Bicyclo[3.1.0]hexan-3-one, 4-methyl-1-(1-methylethyl)-, [1S-(1α,4β,5α)]-


Phase change data

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: William E. Acree, Jr., James S. Chickos

Enthalpy of vaporization

ΔvapH (kJ/mol) Temperature (K) Method Reference Comment
51.8326.AStephenson and Malanowski, 1987Based on data from 311. to 474. K. See also Stull, 1947.

Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin TNO Volatile Compounds in Food - Chemical Concepts
NIST MS number 249064

All mass spectra in this site (plus many more) are available from the NIST/EPA/NIH Mass Spectral Library. Please see the following for information about the library and its accompanying search program.


Gas Chromatography

Go To: Top, Phase change data, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51114.Adams, González Elizondo, et al., 200630. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-5MS1119.Angioni, Barra, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min, 180. C @ 15. min; Tstart: 60. C
CapillaryDB-51114.Lucero, Fredrickson, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C
CapillaryDB-51114.Shatar S., 20053. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51115.Amparo Blázquez, Pérez, et al., 2003He, 40. C @ 5. min, 3. K/min, 280. C @ 5. min; Column length: 25. m; Column diameter: 0.25 mm
CapillaryHP-51110.Özcan, Tzakou, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryBP-11115.Raina, Srivastava, et al., 200225. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryHP-51112.Tzakou and Couladis, 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillarySE-541114.Adams, 200030. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51114.Adams, 2000, 230. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillarySE-541114.Adams, 2000, 330. m/0.26 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51114.Adams, 2000, 430. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51114.Adams, 199930. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51122.Loayza, Abujder, et al., 199540. C @ 2. min, 2. K/min, 210. C @ 120. min; Column length: 30. m

Kovats' RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-5MS1117.Tuberoso, Kowalczyk, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 60C(5min) => 2C/min => 140C= 5C/min => 250C(5min)
CapillaryDB-5MS1127.Radulescu, Chiliment, et al., 200430. m/0.32 mm/0.25 μm, He; Program: 40C (3min) => 5C/min => 160C (2min) => 10C/min => 280C (10min)
CapillaryOV-11093.El-Shazly, Dorai, et al., 200230. m/0.25 mm/0.25 μm, He; Program: 44C(4min) => 3C/min => 74C => 6C/min => 134C => 12C/min => 312C
CapillaryDB-51114.Adams, 199830. m/0.26 mm/0.25 μm; Program: not specified

Kovats' RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillarySupelcowax-101441.Tzakou and Couladis, 200130. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 75. C; Tend: 230. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-51115.Flamini, Cioni, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1110.Kundakovic, Fokialakis, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1112.Saroglou, Marin, et al., 200730. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryZB-51115.Simoniatto, Bonani, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5MS1103.Vagionas, Ngassapa, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillarySPB-11123.Blagojevic, Radulovic, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryDB-51114.Blagojevic, Radulovic, et al., 200630. m/0.2 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryHP-5MS1116.Saroglou, Dorizas, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryRTX-11100.Cozzani, Muselli, et al., 200560. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-51101.Senatore, Napolitano, et al., 200530. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 260. C @ 20. min
CapillarySPB-11089.Antunes, Sevinate-Pinto, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryHP-51116.Javidnia, Miri, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C
CapillaryHP-51116.Flamini, Luigi Cioni, et al., 200330. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryHP-51114.Karioti, Skaltsa, et al., 200330. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryHP-51114.Tsiri, Kretsi, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51114.Tsiri, Kretsi, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51115.Tzakou, Couladis, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1116.Couladis, Chinou, et al., 200230. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 300. C
CapillaryHP-51111.Couladis, Tsortanidou, et al., 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 380. C
CapillaryHP-51115.Couladis, Tzakou, et al., 200130. m/0.25 mm/0.50 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1114.Giamakis, Kretsi, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-5MS1115.Skaltsa, Mavrommati, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryBPX-51135.Zabaras and Wyllie, 200150. m/0.22 mm/0.25 μm, H2, 60. C @ 5. min, 4. K/min, 180. C @ 5. min
CapillaryDB-11108.3Helmig, Klinger, et al., 199960. m/0.32 mm/1. μm, -50. C @ 2. min, 6. K/min; Tend: 175. C
CapillaryDB-11092.Mirza and Sefidkon, 199960. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 220. C
CapillaryOV-11092.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 μm, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryDB-51116.Isidorov, Zenkevich, et al., 199830. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 50. C; Tend: 250. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-5MS1121.3Andriamaharavo, 201430. m/0.25 mm/0.25 μm, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryBPX-51126.Cardeal, da Silva, et al., 200630. m/0.25 mm/0.25 μm; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min)
CapillaryHP-5MS1114.Akpulat, Tepe, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 50C (3min) => 3C/min => 200C => 6C/min => 240C
Capillary5 % Phenyl methyl siloxane1114.Sacchetti, Maietti, et al., 200530. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1451.Kundakovic, Fokialakis, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-20M1426.Maksimovic, Vidic, et al., 200750. m/0.2 mm/0.2 μm, He, 70. C @ 4. min, 4. K/min, 180. C @ 10. min
CapillaryRTX-Wax1426.Cozzani, Muselli, et al., 200560. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-20M1413.Jerkovic, Mastelic, et al., 200350. m/0.2 mm/0.2 μm, He, 70. C @ 4. min, 4. K/min, 180. C @ 10. min
CapillaryHP-Innowax1442.Tzakou, Couladis, et al., 200330. m/0.25 mm/0.5 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C
CapillaryInnowax1442.Couladis, Chinou, et al., 200230. m/0.25 mm/0.5 μm, He, 3. K/min, 260. C @ 10. min; Tstart: 60. C
CapillaryHP-Innowax1442.Couladis, Tzakou, et al., 200130. m/0.25 mm/0.50 μm, He, 3. K/min; Tstart: 60. C; Tend: 260. C
CapillaryDB-Wax1449.Choi and Sawamura, 200060. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryCarbowax 20M1446.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 μm, H2, 50. C @ 1. min, 3. K/min, 200. C @ 20. min

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-11115.Alizadeh and Shaabani, 201230. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryOptima-51116.Al-Qudah, Muhaidat, et al., 201230. m/0.25 mm/0.25 μm, Helium, 60. C @ 1. min, 3. K/min; Tend: 246. C
CapillaryHP-5 MS1114.Jian-Yu, Zhu, et al., 201230. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 3. min
CapillaryHP-51102.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C
CapillaryHP-51103.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C
CapillaryHP-51103.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C
CapillaryHP-51112.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C
CapillaryHP-51112.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C
CapillaryHP-51112.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C
CapillaryHP-5 MS1148.Kadri, Zarai, et al., 201130. m/0.25 mm/0.25 μm, Helium, 35. C @ 3. min, 5. K/min, 250. C @ 10. min
CapillaryMethylsiloxane + 5 % Ph-groups1089.Nadim, Malik, et al., 201130. m/0.25 mm/0.25 μm, Helium, 60. C @ 2. min, 7. K/min, 230. C @ 20. min
CapillaryZB-51082.Vazques, Aimar, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen, 40. C @ 5. min, 5. K/min; Tend: 200. C
CapillaryZB-51082.Vazquez, Demmel, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen, 40. C @ 5. min, 5. K/min, 200. C @ 5. min
CapillaryHP-51114.Abderrahim, Belhamel, et al., 201030. m/0.25 mm/0.25 μm, Hydrogen, 50. C @ 5. min, 5. K/min, 250. C @ 5. min
CapillaryHP-5 MS1121.Radulovic, Blagojevic, et al., 201030. m/0.25 mm/0.25 μm, Helium, 5. K/min, 290. C @ 10. min; Tstart: 70. C
CapillaryHP-5MS1124.Zouari, Zouari, et al., 201030. m/0.25 mm/0.25 μm, Helium, 50. C @ 1. min, 7. K/min, 250. C @ 5. min
CapillaryDB-51112.El-Massry, El-Ghorab, et al., 200930. m/0.25 mm/0.25 μm, Helium, 3. K/min, 220. C @ 40. min; Tstart: 35. C
CapillaryDB-51102.Kazemi and Akhavani, 200950. m/0.20 mm/0.32 μm, Nitrogen, 60. C @ 3. min, 5. K/min; Tend: 220. C
CapillaryDB-51114.Kazemi and Akhavani, 200950. m/0.20 mm/0.32 μm, Nitrogen, 60. C @ 3. min, 5. K/min; Tend: 220. C
CapillaryRTX-11093.Museli, Pau, et al., 200960. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryRTX-11103.Museli, Pau, et al., 200960. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
Capillary5 % Phenyl methyl siloxane1113.Retta, Gattuso, et al., 200960. m/0.25 mm/0.25 μm, Helium, 3. K/min, 225. C @ 3. min; Tstart: 90. C
CapillaryUltra 21099.Byun and Shin, 200850. m/0.20 mm/0.11 μm, Helium, 60. C @ 5. min, 2. K/min, 230. C @ 30. min
CapillarySLB-5 MS1119.Lo Presti, Sciarrone, et al., 200830. m/0.25 mm/0.25 μm, Helium, 50. C @ 2. min, 3. K/min, 250. C @ 10. min
CapillaryHP-5 MS1114.Adams, Beauchamp, et al., 200730. m/0.25 mm/0.25 μm, Helium, 50. C @ 10. min, 3. K/min, 230. C @ 10. min
CapillaryHP-5MS1114.Bozin B., Mlmica-Dukic N., et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDBP-51089.Heravi and Sereshti, 200725. m/0.25 mm/0.22 μm, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 10. min
CapillaryRTX-5 MS1119.Hudaib and Aburjai, 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 45. C; Tend: 210. C
CapillarySPB-11096.Pinto, Salgueiro, et al., 200730. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryDB-51114.Sefidkon, Abbasi, et al., 200730. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDBP-51089.Sereshti and Samadi, 200725. m/0.25 mm/0.22 μm, Helium, 40. C @ 1. min, 3. K/min, 250. C @ 10. min
CapillaryHP-5 MS1114.Vagionas, Graikou, et al., 200730. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1114.Bozin, Mimicá-Dukic, et al., 200630. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1117.Ebrahim Sajjadi and Mehregan, 200630. m/0.25 mm/0.25 μm, 4. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51119.Figuérédo, Cabassu, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 5. K/min, 300. C @ 5. min
CapillaryHP-11097.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.33 μm, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryMethyl Silicone1099.Kitchlu, Bakshi, et al., 200625. m/0.25 mm/0.25 μm, He, 90. C @ 2. min, 7. K/min; Tend: 220. C
CapillaryNB-301100.Orav, Raal, et al., 200630. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-51114.Pino, Marbot, et al., 200630. m/0.25 mm/0.25 μm, Hydrogen, 70. C @ 4. min, 4. K/min; Tend: 280. C
CapillaryDB-51113.Sefidkon and Jamzad, 200630. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 40. C; Tend: 240. C
CapillaryHP-5MS1111.Basta, Tzakou, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51108.Chagonda and Chalchat, 200550. m/0.3 mm/0.25 μm, 2. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-51114.Ferretti, Maggi, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 3. min, 4. K/min, 30. C @ 15. min
CapillaryDB-51110.Khayyat and Karimi, 2005He, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 60. C; Tend: 240. C
CapillaryHP-5MS1118.Sajjadi and Ghannadi, 200530. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 275. C
CapillaryDB-51113.Sefidkon and Jamzad, 2005He, 4. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 240. C
CapillaryHP-5MS1117.Slavkovska, Couladis, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51100.Tzakou and Constantinidis, 200530. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-5MS1116.Mimica-Dukic, Bozin, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryNB-301098.Raal, Paaver, et al., 200450. m/0.20 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-51114.Rohloff, Mordal, et al., 200430. m/0.25 mm/0.25 μm, He, 2.5 K/min, 220. C @ 6. min; Tstart: 35. C
CapillaryHP-51123.Shafi, Nambiar, et al., 200425. m/0.2 mm/0.5 μm, N2, 3. K/min; Tstart: 30. C; Tend: 280. C
CapillaryDB-51108.Cabanillas, Lopez, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryRSL-2001115.Jirovetz, Buchbauer, et al., 200330. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-51111.Juteau, Jerkovic, et al., 200350. m/0.2 mm/0.25 μm, He, 50. C @ 2. min, 3. K/min, 220. C @ 10. min
CapillaryHP-51114.Mookdasanit, Tamura, et al., 2003Helium, 2. K/min, 210. C @ 60. min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C
CapillaryDB-51114.Pino, Marbot, et al., 200330. m/0.25 mm/0.25 μm, H2, 60. C @ 10. min, 4. K/min, 280. C @ 40. min
CapillaryHP-51102.Pitarokili, Tzakou, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51114.Velickovic, Randjelovic, et al., 200325. m/0.32 mm/0.53 μm, H2, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillaryHP-51115.Velickovic, Randjelovic, et al., 200325. m/0.32 mm/0.53 μm, H2, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillaryHP-51102.Velickovic, Ristic, et al., 200325. m/0.32 mm/0.53 μm, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillaryHP-51102.Velickovic, Ristic, et al., 200325. m/0.32 mm/0.53 μm, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillaryHP-51103.Velickovic, Ristic, et al., 200325. m/0.32 mm/0.53 μm, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillaryHP-51114.Velickovic, Randjelovic, et al., 200230. m/0.25 mm/0.25 μm, H2, 4. K/min; Tstart: 40. C; Tend: 280. C
CapillarySPB-11091.Chiasson, Bélanger, et al., 200130. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 40. C; Tend: 240. C
CapillarySPB-11094.Chiasson, Bélanger, et al., 200130. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 40. C; Tend: 240. C
CapillaryHP-51116.Gallori, Flamini, et al., 200130. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryOV-1011094.Orav and Kann, 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 50. C; Tend: 250. C
CapillaryDB-51114.Santos-Gomes and Fernandes-Ferreira, 200130. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 285. C
CapillaryPTE-51114.Stojanovic, Palic, et al., 200160. m/0.32 mm/0.3 μm, H2, 4.3 K/min; Tstart: 60. C; Tend: 285. C
CapillaryDB-51114.Simic, Andjelkovic, et al., 200060. m/0.25 mm/0.30 μm, Hydrogen or helium (He2 wrote in original paper), 4.3 K/min; Tstart: 60. C; Tend: 285. C
CapillaryOV-11086.Bicchi, Binello, et al., 199925. m/0.32 mm/0.30 μm, Hydrogen, 50. C @ 1. min, 3. K/min, 200. C @ 10. min
CapillaryHP-51123.Collin, Deslauriers, et al., 19932. K/min; Tstart: 40. C; Tend: 210. C
CapillaryHP-51124.Collin, Deslauriers, et al., 19932. K/min; Tstart: 40. C; Tend: 210. C
CapillaryCP Sil 5 CB1100.Kaul, Singh, et al., 19935. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 280. C
CapillaryDB-11095.Perry, Baxter, et al., 198610. m/0.25 mm/0.25 μm, H2, 5. K/min; Tstart: 50. C; Tend: 250. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-11081.Albano, Lima, et al., 201230. m/0.25 mm/0.25 μm, Hydrogen; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
CapillaryHP-5 MS1115.Sharopov, Sulaimonova, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
CapillaryPolydimethyl siloxane with 5 % Ph groups1106.da Silva, de Souza, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0C
CapillaryPolydimethyl siloxane with 5 % Ph groups1117.da Silva, de Souza, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0C
CapillaryHP-51102.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen; Program: not specified
CapillaryHP-51114.Velickovic, Ristic, et al., 201225. m/0.32 mm/0.52 μm, Hydrogen; Program: not specified
CapillaryZB-51081.Vazques, Aimar, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen; Program: not specified
CapillaryZB-51081.Vazquez, Demmel, et al., 201130. m/0.25 mm/0.25 μm, Nitrogen; Program: not specified
CapillaryHP-5 MS1115.Mancini, Arnold, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
CapillarySLB-5 MS1118.Costa, De Fina, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 3 0C/min -> 250 0C (1 min) 10 0C/min -> 300 0C (5 min)
CapillarySLB-5 MS1112.Costa, De Fina, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillarySLB-5 MS1117.Lo Presti, Sciarrone, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryBP-51116.Hashemi, Abolghasemi, et al., 200730. m/0.32 mm/0.25 μm, He; Program: 60C => 4C/min => 150C => 10C/min => 220C
CapillaryBPX-51124.Salamci, Kordali, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 50C => 3C/min => 150C(10min) => 10C/min => 250C
CapillaryHP-5MS1115.Formisano C., Senatore F., et al., 200630. m/0.25 mm/0.25 μm, He; Program: 40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C
CapillaryHP-51158.Jordan, Martinez, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
CapillaryCP Sil 8 CB1114.Judzentiene and Buzelyte, 200650. m/0.32 mm/0.25 μm, He; Program: 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)
CapillaryHP-5MS1115.Senatore, Apostolides Arnold, et al., 200630. m/0.25 mm/0.25 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillarySE-521114.Tognolini, Barocelli, et al., 200630. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)
CapillaryBPX-51114.Judzentiene and Mockute, 200530. m/0.25 mm/0.25 μm; Program: 60C(0.2min) => 3K/min => 186C => 10C/min => 240C (5min)
Capillary 1090.El-Shazily, Hafez, et al., 2004Program: not specified
CapillaryOV-11086.El-Shazly and Hussein, 2004He; Column length: 15. m; Column diameter: 0.317 mm; Program: 50C(4min) => 4C/min => 90C => 10C/min => 300C(10min)
CapillaryCP Sil 8 CB1114.Judpentienë and Mockutë, 200450. m/0.32 mm/0.25 μm, He; Program: 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)
CapillaryHP-51115.Senatore, Apostolides Arnold, et al., 200430. m/0.25 mm/0.25 μm; Program: 40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C
CapillaryHP-51158.Sotomayor, Martínez, et al., 200430. m/0.25 mm/0.25 μm, He; Program: 60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
CapillarySE-301102.Vinogradov, 2004Program: not specified
CapillaryHP-51158.Jordán, Martínez, et al., 200330. m/0.25 mm/0.25 μm, He; Program: 60C (4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
CapillaryCP Sil 8 CB1114.Mockute, Nivinskiene, et al., 200350. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 5C/min => 160C => 10C/min => 250C(5min)
CapillaryHP-51106.Usubillaga, Aparicio, et al., 200130. m/0.25 mm/0.25 μm, He; Program: 50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C
CapillaryDB-11081.Baratta, Dorman, et al., 199830. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 240C (10min)
CapillaryCP Sil 5 CB1100.Weyerstahl, Marschall, et al., 1997N2; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryPolydimethyl siloxanes1102.Zenkevich, 1997Program: not specified
CapillaryMethyl Silicone1098.Grundschober, 1991Program: not specified
CapillaryOV-1011096.De Pooter, Vermeesch, et al., 1989Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryRTX-Wax1422.Museli, Pau, et al., 200960. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillarySupelcowax-101442.Pinto, Salgueiro, et al., 200730. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryFFAP1450.Kitchlu, Bakshi, et al., 200620. m/0.25 mm/0.25 μm, He, 6. K/min; Tstart: 90. C; Tend: 250. C
CapillaryNB-20M1438.Orav, Raal, et al., 200630. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-Innowax1452.Ferretti, Maggi, et al., 200530. m/0.25 mm/0.17 μm, He, 60. C @ 3. min, 4. K/min, 210. C @ 15. min
CapillaryDB-Wax1448.Choi, 200460. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1447.Choi, 2004, 260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySW-101409.Raal, Paaver, et al., 200450. m/0.20 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 230. C
CapillarySupelcowax-101444.Cabanillas, Lopez, et al., 200330. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-20M1425.Juteau, Jerkovic, et al., 200350. m/0.2 mm/0.2 μm, He, 70. C @ 4. min, 4. K/min, 180. C @ 10. min
CapillaryInnowax1451.Suleimenov, Atazharova, et al., 2003He, 60. C @ 10. min, 4. K/min, 220. C @ 10. min; Column length: 60. m; Column diameter: 0.25 mm
CapillarySupelcowax1399.Chiasson, Bélanger, et al., 200130. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 40. C; Tend: 240. C
CapillarySupelcowax1400.Chiasson, Bélanger, et al., 200130. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 40. C; Tend: 240. C
CapillaryPEG-20M1435.Orav and Kann, 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 70. C; Tend: 220. C
CapillaryDB-Wax1436.Umano, Hagi, et al., 200060. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 2. K/min; Tend: 200. C
CapillaryCW 20M1421.Bicchi, Binello, et al., 199925. m/0.32 mm/0.25 μm, Hydrogen, 50. C @ 1. min, 3. K/min, 220. C @ 10. min
CapillarySupelcowax-101440.Collin, Deslauriers, et al., 199340. C @ 2. min, 2. K/min, 210. C @ 120. min
CapillarySupelcowax-101441.Collin, Deslauriers, et al., 199340. C @ 2. min, 2. K/min, 210. C @ 120. min
CapillaryDB-Wax1435.Perry, Baxter, et al., 198630. m/0.25 mm/0.25 μm, H2, 5. K/min; Tstart: 50. C; Tend: 250. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryInnowax FSC1451.Baser, Demirci, et al., 200960. m/0.25 mm/0.25 μm, Helium; Program: 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C
CapillaryHP Innowax1451.Mancini, Arnold, et al., 200950. m/0.20 mm/0.25 μm, Helium; Program: 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
CapillaryCarbowax 20M1439.Hudaib and Aburjai, 200730. m/0.25 mm/0.25 μm, He; Program: not specified
CapillaryHP-Innowax1451.Senatore, Apostolides Arnold, et al., 200650. m/0.2 mm/0.2 μm, He; Program: 40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C
CapillaryHP-Innowax FSC1451.Suleimenov Y.M., Atazhanova G.A., et al., 200660. m/0.25 mm/0.25 μm, He; Program: 60(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax FSC1451.Tabanca, Demirci, et al., 200660. m/0.25 mm/0.25 μm, N2; Program: 60C(10min) => 4C/min => 220C => (10min) => 1C/min => 240C
CapillaryHP-Innowax FSC1451.Demirci, Demirci, et al., 200560. m/0.25 mm/0.25 μm, N2; Program: 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C
CapillaryHP-Innowax FSC1451.Demirci, Paper, et al., 200460. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax1451.Senatore, Apostolides Arnold, et al., 200450. m/0.2 mm/0.2 μm; Program: not specified
CapillaryCarbowax 20M1435.Vinogradov, 2004Program: not specified
CapillaryInnowax FSC1451.Baser, Demirci, et al., 200360. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C
CapillaryHP-Innowax FSC1451.Demirci, Baser, et al., 200360. m/0.25 mm/0.25 μm, He; Program: 60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C
CapillaryInnowax1451.Tunaher, Kirimer, et al., 200360. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C (20min)
CapillaryHP-Innowax1451.Viljoen, van Vuuren, et al., 200360. m/0.25 mm/0.25 μm; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax1451.Baser, Demirci, et al., 200260. m/0.25 mm/0.25 μm, He; Program: 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
CapillaryHP-Innowax FSC1451.Hüsnü Can Baser, Demirci, et al., 200260. m/0.25 mm/0.25 μm, N2; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryInnowax FSC1457.Tunalier, Kirimer, et al., 200260. m/0.25 mm/0.25 μm; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax1451.Baser, Demirci, et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C
CapillaryHP-Innowax1451.Gören, Demirci, et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
CapillaryInnowax FSC1451.Tabanca N., Demirci F., et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax1451.Tabanca, Kirimer, et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryNB-3511460.Kerrola, Galambosi, et al., 199425. m/0.32 mm/0.2 μm; Program: 40C(5min) => 4C/min => 170C => 8C/min => 240C (12min)
CapillaryPolyethylene Glycol1442.Grundschober, 1991Program: not specified

References

Go To: Top, Phase change data, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Stephenson and Malanowski, 1987
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Notes

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