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«beta»-D-Glucopyranose, 5TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryCarbowax 20M160.1972.Martinez-Castro, Paez, et al., 1989Chrompack; Column length: 25. m; Column diameter: 0.22 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryVF-5MS1971.3Tretyakov, 201130. m/0.25 mm/0.25 «mu»m, He; Tstart: 60. C; Tend: 270. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51931.Isidorov, Lech, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min, 300. C @ 30. min; Tstart: 50. C
CapillaryHP-51931.Isidorov, Lech, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min, 300. C @ 30. min; Tstart: 50. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-51930.Isidorov, Lech, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified
CapillaryHP-51930.Isidorov, Lech, et al., 200830. m/0.25 mm/0.25 «mu»m, Helium; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Martinez-Castro, Paez, et al., 1989
Martinez-Castro, I.; Paez, M.I.; Sanz, J.; Garcia-Raso, A., Gas Chromatographic Behaviour of Carbohydrate Trimethylsilyl Ethers. II. Aldohexoses, J. Chromatogr., 1989, 462, 49-60, https://doi.org/10.1016/S0021-9673(00)91335-9 . [all data]

Tretyakov, 2011
Tretyakov, K.V., Retention Data (March 2011). NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2011. [all data]

Isidorov, Lech, et al., 2008
Isidorov, V.A.; Lech, P.; Zolciak, A.; Rusak, N.; Szczepaniak, L., Gas Chromatographic - nass spectrometric investigation of metabolites from the needles and roots of pine seedlings at early stages of pathogenic fungi Armillaria ostoyae attack, Trees, 2008, 22, 4, 531-542, https://doi.org/10.1007/s00468-008-0213-z . [all data]


Notes

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