Resorcinol, 2TMS derivative


Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin NIST Mass Spectrometry Data Center
NIST MS number 352781

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Gas Chromatography

Go To: Top, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51389.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51389.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51390.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1386.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1387.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ht1389.Jaroszynska and Ligor, 200530. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryPE-5ms1378.Jaroszynska and Ligor, 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C
CapillaryDB-51389.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51390.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51388.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 7. K/min; Tstart: 50. C; Tend: 240. C
CapillaryDB-51390.Jaroszynska, 200330. m/0.25 mm/0.25 μm, He, 7. K/min; Tstart: 50. C; Tend: 240. C
PackedOV-11378.Mattsson and Petersson, 1977N2, Supelcoport, 4. K/min; Column length: 2. m; Tstart: 80. C; Tend: 240. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryVF-5MS1376.5Tret'yakov, 200830. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51390.Isidorov, Kotowska, et al., 200530. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 50. C; Tend: 300. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySE-301378.Zimmermann, Lauterbach, et al., 1985Program: not specified

References

Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jaroszynska and Ligor, 2005
Jaroszynska, J.; Ligor, T., The identification of phenolic compounds by a gas chromatographic method on three capillary columns with the same non-polar stationary phase, Anal. Chim. Acta., 2005, 539, 1-2, 11-15, https://doi.org/10.1016/j.aca.2005.03.024 . [all data]

Jaroszynska, 2003
Jaroszynska, J., Isolation of free phenolic compounds from arboreal leaves by use of the Florisil/C18 system, Anal. Bioanal. Chem., 2003, 377, 4, 702-708, https://doi.org/10.1007/s00216-003-2155-z . [all data]

Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G., Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives, J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546 . [all data]

Tret'yakov, 2008
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2008. [all data]

Isidorov, Kotowska, et al., 2005
Isidorov, V.A.; Kotowska, U.; Vinogorova, V.T., GC Identification of organic compounds based on partition coefficients of their TMS derivatives in a hexane-acetonitrile system and retention indices, Anal. Sci., 2005, 21, 12, 1483-1489, https://doi.org/10.2116/analsci.21.1483 . [all data]

Zimmermann, Lauterbach, et al., 1985
Zimmermann, V.; Lauterbach, M.; Jaeger, G., Analytical characterization phenolic compounds obtained from phenosolvan-extracts by use of gas-chromatography with capillary columns, Chem. Tech. (Leipzig), 1985, 37, 11, 476-478. [all data]


Notes

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