Phloretic acid, 2TMS derivative

• Formula: C₁₅H₂₆O₃Si₂
• Molecular weight: 310.5361
• IUPAC Standard InChI: InChI=1S/C15H26O3Si2/c1-19(2,3)17-14-10-7-13(8-11-14)9-12-15(16)18-20(4,5)6/h7-8,10-11H,9,12H2,1-6H3 Copy

  
• IUPAC Standard InChIKey: NTWRBVRZYOLGDK-UHFFFAOYSA-N Copy
• CAS Registry Number: 27750-62-5
• Chemical structure:
  This structure is also available as a 2d Mol file
• Other names: Hydrocinnamic acid, p-(trimethylsiloxy)-, trimethylsilyl ester; Trimethylsilyl 3-(4-[(trimethylsilyl)oxy]phenyl)propanoate; 3-(4-Hydroxyphenyl)propionic acid, (2TMS); 3-(4-Hydroxyphenyl)propionic acid, trimethylsilyl ether, trimethylsilyl ester; 4-Hydroxyhydrocinnamic acid, bis-TMS; 4-Hydroxyphenylpropionic acid, di-TMS; Benzenepropanoic acid, 4-hydroxy, bis-TMS; Benzenepropanoic acid, 4-hydroxy, (2TMS); Propanoic acid, 3-(4-hydroxyphenyl), bis-TMS; 3-(4-Hydroxyphenyl)propionic acid, TMS; Benzenepropanoic acid, 4-trimethylsilyloxy, trimethylsilyl ester; Benzenepropanoic acid, 4-hydroxy, TMS; 4-Hydroxyhydrocinnamic acid, TMS; 4-Hydroxyphenylpropionic acid, TMS
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• Information on this page:
  • Gas Chromatography
  • References
  • Notes
• Other data available:
  • Mass spectrum (electron ionization)
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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Normal alkane RI, non-polar column, temperature ramp

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References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kraus and Spiteller, 1997
Kraus, C.; Spiteller, G., Comparison of phenolic compounds from galls and shoots of Picea glauca, Phytochemistry, 1997, 44, 1, 59-67, https://doi.org/10.1016/S0031-9422(96)00388-3 . [all data]

Isidorov and Vinogorova, 2003
Isidorov, V.A.; Vinogorova, V.T., GC-MS analysis of compounds extracted from buds of Populus balsamifera and Populus nigra, Z. Naturforsch. C:, 2003, 58, 355-360. [all data]

Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G., Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives, J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546 . [all data]

Butts, 1972
Butts, W.C., Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds, Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3 . [all data]

Tret'yakov, 2008
Tret'yakov, K.V., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2008. [all data]

Lee, Yanamandra, et al., 2002
Lee, B.Y.; Yanamandra, K.; Thurmon, T.F., Quantitative estimation of organic analytes with a capillary column, Am. Clin. Lab., 2002, May, 30-34. [all data]

Notes

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• Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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