Diethyl dimethylpyrophosphonate
- Formula: C6H16O5P2
- Molecular weight: 230.1358
- IUPAC Standard InChI: InChI=1S/C6H16O5P2/c1-5-9-12(3,7)11-13(4,8)10-6-2/h5-6H2,1-4H3
- IUPAC Standard InChIKey: YCQJGVYQCXLCBH-UHFFFAOYSA-N
- CAS Registry Number: 32288-17-8
- Chemical structure:
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | OV-1 | 1340. | Kostiainen, 2000 | 15. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 10. K/min, 280. C @ 10. min |
| Capillary | DB-1 | 1340. | D'agostino, Provost, et al., 1987 | 15. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 10. K/min, 280. C @ 10. min |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1340. | Savel'eva, Zenkevich, et al., 2003 | 25. m/0.20 mm/0.33 μm, Helium, 40. C @ 1. min, 5. K/min, 270. C @ 15. min |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Kostiainen, 2000
Kostiainen, O.,
Gas Chromatography in Screening of Chemicals Related to the Chemical Weapons Convention
in Encyclopedia of Analytical Chemistry, Meyers, R.A., ed(s)., John Wiley Sons Ltd, Chichester, 2000, 963-979. [all data]
D'agostino, Provost, et al., 1987
D'agostino, P.A.; Provost, L.R.; Visentini, J.,
Analysis of O-Ethyl S-[2-(Diisopropylamino)ethyl] Methylphosphonothiolate (VX) by Capillary Column Gas Chromatography-Mass Spectrometry,
J. Chromatogr., 1987, 402, 221-232, https://doi.org/10.1016/0021-9673(87)80020-1
. [all data]
Savel'eva, Zenkevich, et al., 2003
Savel'eva, E.I.; Zenkevich, I.G.; Radilov, A.S.,
Identification the Products of Chemical Neutralization of O-Isobutyl-S-(2-diethylaminoethyl)methylthiophosphonate in the Composition of Bitumen-Salt Matrices,
Zh. Anal. Khim. (Rus.), 2003, 58, 2, 135-145. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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