β-Sitosterol, TMS derivative

Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Mass spectrum
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Additional Data

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Owner NIST Mass Spectrometry Data Center
Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
Origin John Halket,Royal Holloway, University of London, UK
NIST MS number 331677

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-5 Sil MS3344.Lytovchenko, Beleggia, et al., 200930. m/0.25 mm/0.25 μm, Helium, 70. C @ 5. min, 5. K/min, 310. C @ 1. min
CapillaryHP-53348.Isidorov, Lech, et al., 200830. m/0.25 mm/0.25 μm, Helium, 3. K/min, 300. C @ 30. min; Tstart: 50. C
CapillaryDB-5MS3296.Rogge, Medeiros, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 6. K/min, 300. C @ 15. min

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryRTx-5 Sil MS3356.Birkemeier and Kopka, 200730. m/0.25 mm/0.25 μm, Helium; Program: 70 0C (1 min) 1 0C/min -> 76 0C 6.09 0C/min -> 350 0C (1 min) -> 330 0C (10 min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lytovchenko, Beleggia, et al., 2009
Lytovchenko, A.; Beleggia, R.; Schauer, N.; Isaacson, T.; Leuendorf, J.E.; Hellmann, H.; Rose, J.K.C.; Fernie, A.R., Application of GC-MS fpr the detection of lipophilic compounds in diverse plant tissues, Plant Methods, 2009, 5, 4, 1-11. [all data]

Isidorov, Lech, et al., 2008
Isidorov, V.A.; Lech, P.; Zolciak, A.; Rusak, N.; Szczepaniak, L., Gas Chromatographic - nass spectrometric investigation of metabolites from the needles and roots of pine seedlings at early stages of pathogenic fungi Armillaria ostoyae attack, Trees, 2008, 22, 4, 531-542, https://doi.org/10.1007/s00468-008-0213-z . [all data]

Rogge, Medeiros, et al., 2006
Rogge, W.F.; Medeiros, P.M.; Simoneit, B.R.T., Organic marker compounds for surface soil and fugitive dust from open lot dairies and cattle feedlots, Atmos. Environ., 2006, 40, 1, 27-49, https://doi.org/10.1016/j.atmosenv.2005.07.076 . [all data]

Birkemeier and Kopka, 2007
Birkemeier, C.; Kopka, J., Design of metabolite recovery by variations of the metabolite profiling protocol in Concepts in Plant Metabolomics, Nikolau, B.J.; Wurtele, E.S., ed(s)., Springer, Dordrecht, Netheralnds, 2007, 45-69. [all data]

Notes

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