Cyclohexene, 4-ethenyl-4-methyl-3-(1-methylethenyl)-1-(1-methylethyl)-, (3R-trans)-

Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1RTX-1HP-5 MSHP-5 MS
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.80.50.
Tend (C) 240.230.230.240.180.
Heat rate (K/min) 3.2.2.4.2.
Initial hold (min)    3. 
Final hold (min)  5.5.10. 
I 1335.1340.1340.1327.1326.
ReferenceRodriques, Amorim, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dutra, Pittella, et al., 2012Hammami, Kamoun, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5ZB-5ZB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.50.
Tend (C) 240.240.200.200.300.
Heat rate (K/min) 3.3.5.5.50.
Initial hold (min) 2. 5.5.5.
Final hold (min)    5.5.
I 1339.1339.1352.1357.1337.
ReferenceKahriman, Tosun, et al., 2011Karimi, Farmani, et al., 2011Vazques, Aimar, et al., 2011Vazquez, Demmel, et al., 2011Bi Kouame, Bedi, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5 MSDB-5 MSDB-1
Column length (m) 30.25.30.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.70.60.50.
Tend (C) 250.250.290.240.220.
Heat rate (K/min) 2.4.5.3.4.
Initial hold (min)  1.  2.
Final hold (min)  10.10. 2.
I 1338.1339.1338.1333.1332.
ReferenceHo, Wang, et al., 2010Mirjalili, Salehi, et al., 2010Radulovic, Dordevic, et al., 2010Silva, Pott, et al., 2010Xu, Tang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5 MSDB-5VF-5MSSLB-5 MS
Column length (m) 30.60.30.30.30.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.240.50.
Tend (C) 260.330.230.320.250.
Heat rate (K/min) 2.2.2.20.3.
Initial hold (min) 5.12. 1.2.
Final hold (min) 999.30.  10.
I 1335.1346.1340.1341.1337.
ReferenceDayisoylu and Alma, 2009Patil, Jayaprakasha, et al., 2009Scrivanti, Anton, et al., 2009Kowalski, 2008Lo Presti, Sciarrone, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-1OV-1HP-5MSHP-5MSDB-1
Column length (m) 30.30.30.30.60.
Carrier gas HeliumHeliumHeHeNitrogen
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.65.60.60.60.
Tend (C) 246.260.240.250.250.
Heat rate (K/min) 3.6.3.2.4.
Initial hold (min)    8.1.
Final hold (min)    15.10.
I 1334.1381.1327.1339.1342.
ReferenceRaj, Baby, et al., 2008Wang, Yi, et al., 2008Argyropoulou, Daferera, et al., 2007Ferhat, Meklati, et al., 2007Ghasempour, Shirinpour, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1ZB-5SPB-5DB-1DB-5
Column length (m)  30.30.60.30.
Carrier gas He HeNitrogen 
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.50.60.40.
Tend (C) 220.220.250.250.250.
Heat rate (K/min) 5.4.2.4.2.
Initial hold (min)  5. 1. 
Final hold (min) 6.20. 10.33.
I 1337.1339.1337.1342.1342.
ReferenceKiran, Devi, et al., 2007Mohottalage, Tabacchi, et al., 2007Raal, Orav, et al., 2007Reza, Ebrahim, et al., 2007Sylvestre, Pichette, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1HP-1HP-1HP-1
Column length (m) 30.50.50.50.50.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.220.20.20.2
Phase thickness (μm) 0.250.250.330.330.33
Tstart (C) 40.60.60.60.60.
Tend (C) 260.220.250.250.250.
Heat rate (K/min) 4.2.2.2.2.
Initial hold (min)   4.4.4.
Final hold (min)  20.30.30.30.
I 1333.81336.1334.1330.1332.
ReferenceZizovic, Stamenic, et al., 2007Boti, Yao, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5MSBP-1CP Sil 5 CBDB-5
Column length (m) 50.30. 30.30.
Carrier gas HeHeHeliumN2He
Substrate      
Column diameter (mm) 0.220.25 0.320.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.50.60.50.60.
Tend (C) 220.250.220.300.220.
Heat rate (K/min) 2.2.5.4.4.
Initial hold (min)      
Final hold (min) 20. 6.  
I 1337.1339.1337.1330.1339.
ReferenceFanciullino, Tomi, et al., 2006Farah, Afifi, et al., 2006Kiran, Bhavani, et al., 2006Lis and Milczarek, 2006Morteza-Semnani, Akbarzadeh, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas  HeHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.70.70.70.
Tend (C) 265.220.280.280.280.
Heat rate (K/min) 2.55.4.4.4.
Initial hold (min) 0.510.4.4.4.
Final hold (min)      
I 1337.1329.1379.1338.1339.
ReferenceNickavar B., Kamalinejad M., et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5 MSHP-5MSHP-5MS
Column length (m) 25.30.30.30.25.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.40.60.50.
Tend (C) 240.200.200.275.250.
Heat rate (K/min) 3.2.8.4.3.
Initial hold (min)   3. 3.
Final hold (min)  60.20. 10.
I 1341.1342.1361.1338.1336.
ReferencePotzernheim, Bizzo, et al., 2006Rout, Naik, et al., 2006Schirack, Drake, et al., 2006Asadipour, Mehrabani, et al., 2005Ghasemi Y., Faridi P., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBDB-1DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2N2He Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.35.35.
Tend (C) 250.250.265.280.280.
Heat rate (K/min) 5.5.2.54.4.
Initial hold (min)   1.2.2.
Final hold (min) 10.10.20.  
I 1343.1343.1320.1341.1341.
ReferenceJassbi, Mehrdad, et al., 2005Jassbi, Mehrdad, et al., 2005Khanavi, Ghasemian, et al., 2005Kowalski and Wolski, 2005Kowalski, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5DB-1RTX-5 MSHP-5MS
Column length (m) 30.30.50.30.30.
Carrier gas HeHeN2He 
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.95.50.60.
Tend (C) 280.220.240.280.280.
Heat rate (K/min) 3.4.4.8.3.
Initial hold (min) 30.4. 2. 
Final hold (min)    2. 
I 1313.1339.1333.1343.1338.
ReferenceMarongiu, Piras, et al., 2005Morteza-Semnani and Saeedi, 2005Pala-Paul, Perez-Alonso, et al., 2005Pellati, Benvenuti, et al., 2005Petrakis, Roussis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSRTX-1HP-5MSDB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.50.60.
Tend (C) 265.280.25.240.280.
Heat rate (K/min) 2.53.5.3.3.
Initial hold (min) 1.5. 3. 
Final hold (min) 20. 10.  
I 1325.1337.1339.1386.1310.
ReferenceSarkhail, Amin, et al., 2005Setzer, Noletto, et al., 2005Sonboli, Salehi, et al., 2005Tepe B., Sokmen M., et al., 2005Tzakou and Constantinidis, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-5DB-5RTX-1DB-5
Column length (m) 50.60.25.30.30.
Carrier gas HeHeNitrogenN2He
Substrate      
Column diameter (mm) 0.20.320.250.250.25
Phase thickness (μm) 0.331.0.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 220.200.240.300.300.
Heat rate (K/min) 4.4.3.4.3.
Initial hold (min) 3.    
Final hold (min) 30.30.   
I 1339.1347.1337.1338.1333.
ReferenceWong, Lee, et al., 2005Gauvin, Ravaomanarivo, et al., 2004JAvidnia, Mojab, et al., 2004Kalemba and Thiem, 2004Limberger, Sobral, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSDB-1CP Sil 5 CBHP-5MS
Column length (m) 60.30.30.20.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.50.100.60.
Tend (C) 270.280.265.270.220.
Heat rate (K/min) 4.4.2.58.5.
Initial hold (min)   1.2.20.
Final hold (min)   20. 20.
I 1335.1338.1325.1365.1343.
ReferenceNik, Mirza, et al., 2004Sajjadi and Shahpiri, 2004Sarkhail, Amin, et al., 2004Thappa, Bakshi, et al., 2004Feizbaksh, Saber Tehrani, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RSL-200DB-5HP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2H2HeHeliumHe
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.40.60.70.60.
Tend (C) 200.280.250.210.275.
Heat rate (K/min) 5.6.3.2.4.
Initial hold (min)  5.  5.
Final hold (min)  5. 60. 
I 1334.1335.1337.1337.1339.
ReferenceFekam Boyom, Ngouana, et al., 2003Jirovetz, Buchbauer, et al., 2003Limberger, Simões-Pires, et al., 2003Mookdasanit, Tamura, et al., 2003Morteza-Semnani and Saeedi, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5DB-5HP-5
Column length (m) 50.30.30.30.60.
Carrier gas N2H2HeHe 
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 95.60.60.75.40.
Tend (C) 240.280.280.220.250.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min)  10. 4.15.
Final hold (min)  40.   
I 1324.1339.1331.1340.1341.
ReferencePerez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Priestap, van Baren, et al., 2003Stashenko, Jaramillo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5DB-5OV-101
Column length (m) 25.25.30.25.25.
Carrier gas HeliumHeliumHeN2 
Substrate      
Column diameter (mm) 0.320.320.250.250.32
Phase thickness (μm) 0.530.530.250.25 
Tstart (C) 40.40.60.50.50.
Tend (C) 280.280.240.250.200.
Heat rate (K/min) 4.4.3.4.5.
Initial hold (min)      
Final hold (min)    10. 
I 1335.1338.1340.1340.1342.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Zoghbi, Andrade, et al., 2003Zrira, Elamrani, et al., 2003Boyom, Keumedjio, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5DB-1SE-30RSL-200
Column length (m) 30.30.30.50.30.
Carrier gas HeHeH2HeH2
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 75.60.40.70.40.
Tend (C) 200.240.245.240.280.
Heat rate (K/min) 3.3.3.4.6.
Initial hold (min) 4. 20. 5.
Final hold (min) 8.   5.
I 1338.1340.1327.1336.1340.
ReferenceCicció and Gómez-Laurito, 2002Flamini, Ertugrul, et al., 2002Gancel, Ollé, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5DB-5MSHP-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.230.250.320.250.25
Phase thickness (μm) 0.200.250.250.250.25
Tstart (C) 50.35.40.60.60.
Tend (C) 200.280.290.240.240.
Heat rate (K/min) 3.3.7.3.3.
Initial hold (min) 3.2.   
Final hold (min) 30.15.   
I 1341.1341.1343.1337.1342.
ReferenceKhallouki, Younos, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Lin, Rouseff, et al., 2002Maia, Zoghbi, et al., 2002Novak, Langbehn, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZEBRON-5DB-1HP-1DB-1DB-5MS
Column length (m) 6.50.50.60.30.
Carrier gas HeN2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.80.90.40.60.
Tend (C) 200.225.220.280.270.
Heat rate (K/min) 3.4.3.4.3.
Initial hold (min) 5.  5. 
Final hold (min) 15.    
I 1334.1335.1339.1331.1338.
ReferenceÖztürk, Akay, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002Priestap, van Baren, et al., 2002Sefidkon, 2002Zoghbi, Andrade, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5RTX-1DB-5DB-5
Column length (m) 60.60.30.60.30.
Carrier gas N2HeN2HeH2
Substrate      
Column diameter (mm) 0.2480.320.250.250.25
Phase thickness (μm) 0.25 0.25 0.25
Tstart (C) 60.40.60.50.60.
Tend (C) 220.220.300.250.285.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min) 5.5. 5. 
Final hold (min) 22.15.   
I 1334.1338.1337.1339.1334.
ReferenceBailac, Dellacasa, et al., 2001Cornu, Carnat, et al., 2001Kalemba, Marschall, et al., 2001Rousis, Papadogianni, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5OV-101OV-101DB-1
Column length (m) 30.30.50.50.60.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm)  0.25  0.25
Tstart (C) 60.60.80.80.60.
Tend (C) 240.240.200.200.220.
Heat rate (K/min) 3.3.2.2.3.
Initial hold (min)     5.
Final hold (min)     22.
I 1333.01340.1339.1339.1347.
ReferenceSantos, Moreira, et al., 2001Tellez M., Estell R., et al., 2001Yang, 2001Yang, 2001, 2Bailac, Dellacasa, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-101RTX-1CP Sil 5 CB
Column length (m) 33.30.25.30.25.
Carrier gas N2 N2N2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.500.25 0.250.39
Tstart (C) 50.45.50.60.60.
Tend (C) 135.300.200.300.220.
Heat rate (K/min) 20.15.5.4.5.
Initial hold (min) 2.2.  5.
Final hold (min)  5.  20.
I 1353.1360.1335.1340.1340.
ReferenceFeger, Brandauer, et al., 2000Hedin, McKibben, et al., 2000Ayedoun, Adéoti, et al., 1999Kalemba, 1999Rustaiyan, Masoudi, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101CP Sil 5 CBCP Sil 5 CBCP Sil 5 CB
Column length (m) 30.25.25.25.25.
Carrier gas He N2N2He
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.50.50.50.60.
Tend (C) 240.200.290.290.300.
Heat rate (K/min) 3.5.4.4.6.
Initial hold (min)      
Final hold (min)      
I 1335.1337.1326.1326.1326.
ReferenceEl-Sakhawy, El-Tantawy, et al., 1998Zollo, Biyiti, et al., 1998Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-1OV-101
Column length (m) 30.30.30.23.50.
Carrier gas HeHeliumHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.25 0.170.17
Tstart (C) 65.60.60.60.50.
Tend (C) 300.240.240.250.220.
Heat rate (K/min) 4.3.4.5.5.
Initial hold (min) 2.  3. 
Final hold (min)    30. 
I 1344.1339.1342.1330.1345.
ReferenceElias, Simoneit, et al., 1997Tellez, Estell, et al., 1997Zunino, Novillo-Newton, et al., 1997Ayedoun, Adeoti, et al., 1996Chacko, Jayalekshmy, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101HP-1Methyl SiliconeMethyl SiliconeSE-54
Column length (m) 50.25.50.50.30.
Carrier gas HeHeliumN2N2Hydrogen
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm)  0.250.170.170.25
Tstart (C) 50.60.80.80.60.
Tend (C) 250.220.200.200.250.
Heat rate (K/min) 2.4.2.3.2.
Initial hold (min)  2.  5.
Final hold (min)  20.  2.
I 1330.1330.1381.1376.1333.
ReferenceOrav, Kailas, et al., 1996Thanh, Dung, et al., 1996Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-101OV-101DB-1OV-101
Column length (m) 25.50.50.60.50.
Carrier gas  N2N2 N2
Substrate      
Column diameter (mm) 0.330.250.250.320.25
Phase thickness (μm)      
Tstart (C) 45.80.80.50.80.
Tend (C) 180.200.200.250.200.
Heat rate (K/min) 3.2.2.4.2.
Initial hold (min) 3.  0.1 
Final hold (min)    5. 
I 1333.1339.1347.1333.1340.
ReferenceWyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Binder and Flath, 1989Sugisawa, Yang, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase OV-101SE-30OV-101SE-30
Column length (m) 50.30.30.30.
Carrier gas N2 He 
Substrate     
Column diameter (mm) 0.25 0.5 
Phase thickness (μm)   0.8 
Tstart (C) 80.50.40.50.
Tend (C) 200.240.220.240.
Heat rate (K/min) 2.4.2.4.
Initial hold (min)  2. 2.
Final hold (min)  10. 10.
I 1347.1381.1331.1381.
ReferenceSugisawa, Yang, et al., 1989Ramaswami, Briscese, et al., 1988De Pooter and Schamp, 1986Ramaswami, Briscese, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Pellati, Benvenuti, et al., 2005
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Petrakis, Roussis, et al., 2005
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Sarkhail, Amin, et al., 2005
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Setzer, Noletto, et al., 2005
Setzer, W.N.; Noletto, J.A.; Lawton, R.O.; Haber, W.A., Leaf essential oil composition of five Zanthoxylum species from Monteverde, Costa Rica, Molecular Diversity, 2005, 9, 1-3, 3-13, https://doi.org/10.1007/s11030-005-1298-6 . [all data]

Sonboli, Salehi, et al., 2005
Sonboli, A.; Salehi, P.; Ebrahimi, S.N., Essential oil composition and antibacterial activity of the leaves of Stachys schtschegleevii from Iran, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 2, 171-175, https://doi.org/10.1007/s10600-005-0105-z . [all data]

Tepe B., Sokmen M., et al., 2005
Tepe B.; Sokmen M.; Akpulat H.A.; Daferera D.; Polissiou M.; Sokmen A., Antioxidative activity of the essential oils of Thymus sipyleus subsp sipyleus var. sipyleus and Thymus sipyleus subsp sipyleus var. rosulans, J. Food Eng., 2005, 66, 4, 447-454, https://doi.org/10.1016/j.jfoodeng.2004.04.015 . [all data]

Tzakou and Constantinidis, 2005
Tzakou, O.; Constantinidis, T., Chemotaxonomic significance of volatile compounds in Thymus samius and its related species Thymus atticus and Thymus parnassicus, Biochem. Syst. Ecol., 2005, 33, 11, 1131-1140, https://doi.org/10.1016/j.bse.2005.03.008 . [all data]

Wong, Lee, et al., 2005
Wong, K.C.; Lee, B.C.; Lam, N.F.; Ibrahim, P., Essential oils of the rhizomes of Alpinia conchigera Griff. and Alpinia latilabris Ridl., Flavour Fragr. J., 2005, 20, 4, 431-433, https://doi.org/10.1002/ffj.1458 . [all data]

Gauvin, Ravaomanarivo, et al., 2004
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JAvidnia, K.; Mojab, F.; Mojahedi, S.A., Chemical constituents of the essential oil of Stachys lavandulifolia Vahl from Iran, Iranian J. Pharm. Res., 2004, 3, 61-63. [all data]

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Limberger, Sobral, et al., 2004
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Nik, Mirza, et al., 2004
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Sajjadi and Shahpiri, 2004
Sajjadi, S.E.; Shahpiri, Z., Chemical composition of the essential oil of Salvia limbata C.A.Mey, DARU, 2004, 12, 3, 94-97. [all data]

Sarkhail, Amin, et al., 2004
Sarkhail, P.; Amin, G.; Shafiee, A., Composition of the essential oil of Phlomis persica Boiss and Phlomis chorassanica Bunge from Iran, Flavour Fragr. J., 2004, 19, 6, 538-540, https://doi.org/10.1002/ffj.1338 . [all data]

Thappa, Bakshi, et al., 2004
Thappa, R.K.; Bakshi, S.K.; Dhar, L.; Agarwal, S.G.; Kitchlu, S.; Kaul, M.K.; Suri, K.A., Significance of changed climatic factors on essential oil composition of Echinacea purpurea under subtropical conditions, Flavour Fragr. J., 2004, 19, 5, 452-454, https://doi.org/10.1002/ffj.1352 . [all data]

Feizbaksh, Saber Tehrani, et al., 2003
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Fekam Boyom, Ngouana, et al., 2003
Fekam Boyom, F.; Ngouana, V.; Amvam Zollo, P.H.; Menut, C.; Bessiere, J.M.; Gut, J.; Rosenthal, P.J., Composition and anti-plasmodial activities of essential oils from some Cameroonian medicinal plants, Phytochemistry, 2003, 64, 7, 1269-1275, https://doi.org/10.1016/j.phytochem.2003.08.004 . [all data]

Jirovetz, Buchbauer, et al., 2003
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Notes

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