trans-Linalool oxide (furanoid)


Van Den Dool and Kratz RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxBP-20DB-WaxDB-WaxDB-Wax
Column length (m) 30.50.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.40.40.50.
Tend (C) 200.220.200.200.220.
Heat rate (K/min) 4.2.4.4.4.
Initial hold (min) 1. 1.1.4.
Final hold (min) 10.20.10.10.20.
I 1484.1467.1483.1484.1455.
ReferenceCho, Namgung, et al., 2008Bousmaha, Boti, et al., 2006Cho, Choi, et al., 2006Cho, Choi, et al., 2006Osorio, Alarcon, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10ZB-WaxOV-351DB-WaxCarbowax 20M
Column length (m) 30.30.50.60.60.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (μm) 0.20.250.20.250.25
Tstart (C) 70.50.60.70.45.
Tend (C) 220.220.220.230.250.
Heat rate (K/min) 3.4.5.2.2.
Initial hold (min)  1. 2.0.17
Final hold (min) 15.10. 20. 
I 1466.1443.1450.1478.1450.
ReferenceSalgueiro L.R., Pinto E., et al., 2006Ugliano, Bartowsky, et al., 2006Bonvehí, 2005Choi, 2005Verzera, Campisi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-WaxDB-Wax EtrBP-20DB-WaxDB-Wax
Column length (m) 30.30.50.30.60.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.220.320.25
Phase thickness (μm) 0.150.250.250.50.25
Tstart (C) 35.40.60.40.70.
Tend (C) 220.245.220.245.230.
Heat rate (K/min) 1.83.2.3.2.
Initial hold (min) 10.3. 3.2.
Final hold (min) 10.20.20.20.20.
I 1427.1429.1461.1438.1478.
ReferenceLedauphin, Saint-Clair, et al., 2004Ménager, Jost, et al., 2004Tam, Thuam, et al., 2004Aubert, Ambid, et al., 2003Choi, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-WaxRTX-WaxSupelcowax-10AT-WaxBP-20
Column length (m) 60.30.30.60.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.250.250.320.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 65.45.50.65.60.
Tend (C) 250.250.230.250.220.
Heat rate (K/min) 2.3.3.2.2.
Initial hold (min) 10.6. 10. 
Final hold (min) 60.10.30.60.20.
I 1425.1451.1437.1425.1469.
ReferencePino, Almora, et al., 2003Mondello, Zappia, et al., 2002Moreira, Trugo, et al., 2002Pino, Marbot, et al., 2002Pintore, Usai, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxRTX-WaxBP-20DB-WaxCP-Wax 52CB
Column length (m) 30.30.50.30.60.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.220.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 45.45.60.35.45.
Tend (C) 250.250.220.220.250.
Heat rate (K/min) 3.3.2.4.2.
Initial hold (min) 6.6. 0.50.17
Final hold (min)      
I 1460.1460.1464.1443.51450.
ReferenceShellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002Lota, Serra, et al., 2001Pet'ka, Mocák, et al., 2001Verzera, Campisi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxDB-WaxCarbowax 20M
Column length (m) 30.30.60.60.60.
Carrier gas He N2HeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (μm) 0.50.50.250.250.425
Tstart (C) 60.60.70.50.45.
Tend (C) 245.245.230.230.300.
Heat rate (K/min) 3.3.2.3.3.
Initial hold (min) 3.3.2. 3.
Final hold (min) 20.20.20. 20.
I 1439.1446.1482.1448.1460.
ReferenceWirth, Guo, et al., 2001Bureau, Razungles, et al., 2000Choi and Sawamura, 2000Shimoda, Wu, et al., 1996Mondello, Dugo, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxDB-WaxHP-20MHP-FFAP
Column length (m) 50.60.60.50.50.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.25  
Tstart (C) 30.50.50.60.60.
Tend (C) 170.230.150.190.210.
Heat rate (K/min) 4.2.2.3.3.
Initial hold (min) 2. 10.  
Final hold (min) 20. 20.  
I 1450.1432.1451.1449.1449.
ReferencePíry, Príbela, et al., 1995Shimoda, Shigematsu, et al., 1995Combariza, Tirado, et al., 1994Chung, Eiserich, et al., 1993Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxCarbowax 20MCarbowax 20M
Column length (m) 30.30.30.25.25.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.250.310.31
Phase thickness (μm)  0.250.25  
Tstart (C) 40.50.50.50.50.
Tend (C) 200.220.240.200.200.
Heat rate (K/min) 2.4.4.2.2.
Initial hold (min) 10.3.3.  
Final hold (min)  20.   
I 1461.1465.1461.1451.1460.
ReferenceUmano, Hagi, et al., 1992Humpf and Schreier, 1991Krammer, Winterhalter, et al., 1991Suárez and Duque, 1991Suárez and Duque, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 30.30.30.60.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.25  
Tstart (C) 50.50.40.50.50.
Tend (C) 250.250.240.225.200.
Heat rate (K/min) 4.4.4.1.52.
Initial hold (min) 3.3.3. 5.
Final hold (min)    80.40.
I 1459.1461.1461.1464.1457.
ReferenceFröhlich, Duque, et al., 1989Fröhlich, Duque, et al., 1989Schwab, Mahr, et al., 1989Chen and Ho, 1988Chen, Kuo, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Cho, Namgung, et al., 2008
Cho, I.H.; Namgung, H.-J.; Choi, H.-K.; Kim, Y.-S., Volatiles and key odorants in the pileus and stipe of pine-mushroom (Tricholoma matsutake Sing.), Food Chem., 2008, 106, 1, 71-76, https://doi.org/10.1016/j.foodchem.2007.05.047 . [all data]

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Ugliano, Bartowsky, et al., 2006
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Ledauphin, Saint-Clair, et al., 2004
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Ménager, Jost, et al., 2004
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Aubert, Ambid, et al., 2003
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Choi, 2003
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Pino, Almora, et al., 2003
Pino, J.; Almora, K.; Marbot, R., Volatile components of papaya (Carica papaya L., maradol variety) fruit, Flavour Fragr. J., 2003, 18, 6, 492-496, https://doi.org/10.1002/ffj.1248 . [all data]

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Pino, Marbot, et al., 2002
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Suárez and Duque, 1991
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Fröhlich, Duque, et al., 1989
Fröhlich, O.; Duque, C.; Schreier, P., Volatile constituents of curuba (Passiflora mollissima) fruit, J. Agric. Food Chem., 1989, 37, 2, 421-425, https://doi.org/10.1021/jf00086a033 . [all data]

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Chen and Ho, 1988
Chen, C.-C.; Ho, C.-T., Gas chromatographic analysis of volatile components of ginger oil (Zingiber officinale Roscoe) extracted with liquid carbon dioxide, J. Agric. Food Chem., 1988, 36, 2, 322-328, https://doi.org/10.1021/jf00080a020 . [all data]

Chen, Kuo, et al., 1986
Chen, C.-C.; Kuo, M.-C.; Liu, S.-E.; Wu, C.-M., Volatile components of salted and pickled prunes (Prunus mume Sieb. et Zucc.), J. Agric. Food Chem., 1986, 34, 1, 140-144, https://doi.org/10.1021/jf00067a038 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References