1-Naphthalenol, 1,2,3,4,4a,7,8,8a-octahydro-1,6-dimethyl-4-(1-methylethyl)-, [1R-(1α,4β,4aβ,8aβ)]-


Normal alkane RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSPolydimethyl siloxane with 5 % Ph groupsDB-5Elite-5 MSElite-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program not specified50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0C50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)
I 1645.1645.1603.1640.1640.
ReferencePinheiro, de Queiros, et al., 2013da Silva, de Souza, et al., 2012Courtois, Paine, et al., 2009Kapoor, Singh, et al., 2009Kapoor, Singh, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1DB-5HP-5DB-5
Column length (m) 30.30.30.30.25.
Carrier gas HeliumHydrogenHelium Nitrogen
Substrate      
Column diameter (mm) 0.250.250.250.320.22
Phase thickness (μm) 0.250.250.25 0.25
Program 40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specifiednot specifiednot specified
I 1645.1618.1652.1646.1674.
ReferenceMancini, Arnold, et al., 2009Mendes, Trindade, et al., 2009Porto, Decorti, et al., 2009Riahi, Pourbasheer, et al., 2009Chieng, Assim, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-5SPB-5CP Sil 8 CBCP Sil 8 CB
Column length (m) 30.  30.50.
Carrier gas Helium   Helium
Substrate      
Column diameter (mm) 0.25  0.250.32
Phase thickness (μm) 0.25  0.250.25
Program not specifiednot specifiednot specified60C => 2.5C/min => 170C => 10C/min => 250C (5min)not specified
I 1656.1635.1656.1645.1642.
ReferenceIsidorov, Lech, et al., 2008Kilani, Ledauphin, et al., 2008Kilani, Ledauphin, et al., 2008Kristiawan, Sobolik, et al., 2008Kupcinskiene, Stikliene, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSDB-1Elite-1CBP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified45C => 3C/min => 175C => 15C/min => 300C (10min)not specified60C(2min) => 3C/min => 240C => 10C/min => 300C40C(10min) => 3C/min => 200C => 2C/min => 220C
I 1646.1618.1646.1633.1645.
ReferenceLo Presti, Sciarrone, et al., 2008Nogueira, Marcelo-Curto, et al., 2008Raj, Baby, et al., 2008Cheriti, Saad, et al., 2007Cole, Haber, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSDB-1HP-5MSDB-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas  HeliumHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 75C(4min) => 5C/min => 135C => 1C/min => 220C => 10C/min => 280C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C45C => 3C/min => 175C => 15C/min => 300C (10min)40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C60 0C 3 0C/min -> 210 0C 5 0C/min -> 250 0C
I 1641.1645.1618.1645.1645.
ReferenceDuschatzky, Almeida, et al., 2007Eason and Setzer, 2007Ferreira, Meireles de Sousa, et al., 2007Formisano, Mignola, et al., 2007Haznagy-Radnai, Szigle, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5 MSHP-5 MSHP-5MS
Column length (m) 30. 30.30.30.
Carrier gas H2 HeliumHeliumHe
Substrate      
Column diameter (mm) 0.25 0.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Program 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40C(10min) => 3C/min => 200C => 2C/min => 220C
I 1618.1649.1647.1647.1643.
ReferenceKamatou, Viljoen, et al., 2007Liolios, Laouer, et al., 2007Moriarity, Bansal, et al., 2007Moriarity, Bansal, et al., 2007Moronkola, Ogunwande, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5 MSHP-5 MSHP-5MSPolydimethyl siloxane
Column length (m) 30.30. 30. 
Carrier gas HeHelium He 
Substrate      
Column diameter (mm) 0.250.25 0.25 
Phase thickness (μm) 0.25    
Program 45C => 3C/min => 175C => 15C/min => 300C(10min)40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0Cnot specified40C(10min) => 3C/min => 200C => 2C/min => 220Cnot specified
I 1618.1645.1647.1645.1645.
ReferenceRodrigues, Antunes, et al., 2007Setzer, Stokes, et al., 2007Stokes, Cole, et al., 2007Takaku, Haber, et al., 2007Werka, Boehme, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSCP Sil 8 CBDB-5DB-1DB-5
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)35C => 4C/min => 180C => 10C/min => 250C45C => 3C/min => 175C => 15C/min => 300C (10min)40C(1min) => 9C/min => 130C => 2C/min => 230C
I 1645.1645.1645.1618.1636.
ReferenceSchmidt, Noletto, et al., 2006Butkienë, Nivinskienë, et al., 2005Cysne, Canuto, et al., 2005Figueiredo, Sim-Sim, et al., 2005Hamm, Bleton, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 8 CBCP Sil 8 CBDB-5CP Sil 8 CB
Column length (m) 30.50.50.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (μm) 0.250.250.250.10.25
Program 35C => 4C/min => 180C => 10C/min => 250C60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)35C => 4C/min => 180C => 20C/min => 280C50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
I 1646.1645.1646.1641.1645.
Referencede Menezes, Lemos, et al., 2005Nivinskienë, Butkienë, et al., 2005Radudienë, Judpintienë, et al., 2005Barros-Filho, Nunes, et al., 2004Butkienë, Nivinskienë, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-1SE-30SE-30DB-5
Column length (m) 15.30.  30.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.3170.25  0.25
Phase thickness (μm)  0.25  0.25
Program 50C(4min) => 4C/min => 90C => 10C/min => 300C(10min)45C => 3C/min => 175C => 15C/min => 300C (10min)not specifiednot specified40C (1min) => 9C/min => 130C => 2C/min => 230C
I 1615.1618.1633.1625.1636.
ReferenceEl-Shazly and Hussein, 2004Miguel, Simões, et al., 2004Vinogradov, 2004Vinogradov, 2004Hamm, Lesellier, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 8CB-MSCP Sil 8 CBDB-1Methyl SiliconeDB-5
Column length (m) 50.50.30.  
Carrier gas  HeHe  
Substrate      
Column diameter (mm) 0.320.320.25  
Phase thickness (μm)  0.250.1  
Program 60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C60C(1min) => 5C/min => 160C => 10C/min => 250C(5min)35C => 4C/min => 180C => 10C/min => 250Cnot specifiednot specified
I 1645.1645.1627.1607.1646.
ReferenceMockute, Bernotiene, et al., 2003Mockute, Nivinskiene, et al., 2003Silva, Matos, et al., 2003Bakshu and Raju, 2002Morteza-Semnani and Vahedi, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1CP Sil 5 CBCP Sil 5 CBDB-1
Column length (m) 30.30.25.25.30.
Carrier gas  H2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.39 0.25
Phase thickness (μm) 0.250.25 0.390.25
Program 45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)not specifiednot specified45C => 3C/min => 175C => 15C/min => 240C (10min)
I 1618.1618.1639.1632.1618.
ReferenceFigueiredo, Miguel, et al., 2001da Silva, Pedro, et al., 2000Weyerstahl, Marschall, et al., 1999Weyerstahl, Marschall, et al., 1999, 2Baratta, Dorman, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBDB-1Polydimethyl siloxanesPolydimethyl siloxanes
Column length (m) 25.25.30.  
Carrier gas HeN2He  
Substrate      
Column diameter (mm)   0.25  
Phase thickness (μm) 0.390.390.25  
Program not specifiednot specified45C => 3C/min => 175C => 15C/min => 280Cnot specifiednot specified
I 1628.1638.1618.1646.1633.
ReferenceWeyerstahl, Marschall, et al., 1998Weyerstahl, Marschall, et al., 1998, 2Gaspar, Palma, et al., 1997Zenkevich, 1997Zenkevich, 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase Polydimethyl siloxanesHP-1
Column length (m)  24.
Carrier gas   
Substrate   
Column diameter (mm)  0.32
Phase thickness (μm)  0.25
Program not specified60C(2min) => 4C/min => 120C => 2C/min => 220C (20min)
I 1625.1620.
ReferenceZenkevich, 1997Dung, Thanh, et al., 1996
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pinheiro, de Queiros, et al., 2013
Pinheiro, P.F.; de Queiros, V.T.; Rondelli, V.M.; Costa, A.V.; MArcelino, T. deP.; Pratissoli, D., Insecticidal activity of citronells grass essential oil on Frankliniella schultzei and Myzus persicae, Cienc. Agrotec. Lavras, 2013, 37, 2, 138-144, https://doi.org/10.1590/S1413-70542013000200004 . [all data]

da Silva, de Souza, et al., 2012
da Silva, A.C.; de Souza, P.E.; Machado, J. daC.; da Silva, B.M.; Pinto, J.E.B.P., Effectiveness of essential oils in the treatment of Colletotrichum truncatum-infected soybean seeds, Tropical Plant Patology, 2012, 37, 5, 305-313, https://doi.org/10.1590/S1982-56762012000500001 . [all data]

Courtois, Paine, et al., 2009
Courtois, E.A.; Paine, C.E.; Blandinieres, P.-A.; Stien, D.; Bessiere, J.-M.; Houel, E.; Baraloto, C.; Chave, J., Diversity of the volatile organic compounds emitted by 55 species of tropical trees: a survey in French Guiana, J. Chem. Ecol., 2009, 35, 11, 1349-1362, https://doi.org/10.1007/s10886-009-9718-1 . [all data]

Kapoor, Singh, et al., 2009
Kapoor, I.; Singh, B.; Singh, G.; De Heluani, C.S.; De Lampasona, M.P.; Catalan, C.A.N., Chemistry and in vitro antioxidant activity of volatile oil and oleoresins of black pepper (Piper nigrum), J. Agric. Food Chem., 2009, 57, 12, 5358-5364, https://doi.org/10.1021/jf900642x . [all data]

Mancini, Arnold, et al., 2009
Mancini, E.; Arnold, N.A.; De Martino, L.; De Feo, V.; Formisano, C.; Rigano, D.; Senatore, F., Chemical composition and phytotoxic effects of essential oils of Salvia hierosolymitana Boiss. and Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon, Molecules, 2009, 14, 11, 4725-4736, https://doi.org/10.3390/molecules14114725 . [all data]

Mendes, Trindade, et al., 2009
Mendes, M.D.; Trindade, H.; Figueiredo, A.C.; Barroso, J.G.; Fontinha, S.S.; Pedro, L.G., Volatile and molecular characterization of two Portuguese endemic species: Angelica lignescens and Melanoselinium decipiens, Biochen. Systematics Ecol., 2009, 37, 2, 98-105, https://doi.org/10.1016/j.bse.2008.12.006 . [all data]

Porto, Decorti, et al., 2009
Porto, C.Da.; Decorti, D.; Kikic, I., Flavour compounds of Lavandula angustifolia L. to use in food manufacturing: comparison of three different extraction methods, Food Chem., 2009, 112, 4, 1072-1078, https://doi.org/10.1016/j.foodchem.2008.07.015 . [all data]

Riahi, Pourbasheer, et al., 2009
Riahi, S.; Pourbasheer, E.; Ganjali, M.R.; Norouzi, P., Investigation of different linear and non-linear chemometric methods for modeling of retention index of essential oil components: Concerns to support vector mashine, J. Hazard. Mat., 2009, 166, 2-3, 853-859, https://doi.org/10.1016/j.jhazmat.2008.11.097 . [all data]

Chieng, Assim, et al., 2008
Chieng, T.C.; Assim, Z.B.; Fasihuddin, B.A., Toxicity and antitermite activities of the essential oils from Piper sarmentosum, The Malaysian J. Anal. Sci., 2008, 12, 1, 234-239. [all data]

Isidorov, Lech, et al., 2008
Isidorov, V.A.; Lech, P.; Zolciak, A.; Rusak, N.; Szczepaniak, L., Gas Chromatographic - nass spectrometric investigation of metabolites from the needles and roots of pine seedlings at early stages of pathogenic fungi Armillaria ostoyae attack, Trees, 2008, 22, 4, 531-542, https://doi.org/10.1007/s00468-008-0213-z . [all data]

Kilani, Ledauphin, et al., 2008
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Kristiawan, Sobolik, et al., 2008
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Kupcinskiene, Stikliene, et al., 2008
Kupcinskiene, E.; Stikliene, A.; Judzentiene, A., The essential oil guatitative composition in the needles of Pinus sylvestris L. growing along industrial transects, Environ. Pollution, 2008, 155, 3, 481-491, https://doi.org/10.1016/j.envpol.2008.02.001 . [all data]

Lo Presti, Sciarrone, et al., 2008
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Raj, Baby, et al., 2008
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Cheriti, Saad, et al., 2007
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Cole, Haber, et al., 2007
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Duschatzky, Almeida, et al., 2007
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Eason and Setzer, 2007
Eason, H.M.; Setzer, W.N., BArk essential oil composition of Cedrela tinduzii C. DC. (Meliaceae) from Monteverde, Costa Rica, Rec. NAt. Prod., 2007, 1, 2-3, 24-27. [all data]

Ferreira, Meireles de Sousa, et al., 2007
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Haznagy-Radnai, Szigle, et al., 2007
Haznagy-Radnai, E.; Szigle, Sz.; Mathe, I., Analysis of the essential oil of Downy wounderwort (Stachys Germanica L.), Acta Fac. Pharm. Univer. Comenianae, 2007, 54, 78-83. [all data]

Kamatou, Viljoen, et al., 2007
Kamatou, G.P.P.; Viljoen, A.M.; Figueiredo, A.C.; Tilney, P.M.; Van Zyl, R.L.; Barroso, J.G.; Pedro, L.G.; Van Vuuren, S.F., Trichomes, essential oil composition and biological activities of Salvia albanicus Benth. and S. dolomitica Codd, two species from the Cape region of Soith Africa, South African J. Botany, 2007, 73, 1, 102-108, https://doi.org/10.1016/j.sajb.2006.08.001 . [all data]

Liolios, Laouer, et al., 2007
Liolios, C.; Laouer, H.; Boulaacheb, N.; Gortzi, O.; Chinou, I., Chemical Composition and Antimicrobial Activity of the Essential Oil of Algherian Phlomis bovei De Noe subsp. bovei, Molecules, 2007, 12, 4, 772-781, https://doi.org/10.3390/12040772 . [all data]

Moriarity, Bansal, et al., 2007
Moriarity, D.M.; Bansal, A.; Cole, R.A.; Takaku, S.; Haber, W.A.; Setzer, W.N., Selective cytotoxic activities of leaf essential oils from Monteverde Costa Rica, Natural Product Communications, 2007, 2, 12, 1263-1268. [all data]

Moronkola, Ogunwande, et al., 2007
Moronkola, D.O.; Ogunwande, I.A.; Walker, T.M.; Setzer, W.N.; Oyewole, I.O., Identification of the main volatile compounds in the leaf and flower of Tithonia diversifolia (Hemsl) Gray, J. Nat. Med., 2007, 61, 1, 63-66, https://doi.org/10.1007/s11418-006-0019-5 . [all data]

Rodrigues, Antunes, et al., 2007
Rodrigues, F.S.L.M.; Antunes, L.C.S.; Figueiredo, A.C.; Costa, M.M.; Pereira, J.D.S.; Colaço, R.D.R.; Miranda, H.H.S.; Barroso, J.G.; Pedro, L.G.; Scheffer, J.J.C., Composition of the leaf, flower and fruit volatile oils of Pittosporum tobira (Thunb.) W. T. Aiton grown in three locations in Portugal, Flavour Fragr. J., 2007, 22, 4, 311-316, https://doi.org/10.1002/ffj.1798 . [all data]

Setzer, Stokes, et al., 2007
Setzer, W.N.; Stokes, S.L.; Penton, A.F.; Takaku, S.; Haber, W.A.; Hansell, E.; Caffrey, C.R.; McKerrow, J.H., Cruzain inhibitory activity of leaf essential oils of neotropical Lauraceae and essential oil components, Natural Product Communications, 2007, 2, 12, 1203-1210. [all data]

Stokes, Cole, et al., 2007
Stokes, S.L.; Cole, R.A.; Rangelova, M.P.; Haber, W.A.; Setzer, W.N., Cruzain inhibitory activity of the leaf essential oil from an undescribed species of Eugenia from Monteverde, Costa Rica, Natural Product Communications, 2007, 2, 12, 1211-1213. [all data]

Takaku, Haber, et al., 2007
Takaku, S.; Haber, W.A.; Setzer, W.N., Leaf essential oil composition of 10 species of Ocotea (Lauraceae) from Monteverde, Costa Rica, Biochem. Syst. Ecol., 2007, 35, 8, 525-532, https://doi.org/10.1016/j.bse.2007.02.003 . [all data]

Werka, Boehme, et al., 2007
Werka, J.S.; Boehme, A.K.; Setzer, W.N., Biological activities of essential oils from Monteverde, Costa Rica, Natural Product Communications, 2007, 2, 12, 1215-1219. [all data]

Schmidt, Noletto, et al., 2006
Schmidt, J.M.; Noletto, J.A.; Vogler, B.; Setzer, W.N., Abaco Bush Medicine: Chemical composition of the essential oils of four aromatic medicinal plants from Abaco Island, Bahamas, J. Herbs, Spices Medicinal Plants, 2006, 12, 3, 43-65, https://doi.org/10.1300/J044v12n03_04 . [all data]

Butkienë, Nivinskienë, et al., 2005
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Cysne, Canuto, et al., 2005
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Notes

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