiling of Arabidopsis thaliana - Putative olfactory compounds in plant communication, Phytochemistry, 2005, 66, 16, 1941-1955, https://doi.org/10.1016/j.phytochem.2005.06.021 . [all data]

Stevanovic, Garneau, et al., 2005
Stevanovic, T.; Garneau, F.-X.; Jean, F.-I.; Gagnon, H.; Vilotic, D.; Petrovic, S.; Ruzic, N.; Pichette, A., The essential oil composition of Pinus mugo Turra from Serbia, Flavour Fragr. J., 2005, 20, 1, 96-97, https://doi.org/10.1002/ffj.1390 . [all data]

Szafranek, Chrapkowska, et al., 2005
Szafranek, B.; Chrapkowska, K.; Pawinska, M.; Szafranek, J., Analysis of leaf surface sesquiterpenes in potato varieties, J. Agric. Food Chem., 2005, 53, 8, 2817-2822, https://doi.org/10.1021/jf040437g . [all data]

Vichi, Riu-Aumatell, et al., 2005
Vichi, S.; Riu-Aumatell, M.; Mora-Pons, M.; Buxaderas, S.; Lopez-Tamames, E., Characterization of Volatiles in Different Dry Gins, J. Agric. Food Chem., 2005, 53, 26, 10154-10160, https://doi.org/10.1021/jf058121b . [all data]

Blanc, Muselli, et al., 2004
Blanc, M.-C.; Muselli, A.; Bradesi, P.; Casanova, J., Chemical composition and variability of the essential oil of Inula graveolens from Corsica, Flavour Fragr. J., 2004, 19, 4, 314-319, https://doi.org/10.1002/ffj.1304 . [all data]

Gauvin, Ravaomanarivo, et al., 2004
Gauvin, A.; Ravaomanarivo, H.; Smadja, J., Comparative analysis by gas chromatography?mass spectrometry of the essential oils from bark and leaves of Cedrelopsis grevei Baill, an aromatic and medicinal plant from Madagascar, J. Chromatogr. A, 2004, 1029, 1-2, 279-282, https://doi.org/10.1016/j.chroma.2003.12.012 . [all data]

González, Guerra, et al., 2004
González, S.; Guerra, P.E.; Bottaro, H.; Molares, S.; Demo, M.S.; Oliva, M.M.; Zunino, M.P.; Zygadlo, J.A., Aromatic plants from Patagonia. Part I. Antimicrobial activity and chemical composition of Schinus polygamus (Cav.) Cabrera essential oil, Flavour Fragr. J., 2004, 19, 1, 36-39, https://doi.org/10.1002/ffj.1270 . [all data]

Lago, de Ávila, et al., 2004
Lago, J.H.G.; de Ávila, P., Jr.; de Aquino, E.M.; Moreno, P.R.H.; Ohara, M.T.; Limberger, R.P.; Apel, M.A.; Henriques, A.T., Volatile oils from leaves and stem barks of Cedrela fissilis (Meliaceae): chemical composition and antibacterial activities, Flavour Fragr. J., 2004, 19, 5, 448-451, https://doi.org/10.1002/ffj.1347 . [all data]

Lopez Arze, Collin, et al., 2004
Lopez Arze, J.B.; Collin, G.; Garneau, F.-X.; Jean, F.-I.; Gagnon, H., Essential oils from Bolivia. II. Asteraceae: Ophryosporus heptanthus (Wedd.) H. Rob. et King, J. Essent. Oil Res., 2004, 16, 4, 374-376, https://doi.org/10.1080/10412905.2004.9698747 . [all data]

Lourens, Reddy, et al., 2004
Lourens, A.C.U.; Reddy, D.; Baser, K.H.C.; Viljoen, A.M.; Van Vuuren, S.F., In vitro Biological Activity and Essential Oil Composition of Four Indigenous South Africal Helichrysum Species, J. Ethnopharmacol., 2004, 95, 2-3, 253-258, https://doi.org/10.1016/j.jep.2004.07.027 . [all data]

Orav, Stulova, et al., 2004
Orav, A.; Stulova, I.; Kailas, T.; Müürisepp, M., Effect of storage on the essential oil composition of piper nigrum L. fruits of different ripening states, J. Agric. Food Chem., 2004, 52, 9, 2582-2586, https://doi.org/10.1021/jf030635s . [all data]

Palá-Paúl, Brophy, et al., 2004
Palá-Paúl, J.; Brophy, J.J.; Goldsack, R.J.; Fontaniella, B., Analysis of the volatile components of Lavandula canariensis (L.) Mill., a Canary Islands endemic species, growing in Australia, Biochem. Syst. Ecol., 2004, 32, 1, 55-62, https://doi.org/10.1016/S0305-1978(03)00177-7 . [all data]

Raal, Paaver, et al., 2004
Raal, A.; Paaver, U.; Arak, E.; Orav, A., Content and composition of the essential oil of Thymus serpyllum L. growing wild in Estonia, Medicina (Kaunas), 2004, 40, 8, 795-800. [all data]

Bertoli, Menichini, et al., 2003
Bertoli, A.; Menichini, F.; Mazzetti, M.; Spinelli, G.; Morelli, I., Volatile constituents of the leaves and flowers of Hypericum triquetrifolium Turra, Flavour Fragr. J., 2003, 18, 2, 91-94, https://doi.org/10.1002/ffj.1161 . [all data]

Juteau, Jerkovic, et al., 2003
Juteau, F.; Jerkovic, I.; Masotti, V.; Milos, M.; Mastelic, J.; Bessière, J.-M.; Viano, J., Composition and antimicrobial activity of the essential oil of Artemisia absinthium from Croatia and France, Planta Medica, 2003, 69, 2, 158-161, https://doi.org/10.1055/s-2003-37714 . [all data]

Miyazawa, Teranishi, et al., 2003
Miyazawa, M.; Teranishi, A.; Ishikawa, Y., Components of the essential oil from Petasites japonicus, Flavour Fragr. J., 2003, 18, 3, 231-233, https://doi.org/10.1002/ffj.1203 . [all data]

Mookdasanit, Tamura, et al., 2003
Mookdasanit, J.; Tamura, H.; Yoshizawa T.; Tokunaga T.; Nakanishi, K., Trace Volatile Compounds in Essential Oil of Citrus Sudachi by Means of Modified Solvent Extraction Method, Food Sci Technol. Res., 2003, 9, 1, 54-61, https://doi.org/10.3136/fstr.9.54 . [all data]

Orav, Kailas, et al., 2003
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Raal, Arak, et al., 2003
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Notes

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