Naphthalene, 1,2,3,4,4a,5,6,8a-octahydro-7-methyl-4-methylene-1-(1-methylethyl)-, (1α,4aβ,8aα)-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil PONA GBHP-5DB-5BP-1DB-5
Column length (m) 100.25.30.50.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 140.60.60.60.60.
Tend (C) 230.240.246.220.240.
Heat rate (K/min) 5.4.3.2.3.
Initial hold (min) 10.2.  2.
Final hold (min) 25.  20. 
I 1505.1515.1521.1507.1517.
ReferenceCunicao, Lopes, et al., 2007Dehghan, Solaimanian, et al., 2007Hongratanaworakit and Buchbauer, 2007Lesueur, de Rocca Serra, et al., 2007Martins, Santos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1RTX-1SPB-1HP-5MS
Column length (m) 60.60.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 230.230.230.250.280.
Heat rate (K/min) 2.2.2.5.4.
Initial hold (min)    3.5.
Final hold (min) 30.35.35.15. 
I 1508.1507.1507.1492.1513.
ReferenceMuselli, Rossi, et al., 2007Paolini J., Costa J., et al., 2007Paolini, Muselli, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSDB-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 280.240.280.250.220.
Heat rate (K/min) 4.3.3.3.2.
Initial hold (min) 5.    
Final hold (min)    10.20.
I 1513.1513.1508.1515.1507.
ReferenceSaroglou, Marin, et al., 2007Telascrea, de Araujo, et al., 2007Vagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Blanc, Bradesi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RTX-1HP-5MSDB-5DB-5
Column length (m) 50.60.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.220.220.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.230.280.240.240.
Heat rate (K/min) 2.2.3.3.3.
Initial hold (min)    3.3.
Final hold (min) 20.45. 5.3.
I 1502.1507.1513.1510.1516.
ReferenceBoti, Bighelli, et al., 2006Cavalli, Tomi, et al., 2006Chorianopoulos N., Evergets E., et al., 2006Dob, Dahmane, et al., 2006Dob, Dahmane, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5BP-1HP-5DB-1
Column length (m) 50.30.50.30.30.
Carrier gas HeN2HeHeN2
Substrate      
Column diameter (mm) 0.220.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.220.220.260.220.
Heat rate (K/min) 2.5.2.3.4.
Initial hold (min)  10.   
Final hold (min) 20. 20.  
I 1498.1514.1509.1515.1511.
ReferenceDuquesnoy, Dinh, et al., 2006Flamini, Tebano, et al., 2006Gonny, Cavaleiro, et al., 2006Javidnia K., Miri R., et al., 2006Kuiate, Bessière, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5HP-5MSDB-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.32
Phase thickness (μm) 0.250.250.320.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.250.220.280.280.
Heat rate (K/min) 3.10.5.3.3.
Initial hold (min)  2.3.  
Final hold (min)  10.5.  
I 1510.1524.1513.1484.1503.
ReferenceKukic J., Petrovic S., et al., 2006Liu J.M., Nan P., et al., 2006Masoudi, Esmaeili, et al., 2006Pavlovic, Kovacevic, et al., 2006Pavlovic, Tzakou, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-1SPB-1DB-1HP-5
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.250.250.25
Tstart (C) 70.50.50.60.60.
Tend (C) 220.250.250.240.240.
Heat rate (K/min) 3.5.5.4.4.
Initial hold (min)  3.3.  
Final hold (min) 15.15.15.  
I 1498.1498.1493.1513.1517.
ReferencePinto, Pina-Vaz, et al., 2006Radulovic, Lazarevic, et al., 2006Radulovic, Mananjarasoa, et al., 2006Rezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5MSHP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.250.250.25
Tstart (C) 70.60.60.50.50.
Tend (C) 220.280.300.250.250.
Heat rate (K/min) 3.4.3.5.5.
Initial hold (min)  5. 2.2.
Final hold (min) 15.    
I 1498.1511.1510.1514.1514.
ReferenceSalgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006Silva-Brandão, Solferini, et al., 2006Su, Ho, et al., 2006Su, Ho, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5SPB-1DB-5SE-54
Column length (m) 30.30.30.30.50.
Carrier gas H2HeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.250.27
Tstart (C) 50.40.50.50.50.
Tend (C) 285.300.250.250.300.
Heat rate (K/min) 4.34.5.5.5.
Initial hold (min)  5.3.3. 
Final hold (min)   15.15. 
I 1513.1512.1491.1513.1516.
ReferenceVujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006Boskovic, Radulovic, et al., 2005Boskovic, Radulovic, et al., 2005Brantner, Pfeifhofer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-1CP Sil 5 CBDB-1
Column length (m) 30.30.30.50.25.
Carrier gas N2 HeH2 
Substrate      
Column diameter (mm) 0.250.320.250.220.25
Phase thickness (μm) 0.250.250.250.130.25
Tstart (C) 60.50.40.40.60.
Tend (C) 220.250.260.300.180.
Heat rate (K/min) 5.2.2.4.3.
Initial hold (min) 10.8.5. 10.
Final hold (min)   20.10.10.
I 1514.1496.1530.1497.1514.
ReferenceCelik, Gokturk, et al., 2005Dob, Dahmane, et al., 2005de Feo, Urrunaga Soria, et al., 2005Idzojtic, Kajba, et al., 2005bin Jantan, Yalvema, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5RTX-1
Column length (m) 25.30.30.30.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 75.60.60.60.60.
Tend (C) 210.260.260.260.230.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min) 10.    
Final hold (min) 1.   35.
I 1515.1515.1515.1515.1507.
Referencebin Jantan, Yalvema, et al., 2005, 2Javidnia, Miri, et al., 2005Javidnia, Miri, et al., 2005, 2Javidnia, Miri, et al., 2005, 3Paolini, Costa, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1DB-5SPB-1HP-5MS
Column length (m) 30.30.60.30.30.
Carrier gas N2HeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.20.25
Tstart (C) 50.70.40.70.60.
Tend (C) 200.220.250.220.280.
Heat rate (K/min) 5.3.7.3.3.
Initial hold (min)      
Final hold (min)  15. 15. 
I 1507.1498.1529.1496.1513.
ReferenceTchoumbougnang, Zollo, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Bell, 2004Cavaleiro, Salgueiro, et al., 2004Chorianopoulos, Kalpoutzakis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5MSHP-5HP-5HP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.170.250.250.250.25
Tstart (C) 50.60.40.60.60.
Tend (C) 200.280.250.260.280.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min)  5.  5.
Final hold (min)      
I 1487.1513.1513.1515.1513.
ReferenceFernández-Ocaña, Gómez-Rodríguez, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Isidorov, Krajewska, et al., 2004Javidnia, Miri, et al., 2004Karioti, Hadjipavlou-Litina, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5MSHP-5MSRSL-200BP-1
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeH2N2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.40.50.40.60.
Tend (C) 200.280.300.280.220.
Heat rate (K/min) 5.4.5.6.5.
Initial hold (min)  2.5.5. 
Final hold (min)    5.13.
I 1531.1521.1522.1533.1513.
ReferenceMartinez, Rosa, et al., 2004Mardarowicz, Wianowska, et al., 2004Mumm, Tiemann, et al., 2004Ngassoum, Ousmaila, et al., 2004Raina, Kumar, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5BP-1DB-5MS
Column length (m) 30.25.30.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.220.25
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 50.60.50.60.40.
Tend (C) 290.240.310.220.200.
Heat rate (K/min) 4.3.4.2.4.
Initial hold (min)     5.
Final hold (min)  7. 20.20.
I 1515.1516.1513.1507.1519.
ReferenceReis, Pansarim, et al., 2004Sartoratto, Machado, et al., 2004Singer, Flach, et al., 2004Tam, Thuam, et al., 2004Yu, Kim, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSDB-5BP-1OV-1
Column length (m) 30.30.25.50.25.
Carrier gas HeHeN2HeH2
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.3
Tstart (C) 40.40.75.60.50.
Tend (C) 200.200.210.230.200.
Heat rate (K/min) 4.4.3.2.3.
Initial hold (min) 5.5.10. 1.
Final hold (min) 20.20.1.35.20.
I 1513.1510.1515.1508.1492.
ReferenceYu, Kim, et al., 2004, 2Zheng, Kim, et al., 2004bin Ahmad and bin Jantan, 2003Bianchini, Tomi, et al., 2003Bicchi, Rubiolo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-1SPB-1RTX-1
Column length (m) 30.30.50.30.60.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.20.22
Phase thickness (μm) 0.250.250.330.20.25
Tstart (C) 60.50.60.70.60.
Tend (C) 280.200.250.220.230.
Heat rate (K/min) 3.5.2.3.2.
Initial hold (min)   5.  
Final hold (min)  0.20.15.45.
I 1513.1511.1506.1498.1507.
ReferenceBougatsos, Meyer, et al., 2003Boyom, Assembe, et al., 2003Cavalli, Fernandez, et al., 2003Cavaleiro, Salgueiro, et al., 2003Cavalli, Tomi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-2DB-1DB-1HP-5HP-5
Column length (m) 25.30.30.30.30.
Carrier gas H2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.330.250.250.25 
Tstart (C) 40.40.40.60.25.
Tend (C) 280.250.250.280.150.
Heat rate (K/min) 3.2.2.3.3.
Initial hold (min) 2.5.5. 5.
Final hold (min) 10.20.   
I 1512.1490.1501.1513.1512.
ReferenceCeva-Antunes, Bizzo, et al., 2003de Feo, Bruno, et al., 2003de Feo, Urrunaga Soria, et al., 2003Fokialakis, Melliou, et al., 2003Isidorov, Vinogorova, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSHP-1RTX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.330.25
Tstart (C) 60.60.50.40.45.
Tend (C) 280.280.250.260.250.
Heat rate (K/min) 4.3.3.2.3.
Initial hold (min) 5.  5.6.
Final hold (min)    20. 
I 1513.1513.1513.1514.1519.
ReferenceKarioti, Skaltsa, et al., 2003Ngassapa, Runyoro, et al., 2003Salido, Altarejos, et al., 2003Senatore, Rigano, et al., 2003Shellie, Marriott, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5SPB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.250.250.250.200.25
Tstart (C) 60.60.60.70.50.
Tend (C) 280.280.280.220.280.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.   5.
Final hold (min)    15. 
I 1513.1514.1512.1496.1513.
ReferenceSkaltsa, Demetzos, et al., 2003Tsiri, Kretsi, et al., 2003Tzakou, Couladis, et al., 2003Cavaleiro, Salgueiro, et al., 2002Demetzos, Angelopoulou, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5CP Sil 5 CBRTX-5 MSSE-30
Column length (m) 30.30.50.30.25.
Carrier gas   H2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.150.250.25
Tstart (C) 50.60.40.45.60.
Tend (C) 280.280.300.180.180.
Heat rate (K/min) 3.3.4.2.53.
Initial hold (min) 5.5.3.10.10.
Final hold (min)     10.
I 1513.1512.1514.1513.1509.
ReferenceEconomakis, Skaltsa, et al., 2002Fokialakis, Magiatis, et al., 2002Heinrich, Pfeifhofer, et al., 2002Hudaib, Speroni, et al., 2002bin Jantan, Ayop, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5RTX-5HP-1
Column length (m) 25.30.25.30.24.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm)  0.25 0.250.17
Tstart (C) 70.60.70.45.60.
Tend (C) 275.260.260.300.250.
Heat rate (K/min) 4.4.4.3.4.
Initial hold (min)    6.2.
Final hold (min)    10.20.
I 1513.1513.1513.1520.1501.
ReferenceJavidnia, Miri, et al., 2002Javidnia, Miri, et al., 2002, 2Miri, Ramezani, et al., 2002Mondello, Zappia, et al., 2002Nath, Sarma, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBHP-5HP-5RTX-5 MS
Column length (m) 30.50.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.40.250.500.25
Tstart (C) 60.60.60.60.70.
Tend (C) 280.280.260.280.210.
Heat rate (K/min) 2.3.3.3.4.
Initial hold (min) 10.10.  10.
Final hold (min) 40.60.10. 10.
I 1508.1508.1513.1512.1504.
ReferencePino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Couladis, Baziou, et al., 2001Couladis, Tzakou, et al., 2001Hudaib, Grazia Bellardi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1BP-1HP-5MSHP-5
Column length (m) 30.50.50.30.30.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.250.220.220.250.20
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.220.220.280.180.
Heat rate (K/min) 3.2.2.4.4.
Initial hold (min)    5.8.
Final hold (min)  20.20. 2.
I 1516.1495.1508.1513.1513.
ReferenceNogueira, Bittrich, et al., 2001Rezzi, Bighelli, et al., 2001Rezzi, Cavaleiro, et al., 2001Skaltsa, Mavrommati, et al., 2001Alonzo, Bosco, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5CP Sil 5 CB
Column length (m) 60.30.30.30.50.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.250.250.250.250.13
Tstart (C) 40.50.60.60.40.
Tend (C) 290.280.240.240.300.
Heat rate (K/min) 4.4.3.3.4.
Initial hold (min) 2.5.2.2. 
Final hold (min) 5.   10.
I 1509.1509.1514.1514.1516.
ReferenceBartley and Jacobs, 2000Lazari, Skaltsa, et al., 2000Maia, de Paula, et al., 2000Maia, de Paula, et al., 2000Pfeifhofer, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CBP-1HP-5HP-1CP Sil 5 CB
Column length (m) 30.30.30.60.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.25 
Tstart (C) 50.60.50.50.60.
Tend (C) 280.240.280.250.260.
Heat rate (K/min) 4.4.4.2.55.
Initial hold (min) 5. 5.5. 
Final hold (min)      
I 1514.1506.1512.1510.1512.
ReferenceSkaltsa, Lazari, et al., 2000Zunino, Lopez, et al., 2000Lazari, Skaltsa, et al., 1999Stashenko, Cervantes, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-5HP-5OV-1BP-1
Column length (m) 25.30. 25.50.
Carrier gas   HeH2He
Substrate      
Column diameter (mm) 0.250.250.260.250.22
Phase thickness (μm) 0.30.250.250.30.25
Tstart (C) 50.50.60.50.60.
Tend (C) 200.250.240.200.230.
Heat rate (K/min) 3.3.3.3.2.
Initial hold (min) 1.  1. 
Final hold (min) 20.  20.35.
I 1488.1510.1484.1492.1508.
ReferenceBicchi, Rubiolo, et al., 1998Isidorov, Zenkevich, et al., 1998Oprean, Tamas, et al., 1998Bicchi, Fresia, et al., 1997Mariotti, Costa, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5DB-1Methyl SiliconeDB-1
Column length (m) 50.60.60.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.240.250.20.20
Phase thickness (μm) 0.25 0.250.30.20
Tstart (C) 60.50.50.40.70.
Tend (C) 230.280.250.200.200.
Heat rate (K/min) 2.5.3.52.4.
Initial hold (min)  3.5. 5.
Final hold (min) 35.    
I 1499.1510.1525.1522.1515.
ReferenceMariotti, Tomi, et al., 1997Tzakou, Roussis, et al., 1997Stashenko, Prada, et al., 1996Píry, Príbela, et al., 1995Stashenko, Wiame, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-101DB-5CP Sil 5 CB
Column length (m) 60.50.60.25.
Carrier gas  N2HeN2
Substrate     
Column diameter (mm) 0.320.250.320.22
Phase thickness (μm) 0.5 1. 
Tstart (C) 40.70.40.70.
Tend (C) 290.200.220.295.
Heat rate (K/min) 4.3.3.4.
Initial hold (min) 2.   
Final hold (min) 5.   
I 1508.1526.1536.1483.
ReferenceBartley and Foley, 1994Chung, Eiserich, et al., 1993Le Quere and Latrasse, 1990Montanarella, Bos, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Javidnia K., Miri R., et al., 2006
Javidnia K.; Miri R.; Javidnia A., Constituents of the essential oil of Scabiosa flavida from Iran, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 529-530, https://doi.org/10.1007/s10600-006-0206-3 . [all data]

Kuiate, Bessière, et al., 2006
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Kukic J., Petrovic S., et al., 2006
Kukic J.; Petrovic S.; Pavlovic M.; Couladis M.; Tzakou O.; Niketic M., Composition of essential oil of Stachys alpina L. ssp dinarica Murb., Flavour Fragr. J., 2006, 21, 3, 539-542, https://doi.org/10.1002/ffj.1684 . [all data]

Liu J.M., Nan P., et al., 2006
Liu J.M.; Nan P.; Tsering Q.; Tsering T.; Bai Z.K.; Wang L.; Liu Z.J.; Zhong Y., Volatile constituents of the leaves and flowers of Salvia przewalskii Maxim. from Tibet, Flavour Fragr. J., 2006, 21, 3, 435-438, https://doi.org/10.1002/ffj.1607 . [all data]

Masoudi, Esmaeili, et al., 2006
Masoudi, S.; Esmaeili, A.; Khalilzadeh, M.A.; Rustaiyan, A.; Moazami, N.; Akhgar, M.R.; Varavipoor, M., Volatile constituents of Dorema aucheri Boiss., Seseli libanotis (L.) W. D. Koch var. armeniacum bordz. and Conium maculatum L. three Umbelliferae herbs growing wild in Iran, Flavour Fragr. J., 2006, 21, 5, 801-804, https://doi.org/10.1002/ffj.1722 . [all data]

Pavlovic, Kovacevic, et al., 2006
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Pavlovic, Tzakou, et al., 2006
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Pinto, Pina-Vaz, et al., 2006
Pinto, E.; Pina-Vaz, C.; Salgueiro, L.; Goncalves, M.J.; Costa-de-Oliveira, S.; Cavaleiro, C.; Palmeira, A.; Rodrigues, A.; Martinez-de-Oliveira, J., Antifuncal activity of the essential oil Thymus pulegioides on Candida, Aspergillus and dermatophyte species, Journal of Medical Microbiology, 2006, 55, 10, 1367-1373, https://doi.org/10.1099/jmm.0.46443-0 . [all data]

Radulovic, Lazarevic, et al., 2006
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Radulovic, Mananjarasoa, et al., 2006
Radulovic, N.; Mananjarasoa, E.; Harinantenaina, L.; Yoshinori, A., Essential oil composition of four Croton species from Madagascar and their chemotaxonomy, Biochem. Syst. Ecol., 2006, 34, 8, 648-653, https://doi.org/10.1016/j.bse.2006.02.005 . [all data]

Rezazadeh, Hamedani, et al., 2006
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Salgueiro L.R., Pinto E., et al., 2006
Salgueiro L.R.; Pinto E.; Goncalves M.J.; Costa I.; Palmeira A.; Cavaleiro C.; Pina-Vaz C.; Rodrigues A.G.; Martinez-De-Oliveira J., Antifungal activity of the essential oil of Thymus capitellatus against Candida, Aspergillus and dermatophyte strains, Flavour Fragr. J., 2006, 21, 5, 749-753, https://doi.org/10.1002/ffj.1610 . [all data]

Saroglou, Dorizas, et al., 2006
Saroglou, V.; Dorizas, N.; Kypriotakis, Z.; Skaltsa, H.D., Analysis of the essential oil composition of eight Anthemis species from Greece, J. Chromatogr. A, 2006, 1104, 1-2, 313-322, https://doi.org/10.1016/j.chroma.2005.11.087 . [all data]

Silva-Brandão, Solferini, et al., 2006
Silva-Brandão, K.L.; Solferini, V.N.; Trigo, J.R., Chemical and phylogenetic relationships among Aristolochia L. (Aristolochiaceae) from southeastern Brazil, Biochem. Syst. Ecol., 2006, 34, 4, 291-302, https://doi.org/10.1016/j.bse.2005.10.011 . [all data]

Su, Ho, et al., 2006
Su, Y.C.; Ho, C.L.; Wang, E.I.C., Analysis of leaf essential oils from the indigenous five conifers of Taiwan, Flavour Fragr. J., 2006, 21, 3, 447-452, https://doi.org/10.1002/ffj.1685 . [all data]

Su, Ho, et al., 2006, 2
Su, Y.-C.; Ho, C.-L.; Wang, E.I.-C.; Chang, S.-T., Antifungal activities and chemical compositions of essential oils from leaves of four eucalypts, Taiwan J. For. Sci., 2006, 21, 1, 49-61. [all data]

Vujisic L., Vuckovic I., et al., 2006
Vujisic L.; Vuckovic I.; Tesevic V.; Dokovic D.; Ristic M.S.; Janackovic P.; Milosavljevic S., Comparative examination of the essential oils of Anthemis ruthenica and A-arvensis wild-growing in Serbia, Flavour Fragr. J., 2006, 21, 3, 458-461, https://doi.org/10.1002/ffj.1681 . [all data]

Vundac, Pfeifhofer, et al., 2006
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Boskovic, Radulovic, et al., 2005
Boskovic, Z.; Radulovic, N.; Stojanovic, G., Essential oil composition of four Achillea species from the balkans and its chemotaxonomic significance, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 6, 674-678, https://doi.org/10.1007/s10600-006-0009-6 . [all data]

Brantner, Pfeifhofer, et al., 2005
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Celik, Gokturk, et al., 2005
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Dob, Dahmane, et al., 2005
Dob, T.; Dahmane, D.; Berramdane, T.; Chelghoum, C., Chemical composition of the essential oil of Artemisia campestris L. from Algeria, Pharm. Biol., 2005, 43, 6, 512-514, https://doi.org/10.1080/13880200500220664 . [all data]

de Feo, Urrunaga Soria, et al., 2005
de Feo, V.; Urrunaga Soria, E.; Urrunaga Soria, R.; Pizza, C., Composition and in vitro toxicity of the essential oil of Tagetes terniflora HBK. (Asteraceae), Flavour Fragr. J., 2005, 20, 1, 89-92, https://doi.org/10.1002/ffj.1379 . [all data]

Idzojtic, Kajba, et al., 2005
Idzojtic, M.; Kajba, D.; Franjic, J., Differentiation of F1 hybrids P. nigra J. F. Arnold × P. sylvestris L., P. nigra J. F. Arnold × P. densiflora Siebold et Zucc., P. nigra J. F. Arnold × P. thunbergiana Franco and their parental species by needle volatile composition, Biochem. Syst. Ecol., 2005, 33, 4, 427-439, https://doi.org/10.1016/j.bse.2004.10.008 . [all data]

bin Jantan, Yalvema, et al., 2005
bin Jantan, I.; Yalvema, M.F.; Ahmad, N.W.; Jamal, J.A., Insecticidal activities of the leaf oils of eight Cinnamomum species against Aedes aegypti and Aedes albopictus, Pharm. Biol., 2005, 43, 6, 526-532, https://doi.org/10.1080/13880200500220771 . [all data]

bin Jantan, Yalvema, et al., 2005, 2
bin Jantan, I.; Yalvema, M.F.; Ayop, N.; Ahmad, A.S., Constituents of the essential oils of Cinnamomum sintoc Blume from a mountain forest of Peninsular Malaysia, Flavour Fragr. J., 2005, 20, 6, 601-604, https://doi.org/10.1002/ffj.1495 . [all data]

Javidnia, Miri, et al., 2005
Javidnia, K.; Miri, R.; Mehregan, I.; Sadeghpour, H., Volatile constituents of the essential oil of Nepeta ucrainica L. ssp. kopetdaghensis from Iran, Flavour Fragr. J., 2005, 20, 2, 219-221, https://doi.org/10.1002/ffj.1381 . [all data]

Javidnia, Miri, et al., 2005, 2
Javidnia, K.; Miri, R.; Jamalian, A., Composition of the essential oil of Salvia macrosiphon Boiss. from Iran, Flavour Fragr. J., 2005, 20, 5, 542-543, https://doi.org/10.1002/ffj.1468 . [all data]

Javidnia, Miri, et al., 2005, 3
Javidnia, K.; Miri, R.; Kamalinejad, M.; Edraki, N., Chemical composition of Ferula persica Wild. essential oil from Iran, Flavour Fragr. J., 2005, 20, 6, 605-606, https://doi.org/10.1002/ffj.1496 . [all data]

Paolini, Costa, et al., 2005
Paolini, J.; Costa, J.; Bernardini, A., Analysis of the essential oil from aerial parts of Eupatorium cannabinum subsp. corsicum (L.) by gas chromatography with electron impact and chemical ionization mass spectrometry, J. Chromatogr. A, 2005, 1076, 1-2, 170-178, https://doi.org/10.1016/j.chroma.2005.03.131 . [all data]

Tchoumbougnang, Zollo, et al., 2005
Tchoumbougnang, F.; Zollo, P.H.A.; Boyom, F.F.; Nyegue, M.A.; Bessière, J.M.; Menut, C., Aromatic plants of tropical Central Africa. XLVIII. Comparative study of the essential oils of four Hyptis species from Cameroon: H. lanceolata Poit., H. pectinata (L.) Poit., H. spicigera Lam. and H. suaveolens Poit., Flavour Fragr. J., 2005, 20, 3, 340-343, https://doi.org/10.1002/ffj.1441 . [all data]

Antunes, Sevinate-Pinto, et al., 2004
Antunes, T.; Sevinate-Pinto, I.; Barroso, J.G.; Cavaleiro, C.; Salgueiro, L.R., Micromorphology of trichomes and composition of essential oil of Teucrium capitatum, Flavour Fragr. J., 2004, 19, 4, 336-340, https://doi.org/10.1002/ffj.1310 . [all data]

Bell, 2004
Bell, W.A.-M., Examination of Aroma Volatiles Formed from Thermal Processing of Florida Reconstituted Grapefruit Juice. A Thesis presented to the graduate school of the university of Florida in partial fulfillment of the requirements for the degree of master of science, 2004. [all data]

Cavaleiro, Salgueiro, et al., 2004
Cavaleiro, C.; Salgueiro, L.R.; Miguel, M.G.; da Cunha, A.P., Analysis by gas chromatography?mass spectrometry of the volatile components of Teucrium lusitanicum and Teucrium algarbiensis, J. Chromatogr. A, 2004, 1033, 1, 187-190, https://doi.org/10.1016/j.chroma.2004.01.005 . [all data]

Chorianopoulos, Kalpoutzakis, et al., 2004
Chorianopoulos, N.; Kalpoutzakis, E.; Aligiannis, N.; Mitaku, S.; Nychas, G.-J.; Haroutounian, S.A., Essential oils of Satureja, Origanum, and Thymus species: chemical composition and antibacterial activities against foodborne pathogens, J. Agric. Food Chem., 2004, 52, 26, 8261-8267, https://doi.org/10.1021/jf049113i . [all data]

Fernández-Ocaña, Gómez-Rodríguez, et al., 2004
Fernández-Ocaña, A.M.; Gómez-Rodríguez, M.V.; Velasco-Negueruela, A.; Camacho-Simarro, A.M.; Fernández-López, C.; Altarejos, J., In vivo antifungal activity of the essential oil of Bupleurum gibraltarium against plasmopara halstedii in sunflower, J. Agric. Food Chem., 2004, 52, 21, 6414-6417, https://doi.org/10.1021/jf040219n . [all data]

Grujic-Jovanovic, Skaltsa, et al., 2004
Grujic-Jovanovic, S.; Skaltsa, H.D.; Marin, P.; Sokovic, M., Composition and antibacterial activity of the essential oil of six Stachys species from Serbia, Flavour Fragr. J., 2004, 19, 2, 139-144, https://doi.org/10.1002/ffj.1275 . [all data]

Isidorov, Krajewska, et al., 2004
Isidorov, V.A.; Krajewska, U.; Vinogorova, V.T.; Vetchinnikova, L.V.; Fuksman, I.L.; Bal, K., Gas chromatographic analysis of essential oil from buds of different birch species with preliminary partition of components, Biochem. Syst. Ecol., 2004, 32, 1, 1-13, https://doi.org/10.1016/S0305-1978(03)00175-3 . [all data]

Javidnia, Miri, et al., 2004
Javidnia, K.; Miri, R.; Jafari, A.; Rezai, H., Analysis of the volatile constituents of Nepeta macrosiphon Boiss. grown in Iran, Flavour Fragr. J., 2004, 19, 2, 156-158, https://doi.org/10.1002/ffj.1287 . [all data]

Karioti, Hadjipavlou-Litina, et al., 2004
Karioti, A.; Hadjipavlou-Litina, D.; Mensah, M.L.K.; Fleischer, T.C.; Skaltsa, H., Composition and antioxidant activity of the essential oils of Xylopia aethiopica (Dun) A. Rich. (Annonaceae) leaves, stem bark, root bark, and fresh and dried fruits, growing in Ghana, J. Agric. Food Chem., 2004, 52, 26, 8094-8098, https://doi.org/10.1021/jf040150j . [all data]

Martinez, Rosa, et al., 2004
Martinez, J.; Rosa, P.T.V.; Menut, C.; Leydet, A.; Brat, P.; Pallet, D.; Meireles, M.A.A., Valorization of Brazilian vetiver (Vetiveria zizanioides (L.) Nash ex Small) oil, J. Agric. Food Chem., 2004, 52, 21, 6578-6584, https://doi.org/10.1021/jf049182x . [all data]

Mardarowicz, Wianowska, et al., 2004
Mardarowicz, M.; Wianowska, D.; Dawidowicz, A.L.; Sawicki, R., The influence of sample treatment on SPME extracts from conifers. I. Comparison of terpene composition in Engelmann Spruce (Picea engelmanii) using hydrodistillation, SPME and PLE, Annales Universitatis Mariae Curie-Sklodowska Lublin - Polonia, 2004, 59, 3, 25-42. [all data]

Mumm, Tiemann, et al., 2004
Mumm, R.; Tiemann, T.; Schulz, S.; Hilker, M., Analysis of volatiles from black pine (Pinus nigra): significance of wounding and egg deposition by a herbivorous sawfly, Phytochemistry, 2004, 65, 24, 3221-3230, https://doi.org/10.1016/j.phytochem.2004.10.010 . [all data]

Ngassoum, Ousmaila, et al., 2004
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Raina, Kumar, et al., 2004
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Notes

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