Homoveratric acid, TMS derivative
- Formula: C13H20O4Si
- Molecular weight: 268.3810
- IUPAC Standard InChI: InChI=1S/C13H20O4Si/c1-15-11-7-6-10(8-12(11)16-2)9-13(14)17-18(3,4)5/h6-8H,9H2,1-5H3
- IUPAC Standard InChIKey: ZOTLJAZLFPDMSU-UHFFFAOYSA-N
- CAS Registry Number: 27750-60-3
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Benzeneacetic acid, 3,4-dimethoxy-, trimethylsilyl ester; Acetic acid, (3,4-dimethoxyphenyl)-, trimethylsilyl ester; Homoveratric acid, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 1725. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | DB-5 | 1729. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | DB-5 | 1729. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | DB-5 | 1729. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | PE-5ht | 1725. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | PE-5ht | 1725. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | PE-5ht | 1726. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | PE-5ht | 1727. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.1 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | PE-5ms | 1712. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | PE-5ms | 1712. | Jaroszynska and Ligor, 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 320. C |
| Capillary | DB-5 | 1727. | Jaroszynska, 2003 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C |
| Capillary | DB-5 | 1729. | Jaroszynska, 2003 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 240. C |
| Capillary | DB-5 | 1727. | Jaroszynska, 2003 | 30. m/0.25 mm/0.25 μm, He, 7. K/min; Tstart: 50. C; Tend: 240. C |
| Capillary | DB-5 | 1729. | Jaroszynska, 2003 | 30. m/0.25 mm/0.25 μm, He, 7. K/min; Tstart: 50. C; Tend: 240. C |
| Packed | OV-1 | 1682. | Butts, 1972 | He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Jaroszynska and Ligor, 2005
Jaroszynska, J.; Ligor, T.,
The identification of phenolic compounds by a gas chromatographic method on three capillary columns with the same non-polar stationary phase,
Anal. Chim. Acta., 2005, 539, 1-2, 11-15, https://doi.org/10.1016/j.aca.2005.03.024
. [all data]
Jaroszynska, 2003
Jaroszynska, J.,
Isolation of free phenolic compounds from arboreal leaves by use of the Florisil/C18 system,
Anal. Bioanal. Chem., 2003, 377, 4, 702-708, https://doi.org/10.1007/s00216-003-2155-z
. [all data]
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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