trans-Linalool oxide (furanoid)


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5SPB-1HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.50.60.60.
Tend (C) 200.250.250.280.260.
Heat rate (K/min) 4.4.5.4.5.
Initial hold (min) 1.4.3.5. 
Final hold (min) 10.10.15.  
I 1086.1092.1102.1065.1075.
ReferenceCho, Namgung, et al., 2008Quijano, Salamanca, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007Sabulal, Dan, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBDB-5SPB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.50.50.
Tend (C) 240.200.220.250.250.
Heat rate (K/min) 3.5.3.5.5.
Initial hold (min)    3.3.
Final hold (min)    15.15.
I 1088.1068.1087.1100.1090.
ReferenceTelascrea, de Araujo, et al., 2007Andrianoelisoa H.S., Menut C., et al., 2006Bastos, Ishimoto, et al., 2006Blagojevic, Radulovic, et al., 2006Blagojevic, Radulovic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5DB-1HP-1DB-1
Column length (m) 50.30.30.25.25.
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.250.320.250.20.2
Phase thickness (μm) 0.250.250.250.330.33
Tstart (C) 60.60.50.60.50.
Tend (C) 220.240.220.300.300.
Heat rate (K/min) 2.3.4.5.4.
Initial hold (min)  3. 3. 
Final hold (min) 20.5. 30. 
I 1070.1093.1080.1070.1092.
ReferenceBousmaha, Boti, et al., 2006Dob, Dahmane, et al., 2006Kuiate, Bessière, et al., 2006Nath, Baruah, et al., 2006Osorio, Alarcon, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1HP-5MSDB-5DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 50.70.60.50.50.
Tend (C) 265.220.280.250.200.
Heat rate (K/min) 2.53.4.5.5.
Initial hold (min)   5.2. 
Final hold (min)  15.   
I 1071.1070.1087.1073.1083.
ReferenceRamezani, Behravan, et al., 2006Salgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006Su, Ho, et al., 2006Agnaniet, Makani, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-1DB-1DB-5HP-5
Column length (m) 50.30.25.25.30.
Carrier gas H2N2 N2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.270.250.250.250.25
Tstart (C) 50.50.60.75.60.
Tend (C) 300.260.180.210.260.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min)  3.10.10. 
Final hold (min)  5.10.1. 
I 1074.1071.1071.1071.1071.
ReferenceBrantner, Pfeifhofer, et al., 2005Dob, Berramdane, et al., 2005bin Jantan, Yalvema, et al., 2005bin Jantan, Yalvema, et al., 2005, 2Javidnia, Miri, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSPB-1HP-1HP-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.170.250.25
Tstart (C) 60.70.50.50.60.
Tend (C) 280.220.200.290.260.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min)      
Final hold (min)  15.   
I 1069.1066.1064.1091.1072.
ReferenceAligiannis, Kalpoutzakis, et al., 2004Antunes, Sevinate-Pinto, et al., 2004Fernández-Ocaña, Gómez-Rodríguez, et al., 2004Flach A., Dondon R.C., et al., 2004Javidnia, Miri, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5SPB-1RSL-200SPB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (μm)  0.250.20.250.25
Tstart (C) 60.60.70.40.60.
Tend (C) 260.260.220.280.250.
Heat rate (K/min) 3.3.3.6.4.
Initial hold (min)    5.2.
Final hold (min)   15.5.20.
I 1070.1074.1070.1087.1089.
ReferenceJavidnia, Miri, et al., 2004, 2Javidnia, Miri, et al., 2004, 3Moldão-Martins, Beirão-da-Costa, et al., 2004Ngassoum, Ousmaila, et al., 2004Pino, Marbot, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5HP-5MSBP-1DB-5
Column length (m) 30.30.30.50.25.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.320.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.75.
Tend (C) 220.290.250.220.210.
Heat rate (K/min) 5.4.3.2.3.
Initial hold (min)     10.
Final hold (min) 13.  20.1.
I 1072.1083.1088.1070.1090.
ReferenceRaina, Kumar, et al., 2004Reis, Pansarim, et al., 2004Salido, Valenzuela, et al., 2004Tam, Thuam, et al., 2004bin Ahmad and bin Jantan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSCP Sil 5 CBSPB-5
Column length (m) 30.25.60.60.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 75.60.40.60.60.
Tend (C) 230.260.310.280.250.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min) 10. 1.10.2.
Final hold (min)   20.60.20.
I 1088.1072.1091.1056.1088.
Referencebin Jantan, Yassin, et al., 2003Javidnia, Miri, et al., 2003Lalel, Singh, et al., 2003Pino, Almora, et al., 2003Pino, Marbot, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Mega 5MSDB-5DB-5RTX-5CP Sil 5 CB
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.70.60.45.60.
Tend (C) 240.275.260.300.280.
Heat rate (K/min) 3.4.4.3.2.
Initial hold (min) 2.  6.10.
Final hold (min)    10.40.
I 1094.1075.1074.1088.1055.
ReferenceVerzera, Trozzi, et al., 2003Javidnia, Miri, et al., 2002Javidnia, Miri, et al., 2002, 2Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1HP-5RTX-5RTX-5
Column length (m) 50.50.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.220.250.250.25
Phase thickness (μm) 0.40.250.250.250.25
Tstart (C) 60.60.60.45.45.
Tend (C) 280.220.280.250.250.
Heat rate (K/min) 3.2.3.3.3.
Initial hold (min) 10.  6.6.
Final hold (min) 60.20.   
I 1055.1073.1065.1088.1088.
ReferencePino, Marbot, et al., 2002, 2Pintore, Usai, et al., 2002Pitarokili, Couladis, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5MSHP-5SPB-1BP-1
Column length (m) 50.30.30.60.50.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.220.250.200.320.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.40.60.
Tend (C) 220.250.180.200.220.
Heat rate (K/min) 2.3.4.4.2.
Initial hold (min)   8.  
Final hold (min)   2.20.20.
I 1072.1088.1088.1054.1076.
ReferenceLota, Serra, et al., 2001Salido, Altarejos, et al., 2001Alonzo, Bosco, et al., 2000Chen, Huang, et al., 1998Tam, An, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Methyl SiliconeDB-1HP-101OV-101
Column length (m) 30.25.60.50.50.
Carrier gas H2HeHeN2N2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm)  0.30.25  
Tstart (C) 60.40.70.70.80.
Tend (C) 220.200.250.200.200.
Heat rate (K/min) 2.2.2.53.2.
Initial hold (min) 3. 5.  
Final hold (min)   15.  
I 1082.1080.1082.1089.1076.
ReferenceSakho, Chassagne, et al., 1997Píry, Príbela, et al., 1995Combariza, Tirado, et al., 1994Chung, Eiserich, et al., 1993Yang, Sugisawa, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-101RSL-150
Column length (m) 50.30.
Carrier gas N2He
Substrate   
Column diameter (mm) 0.250.53
Phase thickness (μm)  1.2
Tstart (C) 80.30.
Tend (C) 200.220.
Heat rate (K/min) 2.3.
Initial hold (min)   
Final hold (min)   
I 1076.1061.
ReferenceYang, Sugisawa, et al., 1992Sagrero-Nieves, de Pooter, et al., 1989
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Salido, Valenzuela, et al., 2004
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Notes

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