(1S,2E,6E,10R)-3,7,11,11-Tetramethylbicyclo[8.1.0]undeca-2,6-diene

Formula: C₁₅H₂₄
Molecular weight: 204.3511
IUPAC Standard InChI: InChI=1S/C15H24/c1-11-6-5-7-12(2)10-14-13(9-8-11)15(14,3)4/h6,10,13-14H,5,7-9H2,1-4H3/b11-6+,12-10+
IUPAC Standard InChIKey: VPDZRSSKICPUEY-BFPRWLMKSA-N
CAS Registry Number: 24703-35-3
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Stereoisomers:
Other names: Bicyclo[8.1.0]undeca-2,6-diene, 3,7,11,11-tetramethyl-, (1S,2E,6E,10R)-; Bicyclo[8.1.0]undeca-2,6-diene, 3,7,11,11-tetramethyl-, (E,E)-(1S,10R)-(+)-; Bicyclo[8.1.0]undeca-2,6-diene, 3,7,11,11-tetramethyl-, [1S-(1R*,2E,6E,10S*)]-; (+)-Bicyclogermacrene; Bicyclogermacren; Bicyclogermacrene; β-Cyclogermacrane; Bicylogermacrene
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Other data available:
- Gas Chromatography
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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Equity-5MS	BP-1	BP-1	HP-5	DB-5
Column length (m)	30.	50.	50.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	250.	220.	220.	240.	240.
Heat rate (K/min)	3.	2.	2.	4.	3.
Initial hold (min)				2.
Final hold (min)	10.	20.	20.
I	1496.	1496.	1493.	1501.	1495.
Reference	Belsito E.L., Carbone C., et al., 2007	Boti, Koukoua, et al., 2007	Castilho, Liu, et al., 2007	Dehghan, Solaimanian, et al., 2007	Flamini, Cioni, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	BP-1	Methyl Silicone	RTX-1
Column length (m)	30.	30.	50.	30.	60.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	80.	60.
T_end (C)	220.	280.	220.	220.	230.
Heat rate (K/min)	5.	3.	2.	2.	2.
Initial hold (min)	10.
Final hold (min)			20.	15.	30.
I	1496.	1493.	1483.	1489.	1488.
Reference	Flamini, Tebano, et al., 2007	Kundakovic, Fokialakis, et al., 2007	Lesueur, de Rocca Serra, et al., 2007	Melo, Corrêa, et al., 2007	Muselli, Rossi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	SPB-1	HP-5MS	DB-5
Column length (m)	60.	60.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	230.	230.	250.	280.	200.
Heat rate (K/min)	2.	2.	5.	4.	2.
Initial hold (min)			3.	5.
Final hold (min)	35.	35.	15.		60.
I	1494.	1494.	1477.	1494.	1490.
Reference	Paolini J., Costa J., et al., 2007	Paolini, Muselli, et al., 2007	Radulovic, Lazarevic, et al., 2007	Radulovic, Lazarevic, et al., 2007	Rout, Rao, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5MS	DB-5	SPB-1
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	250.	240.	280.	240.	250.
Heat rate (K/min)	5.	3.	3.	3.	5.
Initial hold (min)				2.	3.
Final hold (min)	10.				15.
I	1501.	1494.	1497.	1497.	1477.
Reference	Sonboli, Azizian, et al., 2007	Telascrea, de Araujo, et al., 2007	Vagionas, Ngassapa, et al., 2007	Batista-Pereira, Fernandes, et al., 2006	Blagojevic, Radulovic, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5	HP-5	HP-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	He	He	N2	N2	He
Substrate
Column diameter (mm)	0.2	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	250.	280.	220.	220.	260.
Heat rate (K/min)	5.	3.	5.	5.	3.
Initial hold (min)	3.		3.	10.
Final hold (min)	15.		5.
I	1491.	1494.	1494.	1496.	1501.
Reference	Blagojevic, Radulovic, et al., 2006	Chorianopoulos N., Evergets E., et al., 2006	Esmaeili, Nematollahi, et al., 2006	Flamini, Tebano, et al., 2006	Javidnia, Miri, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	DB-5	HP-5MS	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	N2	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	50.	60.	60.	60.	60.
T_end (C)	220.	280.	220.	280.	280.
Heat rate (K/min)	4.	3.	5.	3.	3.
Initial hold (min)			3.
Final hold (min)			5.
I	1500.	1499.	1494.	1467.	1484.
Reference	Kuiate, Bessière, et al., 2006	Kukic J., Petrovic S., et al., 2006	Masoudi, Esmaeili, et al., 2006	Pavlovic, Kovacevic, et al., 2006	Pavlovic, Tzakou, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-1	HP-5	OV-1	SPB-1
Column length (m)	30.	30.	25.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.2
T_start (C)	50.	60.	60.	50.	70.
T_end (C)	250.	240.	240.	220.	220.
Heat rate (K/min)	5.	4.	4.	3.	3.
Initial hold (min)	3.			1.
Final hold (min)	15.			5.	15.
I	1478.	1493.	1502.	1495.	1482.
Reference	Radulovic, Mananjarasoa, et al., 2006	Rezazadeh, Hamedani, et al., 2006	Rezazadeh, Hamedani, et al., 2006	Rubiolo P., Matteodo M., et al., 2006	Salgueiro L.R., Pinto E., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	DB-5	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	40.
T_end (C)	280.	300.	250.	285.	300.
Heat rate (K/min)	4.	3.	5.	4.3	4.
Initial hold (min)	5.		2.		5.
Final hold (min)
I	1495.	1493.	1500.	1496.	1494.
Reference	Saroglou, Dorizas, et al., 2006	Silva-Brandão, Solferini, et al., 2006	Su, Ho, et al., 2006	Vujisic L., Vuckovic I., et al., 2006	Vundac, Pfeifhofer, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	SE-54	HP-5	DB-1
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	He	He	H2	N2	N2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.27	0.25	0.25
T_start (C)	50.	50.	50.	60.	50.
T_end (C)	250.	250.	300.	220.	260.
Heat rate (K/min)	5.	5.	5.	5.	2.
Initial hold (min)	3.	3.		10.	3.
Final hold (min)	15.	15.			5.
I	1480.	1497.	1500.	1494.	1494.
Reference	Boskovic, Radulovic, et al., 2005	Boskovic, Radulovic, et al., 2005	Brantner, Pfeifhofer, et al., 2005	Celik, Gokturk, et al., 2005	Dob, Berramdane, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	HP-5	DB-1	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	40.	60.
T_end (C)	250.	220.	220.	250.	260.
Heat rate (K/min)	3.	5.	5.	3.	3.
Initial hold (min)		10.	10.
Final hold (min)	20.			20.
I	1472.	1495.	1497.	1468.	1500.
Reference	Fanciullino, Gancel, et al., 2005	Flamini, Luigi Cioni, et al., 2005	Flamini, Luigi Cioni, et al., 2005, 2	Gancel, Ollitrault, et al., 2005	Javidnia, Miri, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5	DB-1	BP-1	Mega 5MS
Column length (m)	60.	30.	30.	50.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	50.	60.	40.
T_end (C)	230.	260.	200.	230.	240.
Heat rate (K/min)	2.	2.	5.	2.	3.
Initial hold (min)		5.			2.
Final hold (min)	35.	20.		35.
I	1494.	1492.	1495.	1494.	1482.
Reference	Paolini, Costa, et al., 2005	Senatore, Napolitano, et al., 2005	Tchoumbougnang, Zollo, et al., 2005	Vellutini, Baldovini, et al., 2005	Verzera, Trozzi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	SPB-1	HP-5	SPB-1	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.2	0.25
T_start (C)	60.	70.	60.	70.	60.
T_end (C)	280.	220.	220.	220.	220.
Heat rate (K/min)	3.	3.	5.	3.	5.
Initial hold (min)			10.		10.
Final hold (min)		15.		15.
I	1492.	1482.	1495.	1482.	1496.
Reference	Aligiannis, Kalpoutzakis, et al., 2004	Antunes, Sevinate-Pinto, et al., 2004	Bertoli, Menichini, et al., 2004	Cavaleiro, Salgueiro, et al., 2004	Ceccarini, Macchia, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RTX-5	HP-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	45.	60.	60.	60.
T_end (C)	280.	300.	240.	240.	240.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)		6.
Final hold (min)		10.
I	1494.	1500.	1496.	1496.	1496.
Reference	Chorianopoulos, Kalpoutzakis, et al., 2004	Dugo, Mondello, et al., 2004	Flamini, Bader, et al., 2004	Flamini, Cioni, et al., 2004	Flamini, Cioni, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	HP-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	220.	280.	260.	260.	260.
Heat rate (K/min)	5.	4.	3.	3.	3.
Initial hold (min)	10.	5.
Final hold (min)
I	1496.	1494.	1498.	1495.	1495.
Reference	Flamini, Luigi Cioni, et al., 2004	Grujic-Jovanovic, Skaltsa, et al., 2004	Javidnia, Miri, et al., 2004	Javidnia, Miri, et al., 2004, 2	Javidnia, Miri, et al., 2004, 3
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	RSL-200	DB-5	HP-5MS	Optima 5
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.2	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.2	0.25	0.25	0.25	0.25
T_start (C)	70.	40.	50.	60.	60.
T_end (C)	220.	280.	290.	280.	280.
Heat rate (K/min)	3.	6.	4.	3.	3.
Initial hold (min)		5.
Final hold (min)	15.	5.			20.
I	1482.	1508.	1498.	1477.	1484.
Reference	Moldão-Martins, Beirão-da-Costa, et al., 2004	Ngassoum, Ousmaila, et al., 2004	Reis, Pansarim, et al., 2004	Tzakou, Vagias, et al., 2004	Vérité, Nacer, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5MS	DB-5	DB-5	OV-1
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.3
T_start (C)	40.	40.	60.	60.	50.
T_end (C)	200.	200.	240.	240.	200.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)	5.	5.			1.
Final hold (min)	20.	20.	30.		20.
I	1502.	1501.	1495.	1496.	1470.
Reference	Yu, Kim, et al., 2004	Zheng, Kim, et al., 2004	Bader, Caponi, et al., 2003	Bader, Flamini, et al., 2003	Bicchi, Rubiolo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	HP-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	250.	220.	220.	220.	220.
Heat rate (K/min)	3.	5.	5.	5.	5.
Initial hold (min)		10.	10.	10.	10.
Final hold (min)	20.
I	1467.	1496.	1495.	1496.	1496.
Reference	Brat, Rega, et al., 2003	Dural, Bagci, et al., 2003	Ertugrul, Dural, et al., 2003	Flamini, Luigi Cioni, et al., 2003	Flamini, Luigi Cioni, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-1	DB-5	HP-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	220.	280.	250.	260.	280.
Heat rate (K/min)	5.	3.	3.	4.	3.
Initial hold (min)	10.
Final hold (min)			20.
I	1496.	1490.	1468.	1496.	1494.
Reference	Flamini, Luigi Cioni, et al., 2003, 3	Fokialakis, Melliou, et al., 2003	Gancel, Ollitrault, et al., 2003	Javidnia, Miri, et al., 2003	Ngassapa, Runyoro, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-1	RTX-5	HP-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.33	0.25	0.25	0.25	0.25
T_start (C)	40.	45.	60.	60.	60.
T_end (C)	260.	250.	280.	280.	280.
Heat rate (K/min)	2.	3.	4.	3.	3.
Initial hold (min)	5.	6.	5.
Final hold (min)	20.
I	1491.	1500.	1494.	1500.	1500.
Reference	Senatore, Rigano, et al., 2003	Shellie, Marriott, et al., 2003	Skaltsa, Demetzos, et al., 2003	Tsiri, Kretsi, et al., 2003	Tsiri, Kretsi, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Mega 5MS	SPB-1	DB-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.20	0.25	0.25	0.25
T_start (C)	40.	70.	60.	60.	60.
T_end (C)	240.	220.	240.	220.	280.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)	2.			10.	5.
Final hold (min)		15.
I	1482.	1481.	1496.	1496.	1499.
Reference	Verzera, Trozzi, et al., 2003	Cavaleiro, Salgueiro, et al., 2002	Flamini, Cioni, et al., 2002	Flamini, Cioni, et al., 2002, 2	Fokialakis, Magiatis, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-5	HP-5	BP-1	RTX-5
Column length (m)	50.	30.	30.	50.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	45.
T_end (C)	300.	260.	280.	220.	300.
Heat rate (K/min)	4.	4.	3.	2.	3.
Initial hold (min)	3.				6.
Final hold (min)				20.	10.
I	1496.	1495.	1490.	1494.	1502.
Reference	Heinrich, Pfeifhofer, et al., 2002	Javidnia, Miri, et al., 2002	Kovacevic, Pavlovic, et al., 2002	Lota, de Rocca Serra, et al., 2002	Mondello, Zappia, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	SPB-5	HP-5	RTX-5	RTX-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	45.	45.
T_end (C)	280.	250.	280.	250.	250.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)	6.	2.		6.	6.
Final hold (min)		20.
I	1497.	1494.	1464.	1480.	1488.
Reference	Pino, Marbot, et al., 2002	Pino, Marbot, et al., 2002, 2	Pitarokili, Couladis, et al., 2002	Shellie, Mondello, et al., 2002	Shellie, Mondello, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	280.	280.	260.	280.	240.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)	5.	5.		5.
Final hold (min)			10.
I	1492.	1491.	1496.	1494.	1497.
Reference	Aligiannis, Kalpoutzakis, et al., 2001	Aligiannis, Kalpoutzakis, et al., 2001, 2	Couladis, Baziou, et al., 2001	Giamakis, Kretsi, et al., 2001	Nogueira, Bittrich, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	BPX-5	HP-5	HP-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	50.	60.
T_end (C)	280.	180.	200.	280.	240.
Heat rate (K/min)	4.	4.	2.	4.	3.
Initial hold (min)	5.	5.	5.	5.	2.
Final hold (min)		5.	20.
I	1494.	1517.	1489.	1495.	1472.
Reference	Skaltsa, Mavrommati, et al., 2001	Zabaras and Wyllie, 2001	Kim, Thuy, et al., 2000	Lazari, Skaltsa, et al., 2000	Maia, de Paula, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	DB-5	OV-101
Column length (m)	30.	30.	30.	30.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	240.	240.	240.	240.	200.
Heat rate (K/min)	3.	3.	3.	3.	5.
Initial hold (min)	2.	2.	2.	2.
Final hold (min)
I	1474.	1496.	1497.	1497.	1494.
Reference	Maia, de Paula, et al., 2000	Maia, de Paula, et al., 2000	Maia, de Paula, et al., 2000	Maia, de Paula, et al., 2000	Menut, Bessiere, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	Mega 5MS	Mega 5MS	CBP-1	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	70.	40.	40.	60.	50.
T_end (C)	230.	240.	240.	240.	280.
Heat rate (K/min)	2.	3.	3.	4.	4.
Initial hold (min)		2.	2.		5.
Final hold (min)
I	1500.	1482.	1482.	1494.	1493.
Reference	Song, Sawamura, et al., 2000	Verzera, la Rosa, et al., 2000	Verzera, Trozzi, et al., 2000	Zunino, Lopez, et al., 2000	Lazari, Skaltsa, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	HP-1	OV-1	DB-5	OV-1
Column length (m)	25.	60.	25.	30.	25.
Carrier gas	N2	He		H2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.3	0.25	0.3
T_start (C)	50.	50.	50.	60.	50.
T_end (C)	200.	250.	200.	240.	200.
Heat rate (K/min)	5.	2.5	3.	3.	3.
Initial hold (min)		5.	1.		1.
Final hold (min)			20.		20.
I	1496.	1490.	1472.	1496.	1477.
Reference	Menut, Bessiere, et al., 1999	Stashenko, Cervantes, et al., 1999	Bicchi, Rubiolo, et al., 1998	Nogueira, Marsaioli, et al., 1998	Bicchi, Fresia, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary
Active phase	BP-1	Methyl Silicone	DB-5
Column length (m)	50.	25.	60.
Carrier gas	He	He	He
Substrate
Column diameter (mm)	0.22	0.2	0.32
Phase thickness (μm)	0.25	0.3	1.
T_start (C)	60.	40.	40.
T_end (C)	230.	200.	220.
Heat rate (K/min)	2.	2.	3.
Initial hold (min)
Final hold (min)	35.
I	1493.	1507.	1515.
Reference	Mariotti, Costa, et al., 1997	Píry, Príbela, et al., 1995	Le Quere and Latrasse, 1990
Comment	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

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Flamini, Luigi Cioni, et al., 2005
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Flamini, Luigi Cioni, et al., 2005, 2
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Javidnia, Miri, et al., 2005
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Paolini, Costa, et al., 2005
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Senatore, Napolitano, et al., 2005
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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