Naphtho[1,2-k]fluoranthene
- Formula: C24H14
- Molecular weight: 302.3680
- IUPAC Standard InChI: InChI=1S/C24H14/c1-2-8-18-15(5-1)11-12-17-13-22-19-9-3-6-16-7-4-10-20(24(16)19)23(22)14-21(17)18/h1-14H
- IUPAC Standard InChIKey: TUNJIKOIQLBFSB-UHFFFAOYSA-N
- CAS Registry Number: 238-04-0
- Chemical structure:
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Lee's RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|
| Active phase | HP-5 | DB-5MS | XTI-5 | DB-5 |
| Column length (m) | 60. | 30. | 15. | 30. |
| Carrier gas | He | H2 | ||
| Substrate | ||||
| Column diameter (mm) | 0.25 | 0.25 | 0.28 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 35. | 60. | 70. | 40. |
| Tend (C) | 300. | 320. | 350. | 280. |
| Heat rate (K/min) | 3. | 5. | 5. | 4. |
| Initial hold (min) | 3. | 2. | 2. | |
| Final hold (min) | 20. | 5. | ||
| I | 536.5 | 540.4 | 532.52 | 536.99 |
| Reference | Marynowski, Pieta, et al., 2004 | Sauvain and Duc, 2004 | Engkvist, Borowski, et al., 1996 | Wise, Benner, et al., 1988 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Lee's RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Marynowski, Pieta, et al., 2004
Marynowski, L.; Pieta, M.; Janeczek, J.,
Composition and source of polycyclic aromatic compounds in deposited dust from selected sites around the Upper Silesia, Poland,
Geol. Q., 2004, 48, 2, 169-180. [all data]
Sauvain and Duc, 2004
Sauvain, J.-J.; Duc, T.V.,
Approaches to identifying and quantifying polycyclic aromatic hydrocarbons of molecular weight 302 in diesel particulates,
J. Sep. Sci., 2004, 27, 1-2, 78-88, https://doi.org/10.1002/jssc.200301620
. [all data]
Engkvist, Borowski, et al., 1996
Engkvist, O.; Borowski, P.; Bemgård, A.; Karlström, G.; Lindh, R.; Colmsjö, A.,
On the relation between retention indexes and the interaction between the solute and the column in gas-liquid chromatography,
J. Chem. Inf. Comput. Sci., 1996, 36, 6, 1153-1161, https://doi.org/10.1021/ci960345u
. [all data]
Wise, Benner, et al., 1988
Wise, S.A.; Benner, B.A.; Byrd, G.D.; Chesler, S.N.; Rebbert, R.E.; Schantz, M.M.,
Determination of polycyclic aromatic hydrocarbons in a coal tar standard reference material,
Anal. Chem., 1988, 60, 9, 887-894, https://doi.org/10.1021/ac00160a012
. [all data]
Notes
Go To: Top, Lee's RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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