Vanillyl alcohol, 2TMS derivative
- Formula: C14H26O3Si2
- Molecular weight: 298.5254
- IUPAC Standard InChI: InChI=1S/C14H26O3Si2/c1-15-14-10-12(11-16-18(2,3)4)8-9-13(14)17-19(5,6)7/h8-10H,11H2,1-7H3
- IUPAC Standard InChIKey: ZBFHUPIBELOLII-UHFFFAOYSA-N
- CAS Registry Number: 33740-07-7
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Vanillyl alcohol, bis(trimethylsilyl)- deriv.; Vanillyl alcohol, bis(trimethylsilyl)-; (2-Methoxy-4-([(trimethylsilyl)oxy]methyl)phenoxy)(trimethyl)silane; Benzenemethanol, 4-hydroxy-3-methoxy, bis-TMS; Vanillic alcohol, di-TMS; Vanillic alcohol, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 1633. | Mattsson and Petersson, 1977 | N2, Supelcoport, 4. K/min; Column length: 2. m; Tstart: 80. C; Tend: 240. C |
| Packed | SE-30 | 1632. | Lhuguenot, Maume, et al., 1971 | N2, Gas Chrom P (120-140 mesh), 1. K/min; Column length: 3. m; Tstart: 100. C; Tend: 180. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G.,
Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives,
J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546
. [all data]
Lhuguenot, Maume, et al., 1971
Lhuguenot, J.C.; Maume, B.F.; Baron, C.,
Gas Chromatographic and Mass Spectrometric Study of Vanillin Related Compounds,
Chromatographia, 1971, 4, 5, 204-208, https://doi.org/10.1007/BF02281053
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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