1-Octen-3-ol

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5MSDB-5MSHP-5DB-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.40.40.
Tend (C) 230.200.200.250.200.
Heat rate (K/min) 2.4.4.5.4.
Initial hold (min)  1.1.1.1.
Final hold (min) 30.10.10.10.10.
I 959.983.983.977.1002.
ReferenceBendahou, Muselli, et al., 2008Cho, Namgung, et al., 2008Cho, Namgung, et al., 2008Benzo, Gilardoni, et al., 2007Cho I.H., Lee S.M., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5MSDB-5MSDB-5DB-5
Column length (m) 60.30.30.30.60.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (μm) 1.0.250.250.51.
Tstart (C) 40.35.35.40.40.
Tend (C) 230.225.225.265.260.
Heat rate (K/min) 3.10.10.7.4.
Initial hold (min) 2.5.5. 2.
Final hold (min) 10.25.25.5.10.
I 979.992.1012.981.980.
ReferenceEngel and Ratel, 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Drake M., et al., 2007Mahattanatawee K., Perez-Cacho P.R., et al., 2007Methven L., Tsoukka M., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101HP-5MSDB-5DB-5HP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.320.320.25
Phase thickness (μm) 0.20.250.250.250.25
Tstart (C) 70.60.40.40.60.
Tend (C) 200.280.250.250.280.
Heat rate (K/min) 3.4.5.5.3.
Initial hold (min) 2.5.2.2. 
Final hold (min) 15. 5.5. 
I 963.975.974.976.979.
ReferencePoliteo, Jukic, et al., 2007Saroglou, Arfan, et al., 2007Wu, Zorn, et al., 2007Wu, Zorn, et al., 2007Chorianopoulos N., Evergets E., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5HP-5DB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.50.60.
Tend (C) 200.240.220.220.280.
Heat rate (K/min) 4.3.5.4.3.
Initial hold (min) 1.3.10.  
Final hold (min) 10.5.   
I 1002.978.981.971.976.
ReferenceCho, Kim, et al., 2006Dob, Dahmane, et al., 2006Flamini, Tebano, et al., 2006Kuiate, Bessière, et al., 2006Kukic J., Petrovic S., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1DB-1HP-5HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Tstart (C) 60.70.60.60.60.
Tend (C) 250.220.240.240.280.
Heat rate (K/min) 10.3.4.4.4.
Initial hold (min) 2.   5.
Final hold (min) 10.15.   
I 981.959.982.978.978.
ReferenceLiu J.M., Nan P., et al., 2006Pinto, Pina-Vaz, et al., 2006Rezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006Saroglou, Dorizas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5HP-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeH2HeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.40.80.50.
Tend (C) 250.285.300.300.200.
Heat rate (K/min) 5.4.34.4.5.
Initial hold (min) 2. 5.  
Final hold (min)      
I 979.968.980.984.965.
ReferenceSu, Ho, et al., 2006Vujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006Zhao C.X., Li, et al., 2006Agnaniet, Makani, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54CP-Sil 8CB-MS5 % Phenyl methyl siloxaneHP-5HP-5
Column length (m) 50.0.30.30.30.
Carrier gas H2HeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.270.251.0.250.25
Tstart (C) 50.40.40.60.60.
Tend (C) 300.280.250.220.260.
Heat rate (K/min) 5.4.7.5.3.
Initial hold (min)  2.10.10. 
Final hold (min)  5.5.  
I 976.983.999.982.975.
ReferenceBrantner, Pfeifhofer, et al., 2005Elmore, Cooper, et al., 2005Estevez, Ventanas, et al., 2005Flamini, Luigi Cioni, et al., 2005Javidnia, Miri, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5HP-5DB-1
Column length (m) 30.25.25.25.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.20.20.20.25
Phase thickness (μm) 0.251.1.1.0.25
Tstart (C) 60.40.40.40.50.
Tend (C) 250.280.280.280.200.
Heat rate (K/min) 4.5.5.5.5.
Initial hold (min) 2.    
Final hold (min) 20.5.5.5. 
I 978.984.984.984.969.
ReferencePino, Mesa, et al., 2005Solina, Baumgartner, et al., 2005Solina, Baumgartner, et al., 2005Solina, Baumgartner, et al., 2005Tchoumbougnang, Zollo, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSPB-1HP-5SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.320.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.2
Tstart (C) 40.60.70.60.70.
Tend (C) 250.280.220.220.220.
Heat rate (K/min) 5.3.3.5.3.
Initial hold (min) 2.  10. 
Final hold (min) 5. 15. 15.
I 973.978.959.984.959.
ReferenceWu, Zorn, et al., 2005Aligiannis, Kalpoutzakis, et al., 2004Antunes, Sevinate-Pinto, et al., 2004Bertoli, Menichini, et al., 2004Cavaleiro, Salgueiro, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5MSCP-Sil 8CB-MSHP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeN2He He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.60.40.60.
Tend (C) 280.220.280.280.260.
Heat rate (K/min) 3.5.4.4.3.
Initial hold (min)  10.5.2. 
Final hold (min)    5. 
I 979.980.977.980.975.
ReferenceChorianopoulos, Kalpoutzakis, et al., 2004Flamini, Luigi Cioni, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Hierro, de la Hoz, et al., 2004Javidnia, Miri, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1RSL-200Methyl SiliconeSPB-5HP-5
Column length (m) 30.30.50.30.25.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.20.320.250.250.2
Phase thickness (μm) 0.20.25 0.250.33
Tstart (C) 70.40.50.60.60.
Tend (C) 220.280.240.250.240.
Heat rate (K/min) 3.6.3.4.3.
Initial hold (min)  5. 2. 
Final hold (min) 15.5. 20.7.
I 959.976.988.978.978.
ReferenceMoldão-Martins, Beirão-da-Costa, et al., 2004Ngassoum, Ousmaila, et al., 2004Özcan and Chalchat, 2004Pino, Marbot, et al., 2004Sartoratto, Machado, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP-Sil 8CB-MSHP-5HP-5DB-1
Column length (m) 30.60.30.30.30.
Carrier gas He N2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.40.
Tend (C) 240.280.220.220.250.
Heat rate (K/min) 3.4.5.5.2.
Initial hold (min)  2.10.10.5.
Final hold (min) 30.5.  20.
I 980.986.980.980.964.
ReferenceBader, Caponi, et al., 2003Bruna, Hierro, et al., 2003Dural, Bagci, et al., 2003Emilio Tomei, Manganelli, et al., 2003de Feo, Bruno, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.5 0.25
Tstart (C) 60.60.40.60.60.
Tend (C) 240.220.265.260.280.
Heat rate (K/min) 3.5.7.4.3.
Initial hold (min)  10.   
Final hold (min)   5.  
I 981.980.980.980.978.
ReferenceFlamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Högnadóttir and Rouseff, 2003Javidnia, Miri, et al., 2003Ngassapa, Runyoro, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5BPX-5SPB-1
Column length (m) 30.30.30.50.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.320.20
Phase thickness (μm) 0.250.251.0.50.20
Tstart (C) 50.60.50.60.70.
Tend (C) 250.280.200.250.220.
Heat rate (K/min) 3.4.2.54.3.
Initial hold (min)  5. 5. 
Final hold (min)    20.15.
I 980.977.977.3993.959.
ReferenceSalido, Altarejos, et al., 2003Skaltsa, Demetzos, et al., 2003Xu, van Stee, et al., 2003Bredie, Mottram, et al., 2002Cavaleiro, Salgueiro, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBDB-5CP Sil 8 CBDB-5
Column length (m) 60.60.30.60.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.50.40.60.
Tend (C) 250.250.280.280.240.
Heat rate (K/min) 4.4.3.4.3.
Initial hold (min) 8.8.5.2. 
Final hold (min) 10.10.   
I 986.991.978.983.980.
ReferenceDuckham, Dodson, et al., 2002Duckham, Dodson, et al., 2002Economakis, Skaltsa, et al., 2002Elmore, Campo, et al., 2002Flamini, Cioni, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSDB-5DB-1RTX-5RTX-5
Column length (m) 30.25.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 45.70.60.45.45.
Tend (C) 180.275.220.250.250.
Heat rate (K/min) 2.54.2.3.3.
Initial hold (min) 10.  6.6.
Final hold (min)   20.  
I 984.978.960.986.988.
ReferenceHudaib, Speroni, et al., 2002Javidnia, Miri, et al., 2002Pintore, Usai, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5CP-Sil 8CB-MSHP-1HP-5
Column length (m) 30.30.60.60.50.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.50.50.
Tend (C) 280.280.280.250.250.
Heat rate (K/min) 3.3.4.2.52.5
Initial hold (min) 5.5.2.5.5.
Final hold (min)      
I 980.980.986.967.978.
ReferenceAligiannis, Kalpoutzakis, et al., 2001Aligiannis, Kalpoutzakis, et al., 2001, 2Bruna, Hierro, et al., 2001Guilliard, Delgado, et al., 2001Guilliard, Delgado, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5BPX-5BPX-5CP Sil 5 CB
Column length (m) 60.30.50.50.50.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.320.250.320.320.32
Phase thickness (μm) 1.0.250.250.250.4
Tstart (C) 40.60.35.35.60.
Tend (C) 220.240.250.250.280.
Heat rate (K/min) 2.3.4.4.3.
Initial hold (min) 5. 3.3.10.
Final hold (min)   10.10.60.
I 964.992.980.987.964.
ReferenceKim, 2001Nogueira, Bittrich, et al., 2001Oruna-Concha, Duckham, et al., 2001Oruna-Concha, Duckham, et al., 2001Pino and Marbot, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP Sil 8 CBBP-5HP-5HP-101
Column length (m) 30.60.50.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.2
Phase thickness (μm) 0.250.251.0.250.2
Tstart (C) 60.40.40.40.70.
Tend (C) 280.280.190.200.200.
Heat rate (K/min) 4.4.2.2.3.
Initial hold (min) 5.2.5.5.2.
Final hold (min)    20.10.
I 977.983.985.981.979.
ReferenceSkaltsa, Mavrommati, et al., 2001Elmore, Mottram, et al., 2000Escudero, Cacho, et al., 2000Kim, Thuy, et al., 2000Milos and Radonic, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101DB-5DB-5DB-5DB-1
Column length (m) 25.30.30.30.60.
Carrier gas HeH2H2H2N2
Substrate      
Column diameter (mm) 0.20.320.320.320.25
Phase thickness (μm) 0.21.1.1.1.
Tstart (C) 70.40.40.40.30.
Tend (C) 200.210.210.210.200.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min) 2.    
Final hold (min) 10.   30.
I 980.980.982.985.965.
ReferenceMilos and Radonic, 2000Moio, Piombino, et al., 2000Moio, Piombino, et al., 2000Moio, Piombino, et al., 2000Wu, Wang, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BPX-5BPX-5BPX-5OV-1
Column length (m) 30.50.50.50.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.250.250.500.3
Tstart (C) 50.50.50.40.50.
Tend (C) 280.250.250.280.200.
Heat rate (K/min) 4.4.4.4.3.
Initial hold (min) 5.5.5. 1.
Final hold (min)  5.5. 20.
I 976.986.987.991.963.
ReferenceLazari, Skaltsa, et al., 1999Mandin, Duckham, et al., 1999Mandin, Duckham, et al., 1999Aaslyng, Elmore, et al., 1998Bicchi, Rubiolo, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-1DB-1
Column length (m) 30.30.30.25.25.
Carrier gas H2H2H2HeHe
Substrate      
Column diameter (mm) 0.320.320.320.20.2
Phase thickness (μm) 1.1.1.0.110.11
Tstart (C) 40.40.40.50.50.
Tend (C) 210.210.210.250.250.
Heat rate (K/min) 3.3.3.5.5.
Initial hold (min)      
Final hold (min)      
I 982.985.985.964.964.
ReferenceMoio and Addeo, 1998Moio and Addeo, 1998Moio and Addeo, 1998Warthen, Lee, et al., 1997Warthen, Lee, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-5DB-5DB-5DB-1
Column length (m) 50.30.30.30.30.
Carrier gas  H2H2H2N2
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.251.1.1.0.25
Tstart (C) 50.40.40.40.150.
Tend (C) 250.220.220.220.280.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)      
Final hold (min)      
I 965.982.983.980.960.
ReferenceMisharina and Golovnya, 1996Moio L., Rillo L., et al., 1996Moio L., Rillo L., et al., 1996Moio L., Rillo L., et al., 1996Coen, Engel, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Methyl SiliconeOV-101HP-101CP Sil 5 CB
Column length (m) 30.25.15.50.25.
Carrier gas N2He N2 
Substrate      
Column diameter (mm) 0.320.20.320.250.22
Phase thickness (μm) 0.250.3   
Tstart (C) 150.40.35.70.70.
Tend (C) 280.200.250.200.205.
Heat rate (K/min) 3.2.6.3.4.
Initial hold (min)   3.  
Final hold (min)      
I 960.970.962.981.962.
ReferenceCoen, Engel, et al., 1995Píry, Príbela, et al., 1995Chisholm, Guiher, et al., 1994Chung, Eiserich, et al., 1993Hendriks and Bruins, 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillary
Active phase OV-101OV-1
Column length (m) 2.5183.
Carrier gas   
Substrate Gas-Chrom Q 
Column diameter (mm)  0.762
Phase thickness (μm)   
Tstart (C) 50.0.
Tend (C) 220.230.
Heat rate (K/min) 2.1.
Initial hold (min)   
Final hold (min)   
I 982.970.
ReferenceNixon, Wong, et al., 1979Schreyen, Dirinck, et al., 1976
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendahou, Muselli, et al., 2008
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Methven L., Tsoukka M., et al., 2007
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References