17-Norkaur-15-ene, 13-methyl-, (8β,13β)-
- Formula: C20H32
- Molecular weight: 272.4681
- IUPAC Standard InChI: InChI=1S/C20H32/c1-17(2)8-5-9-19(4)15(17)7-11-20-13-12-18(3,14-20)10-6-16(19)20/h12-13,15-16H,5-11,14H2,1-4H3
- IUPAC Standard InChIKey: GXMKKDDGINQVBE-UHFFFAOYSA-N
- CAS Registry Number: 3564-54-3
- Chemical structure:
This structure is also available as a 2d Mol file - Species with the same structure:
- Stereoisomers:
- Other names: 17-Nor-8β,13β-kaur-15-ene, 13-methyl-; (+)-Beyerene; (+)-Hibaene; (+)-Stachene; ent-Beyer-15-ene; Beyerene; Hibaene, (+)-; Stachen; Stachene; Stachene, (+)-; Stach-15-ene, (+)-; Hibaene
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Mass spectrum (electron ionization)
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Spectrum
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Additional Data
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| Owner | NIST Mass Spectrometry Data Center Collection (C) 2014 copyright by the U.S. Secretary of Commerce on behalf of the United States of America. All rights reserved. |
|---|---|
| Origin | A. MCCORMICK GC-MS UNIT, CHEM. DEPT., UNIVERSITY OF GLASGOW |
| NIST MS number | 13168 |
Gas Chromatography
Go To: Top, Mass spectrum (electron ionization), References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | OV-101 | 170. | 1913. | Clarke, Perry, et al., 1994 | |
| Capillary | SE-30 | 170. | 1913. | Perry and Weavers, 1984 | |
| Capillary | SE-30 | 190. | 1941. | Perry and Weavers, 1984 |
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-54 | 1924. | Adams, 2000 | 30. m/0.26 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 246. C |
Kovats' RI, polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | Carbowax 20M | 170. | 2200. | Perry and Weavers, 1984 | |
| Capillary | Carbowax 20M | 190. | 2241. | Perry and Weavers, 1984 |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-1 | 1951. | Sing, Smadja, et al., 1992 | 50. m/0.32 mm/1.05 μm, He; Program: 20C(0.5min) => 60C => 4C/min => 250C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5MS | 1962. | Marongiu, Porcedda, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 3. K/min, 240. C @ 30. min; Tstart: 60. C |
References
Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Clarke, Perry, et al., 1994
Clarke, D.B.; Perry, N.B.; Weavers, R.T.,
Foliage Oil Terpenes of Prumnopitys ferruginea (D. Don) Laubenf. Variation in Acorenone Levels,
J. Essnt. Oil Res., 1994, 6, 6, 549-554, https://doi.org/10.1080/10412905.1994.9699344
. [all data]
Perry and Weavers, 1984
Perry, N.B.; Weavers, R.T.,
Kovats indices of diterpene hydrocarbons on fused-silica capillary columns,
J. Chromatogr., 1984, 284, 478-481, https://doi.org/10.1016/S0021-9673(01)87850-X
. [all data]
Adams, 2000
Adams, R.P.,
Systematics of the one seeded Juniperus of the eastern hemisphere based on leaf essential oils and random amplified polymorphic DNAs (RAPDs),
Biochem. Syst. Ecol., 2000, 28, 6, 529-543, https://doi.org/10.1016/S0305-1978(99)00096-4
. [all data]
Sing, Smadja, et al., 1992
Sing, A.S.C.; Smadja, J.; Brevard, H.; Maignial, L.; Chaintreau, A.; Marion, J.-P.,
Volatile constituents of faham (Jumellea fragrans (Thou.) Schltr.),
J. Agric. Food Chem., 1992, 40, 4, 642-646, https://doi.org/10.1021/jf00016a024
. [all data]
Marongiu, Porcedda, et al., 2001
Marongiu, B.; Porcedda, S.; Porta, G.D.; Reverchon, E.,
Extraction and isolation of Salvia desoleana and Mentha spicata subsp. insularis essential oils by supercritical CO2,
Flavour Fragr. J., 2001, 16, 5, 384-388, https://doi.org/10.1002/ffj.1021
. [all data]
Notes
Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, References
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