3,3-Dimethylacrylic acid, TMS derivative
- Formula: C8H16O2Si
- Molecular weight: 172.2969
- IUPAC Standard InChI: InChI=1S/C8H16O2Si/c1-7(2)6-8(9)10-11(3,4)5/h6H,1-5H3
- IUPAC Standard InChIKey: KNFZPFSOTLGZEE-UHFFFAOYSA-N
- CAS Registry Number: 25436-25-3
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 2-Butenoic acid, 3-methyl-, trimethylsilyl ester; Crotonic acid, 3-methyl-, trimethylsilyl ester; Acrylic acid, 3,3-dimethyl-, trimethylsilyl ester; Trimethylsilyl 3-methyl-2-butenoate; 3-Methyl-2-butenoic acid, trimethylsilyl ester; 3,3-Dimethylacrylic acid, trimethylsilyl ester; Trimethylsilyl 3-methylbut-2-enoate; Trimethylsilyl 3,3-dimethylacrylate
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SE-52 | 1015. | Lefevere, Verhaeghe, et al., 1988 | 25. m/0.20 mm/0.40 μm, He, 5. K/min; Tstart: 50. C; Tend: 270. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 1002.7 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
| Capillary | VF-5MS | 1007.2 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Lefevere, Verhaeghe, et al., 1988
Lefevere, M.F.; Verhaeghe, B.J.; Declerck, D.M.; de Leenheer, A.P.,
Automated profiling of urinary organic acids by dual-column gas chromatography and gas chromatography/mass spectrometry,
Biomed. Environ. Mass Spectrom., 1988, 15, 6, 311-322, https://doi.org/10.1002/bms.1200150603
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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