Pyridine, 2-(1-methyl-2-pyrrolidinyl)-
- Formula: C10H14N2
- Molecular weight: 162.2316
- IUPAC Standard InChI: InChI=1S/C10H14N2/c1-12-8-4-6-10(12)9-5-2-3-7-11-9/h2-3,5,7,10H,4,6,8H2,1H3
- IUPAC Standard InChIKey: AQCRXZYYMOXFAN-UHFFFAOYSA-N
- CAS Registry Number: 23950-04-1
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: α-Nicotine; α-Pyridyl-α-methylpyrrolidine; 2-Nicotine; o-Nicotine; Nicotine
- Permanent link for this species. Use this link for bookmarking this species for future reference.
- Information on this page:
- Other data available:
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Gas Chromatography
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | OV-1 | 160. | 1362. | Erdmann, Rochholz, et al., 1992 | |
| Capillary | BP-1 | 130. | 1328. | Japp, Gill, et al., 1987 | 25. m/0.22 mm/0.25 μm, N2 |
| Capillary | BP-1 | 130. | 1327. | Japp, Gill, et al., 1987 | 25. m/0.53 mm/1. μm, N2 |
| Packed | SE-30 | 160. | 1360. | Musumarra, Scarlata, et al., 1987 | N2, 1% se-30 on Anachrom ABS(80-100mesh); Column length: 2. m |
| Packed | OV-101 | 200. | 1377. | Huber, Kenndler, et al., 1979 | N2; Column length: 2. m |
| Packed | Apiezon L | 150. | 1355. | Huber, Kenndler, et al., 1979 | |
| Packed | OV-1 | 150. | 1345. | Berninger and Möller, 1977 | |
| Packed | Apiezon L | 150. | 1355. | Donike and Stratmann, 1976 | Chromosorb W |
| Packed | OV-101 | 150. | 1341. | Möller, 1976 | N2, Chromosorb W; Column length: 2. m |
| Packed | OV-101 | 190. | 1370. | Möller, 1976 | N2, Chromosorb W; Column length: 2. m |
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 1310. | Jenett-Siems, Weigl, et al., 2005 | He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C; Tend: 300. C |
| Capillary | SE-30 | 1328. | Schepers, Wijsbeek, et al., 1982 | 25. m/0.49 mm/1.14 μm, 100. C @ 2. min, 8. K/min, 275. C @ 15. min |
Kovats' RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-101 | 1340. | McLinden and Stenhouse, 1979 | N2, Chromosorb W; Column length: 2. m; Program: not specified |
| Packed | OV-1 | 1340. | Berninger, Grunnagel, et al., 1975 | N2, Chromosorb G, AW-DMCS; Column length: 2. m; Program: not specified |
| Packed | OV-1 | 1360. | Berninger, Grunnagel, et al., 1975 | N2, Chromosorb G, AW-DMCS; Column length: 2. m; Program: not specified |
| Packed | SE-30 | 1340. | Moffat, Stead, et al., 1974 | Column length: 2. m; Program: not specified |
Kovats' RI, polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | PEG-20M | 160. | 1848. | Huber, Kenndler, et al., 1979 | N2 |
| Packed | PEG-20M | 160. | 1848. | Donike and Stratmann, 1976 | Chromosorb W |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5MS | 1339. | Kim, Shin, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 200. C @ 20. min |
| Capillary | DB-5 | 1360. | Moio, Piombino, et al., 2000 | 30. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 210. C |
| Capillary | DB-5 | 1381. | Moio and Addeo, 1998 | 30. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 210. C |
| Capillary | DB-5 | 1384. | Moio and Addeo, 1998 | 30. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 210. C |
| Capillary | SPB-1 | 1354. | Christ, Noomano, et al., 1988 | 30. m/0.75 mm/1.0 μm, He, 10. K/min, 280. C @ 12. min; Tstart: 160. C |
| Capillary | CBP-1 | 1301. | Oyama, Sano, et al., 1987 | N2, 6. K/min; Column length: 12. m; Column diameter: 0.53 mm; Tstart: 120. C; Tend: 250. C |
| Capillary | DB-1 | 1326. | Perrigo, Peel, et al., 1985 | 15. m/0.32 mm/0.25 μm, He, 8. K/min, 280. C @ 5. min; Tstart: 120. C |
| Capillary | Methyl Silicone | 1311.0 | Newton and Foery, 1984 | 12. m/0.2 mm/0.33 μm, He, 50. C @ 1. min, 20. K/min, 300. C @ 3. min |
| Capillary | 5 % Phenyl methyl siloxane | 1346.0 | Newton and Foery, 1984 | 12. m/0.2 mm/0.33 μm, He, 50. C @ 1. min, 20. K/min, 300. C @ 3. min |
| Capillary | DB-1 | 1326. | Perrigo, Ballantyne, et al., 1984 | 15. m/0.25 mm/0.25 μm, He, 8. K/min, 280. C @ 5. min; Tstart: 120. C |
| Capillary | DB-1 | 1329. | Perrigo, Ballantyne, et al., 1984 | 15. m/0.25 mm/0.25 μm, He, 12. K/min, 280. C @ 5. min; Tstart: 120. C |
| Capillary | DB-1 | 1330. | Perrigo, Ballantyne, et al., 1984 | 15. m/0.25 mm/0.25 μm, He, 15. K/min, 280. C @ 5. min; Tstart: 120. C |
| Capillary | DB-1 | 1323. | Perrigo, Ballantyne, et al., 1984 | 15. m/0.25 mm/0.25 μm, He, 5. K/min, 280. C @ 5. min; Tstart: 120. C |
| Capillary | SE-30 | 1315. | Anderson and Stafford, 1983 | 15. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 100. C; Tend: 295. C |
| Packed | SE-30 | 1340. | Perrigo and Peel, 1981 | N2, Chromosorb W, 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 1.8 m |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | CP Sil 5 CB | 1332. | Aderjan and Bogusz, 1988 | 10. m/0.53 mm/5.0 μm, He; Program: 100 0C (2 min ) 15 0C/min -> 200 0C 10 0C/min -> 300 0C (8 min hold) |
| Capillary | CP Sil 5 CB | 1348. | Aderjan and Bogusz, 1988 | 10. m/0.53 mm/5.0 μm, He; Program: not specified |
| Capillary | BP-1 | 1331. | Stowell and Wilson, 1987 | 12. m/0.22 mm/0.25 μm, He; Program: 120C => 8C/min => 270C => 25C/min => 300C |
Van Den Dool and Kratz RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-Wax | 1842. | Kim, Shin, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 2. K/min, 200. C @ 20. min |
Normal alkane RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | Apieson L / KOH | 150. | 1341. | Caddy, Fish, et al., 1973 | |
| Capillary | Apieson L / KOH | 150. | 1343. | Caddy, Fish, et al., 1973 | |
| Capillary | Apieson L / KOH | 150. | 1346. | Caddy, Fish, et al., 1973 | |
| Capillary | Apieson L / KOH | 150. | 1350. | Caddy, Fish, et al., 1973 | |
| Capillary | Apieson L / KOH | 150. | 1353. | Caddy, Fish, et al., 1973 | |
| Capillary | Apieson L / KOH | 150. | 1354. | Caddy, Fish, et al., 1973 | |
| Capillary | Apieson L / KOH | 190. | 1387. | Caddy, Fish, et al., 1973 |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | Polydimethyl siloxane | 1346. | MHA, 9999 | Nitrogen; Column length: 2. m; Tstart: 100. C; Tend: 300. C |
| Capillary | DB-5 | 1355. | Grung, Lichtenthaler, et al., 2007 | 30. m/0.25 mm/0.25 μm, 5. K/min, 280. C @ 10. min; Tstart: 40. C |
| Capillary | HP-5 | 1366.5 | Leffingwell and Alford, 2005 | 60. m/0.32 mm/0.25 μm, He, 30. C @ 2. min, 2. K/min, 260. C @ 28. min |
| Capillary | DB-1 | 1312. | Tofern, Kaloga, et al., 1999 | He, 6. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C; Tend: 300. C |
| Capillary | DB-5 | 1379. | Moio, Dekimpe, et al., 1993 | 30. m/0.32 mm/1. μm, H2, 3. K/min; Tstart: 40. C; Tend: 220. C |
| Capillary | Ultra-1 | 1307. | Okumura, 1991 | 25. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 80. C; Tend: 260. C |
| Capillary | BP-1 | 1330. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 12. K/min; Tstart: 120. C; Tend: 270. C |
| Capillary | BP-1 | 1332. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 15. K/min; Tstart: 120. C; Tend: 270. C |
| Capillary | BP-1 | 1338. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 25. K/min; Tstart: 120. C; Tend: 270. C |
| Capillary | BP-1 | 1324. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 6. K/min; Tstart: 120. C; Tend: 270. C |
| Capillary | BP-1 | 1328. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 8. K/min; Tstart: 120. C; Tend: 270. C |
| Capillary | BP-1 | 1315. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 5. K/min; Tstart: 100. C; Tend: 295. C |
| Capillary | BP-1 | 1326. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 8. K/min; Tstart: 120. C; Tend: 280. C |
| Capillary | BP-1 | 1311. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 20. K/min; Tstart: 50. C; Tend: 300. C |
| Packed | SE-30 | 1340. | Marozzi, Gambaro, et al., 1982 | Gas Chrom P, 2.5 K/min; Column length: 2. m; Tstart: 120. C; Tend: 200. C |
| Packed | SE-30 | 1335. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1325. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1326. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1327. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1327. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1329. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1329. | Peel and Perrigo, 1976 | Nitrogen, Chromosorb W AW DMS (80-100 mesh), 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
| Packed | SE-30 | 1335. | Peel and Perrigo, 1975 | N2, Chromosorb W AW DMS, 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 2. m |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | 5 % Phenyl methyl siloxane | 1362. | Grigoriev and Savchuk, 2010 | 25. m/0.20 mm/0.33 μm; Program: 50 0C (0.5 min) 99 0C/min -> 100 0C (1 min) 15 0C/min -> 280 0C (20 min) |
| Capillary | 5 % Phenyl methyl siloxane | 1375. | Grigoriev and Savchuk, 2010 | 25. m/0.20 mm/0.33 μm; Program: 50 0C (0.5 min) 99 0C/min -> 100 0C (1 min) 15 0C/min -> 280 0C (20 min) |
| Capillary | DB-5MS | 1346. | Polzin, Stanfill, et al., 2007 | Column length: 30. m; Program: not specified |
| Capillary | SF-96 | 1337. | Kawasaki, Matsui, et al., 1998 | Column length: 40. m; Column diameter: 0.28 mm; Program: 75C => 3C/min => 190C(25min) => 3C/min => 210C |
| Capillary | BP-1 | 1331. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He; Program: 120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min) |
| Capillary | BP-1 | 1340. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He; Program: not specified |
| Other | Methyl Silicone | 1348. | Ardrey and Moffat, 1981 | Program: not specified |
| Capillary | Apieson L / KOH | 1346. | Caddy, Fish, et al., 1973 | Program: not specified |
Normal alkane RI, polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Capillary | Carbowax 20M / KOH | 150. | 1865. | Caddy, Fish, et al., 1973 | |
| Capillary | Carbowax 20M / KOH | 150. | 1876. | Caddy, Fish, et al., 1973 | |
| Capillary | Carbowax 20M / KOH | 150. | 1887. | Caddy, Fish, et al., 1973 |
Normal alkane RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Carbowax 20M | 1829. | Liardon and Ledermann, 1980 | H2, 2. K/min; Column length: 39. m; Column diameter: 0.30 mm; Tstart: 60. C; Tend: 220. C |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Erdmann, Rochholz, et al., 1992
Erdmann, F.; Rochholz, G.; Schütz, H.,
Retention-indices on OV-1 of approximately 170 commonly used pesticides,
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Japp, Gill, et al., 1987
Japp, M.; Gill, R.; Osselton, M.D.,
Comparison of drug retention indices determined on packed, wide bore capillary and narrow bore capillary columns,
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Musumarra, Scarlata, et al., 1987
Musumarra, G.; Scarlata, G.; Romano, G.; Cappello, G.; Clementi, S.; Giulietti, G.,
Qualitative organic analysis. Part 2. Identification of drugs by principal components analysis of standardized TLC data in four eluent systems and of retention indices on SE 30,
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Huber, Kenndler, et al., 1979
Huber, J.F.K.; Kenndler, E.; Reich, G.,
Quantitation of the Information Content of Multi-Dimensional Gas Chromatography and Low- Resolution Mass Spectrometry in the Identification of Doping Drugs,
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Berninger and Möller, 1977
Berninger, H.; Möller, M.R.,
Retentionsindices zur gaschromatographischen Identifizierung von Arzneimitteln,
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Donike and Stratmann, 1976
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Gas-chromatographische identifizierung von stimulantien der phenyläthylaminreihe mit hilfe der retnetions-indices,
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Möller, 1976
Möller, M.R.,
Comparability of retention indices of polar substances at elevated temperatures,
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Jenett-Siems, Weigl, et al., 2005
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Chemotaxonomy of the pantropical genus Merremia (Convolvulaceae) based on the distribution of tropane alkaloids,
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Schepers, Wijsbeek, et al., 1982
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Applicability of capillary gas chromatography to substance identification in toxicology by means of retention indices,
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McLinden and Stenhouse, 1979
McLinden, V.J.; Stenhouse, A.M.,
A chromatography system for drug identification,
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Berninger, Grunnagel, et al., 1975
Berninger, H.; Grunnagel, R.; Mall, S.; Moller, M.R.,
Gas chromatographic identification of unknown substances from body fluids by menas of retention indices,
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Moffat, Stead, et al., 1974
Moffat, A.C.; Stead, A.H.; Smalldon, K.W.,
Optimum use of paper, thin-layer and gas-liquid chromatography for the identification of basic drugs. III. Gas-liquid chromatography,
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Kim, Shin, et al., 2001
Kim, T.H.; Shin, J.H.; Baek, H.H.; Lee, H.J.,
Volatile flavour compounds in suspension culture of Agastache rugosa Kuntze (Korean mint),
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Moio, Piombino, et al., 2000
Moio, L.; Piombino, P.; Addeo, F.,
Odour-impact compounds of Gorgonzola cheese,
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Moio and Addeo, 1998
Moio, L.; Addeo, F.,
Grana Padano cheese aroma,
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Christ, Noomano, et al., 1988
Christ, D.W.; Noomano, P.; Rosas, M.; Rhone, D.,
Retention indices by wide-bore capillary gas chromatography with nitrogen-phosphorus detection,
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Studies on systematic analysis of poisonous compounds in forensic chemistry. II. Application of capillary column gas chromatography to substance identification by means of retention indices,
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Perrigo, Peel, et al., 1985
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Use of Dual-Column Fused-Silica Capillary Gas Chromatography in Combination with Detector Response Factors for Analytical Toxicology.,
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Newton and Foery, 1984
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Retention indices and dual capillary gas chromatography for rapid identification of sedative hypnotic drugs in emergency toxicology,
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Perrigo, Ballantyne, et al., 1984
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Condierations in developing a data base for drugs on a DBI capillary column,
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Applications of capillary gas chromatography in routine toxicological analyses,
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The use of retention indices and temperature-programmed gas chromatography in analytical toxicology,
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Aderjan and Bogusz, 1988
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Nitroalkanes as a multidetector retention index scale for drug identification in gas chromatography,
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Stowell and Wilson, 1987
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A simple approach to the interlaboratory transfer of drug retention indices determined by temperature programmed capillary gas chromatography,
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Caddy, B.; Fish, F.; Scott, D.,
Chromatographic screening for drugs of abuse using capillary columds. II. Peak identification on support coated open tubular columns for a series of central nervous system stimulating drugs,
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MHA, 9999
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Grung, Lichtenthaler, et al., 2007
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Effects-directed analysis of organic toxicants in wastewater effluent from Zagreb, Croatia,
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Leffingwell and Alford, 2005
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Volatile constituents of Perique tobacco,
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Tofern, Kaloga, et al., 1999
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Occurrence of loline alkaloids in Argyreia mollis (Convolvulaceae),
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Moio, Dekimpe, et al., 1993
Moio, L.; Dekimpe, J.; Etievant, P.; Addeo, F.,
Neutral volatile compounds in the raw milks from different species,
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Okumura, 1991
Okumura, T.,
retention indices of environmental chemicals on methyl silicone capillary column,
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Stowell and Wilson, 1985
Stowell, A.; Wilson, L.,
Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]
Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F.,
Use of the retention index in gas chromatographic studies of drugs,
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Peel and Perrigo, 1976
Peel, H.W.; Perrigo, B.,
A practical gas chromatographic screening procedure for toxicological analysis,
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Peel and Perrigo, 1975
Peel, H.W.; Perrigo, B.,
A practical gas chromatographic screening procedure for toxicological analysis,
Can.Soc.Forens.Sci.J., 1975, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247
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Grigoriev and Savchuk, 2010
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Polzin, Stanfill, et al., 2007
Polzin, G.M.; Stanfill, S.B.; Brown, C.R.; Ashley, D.L.; Watson, C.H.,
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Kawasaki, Matsui, et al., 1998
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Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C.,
Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase,
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Liardon and Ledermann, 1980
Liardon, R.; Ledermann, S.,
volatile components of fermented soya hydrolysate. II. Composition of basic fraction,
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. [all data]
Notes
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