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Sulfuric acid, 2TMS derivative


Phase change data

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: Robert L. Brown and Stephen E. Stein

Quantity Value Units Method Reference Comment
Tfus329. - 331.KN/ABuckingham and Donaghy, 1982 
Tfus318. - 319.KN/ABuckingham and Donaghy, 1982 

Reduced pressure boiling point

Tboil (K) Pressure (bar) Reference
391.0.024Buckingham and Donaghy, 1982
363.0.005Buckingham and Donaghy, 1982

Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryUltra-21171.Tuchman, Bowers, et al., 198425. m/0.31 mm/0.52 «mu»m, He, 5. K/min; Tstart: 50. C; Tend: 300. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
PackedSE-301148.Butts and Rainey, 19715. K/min; Tstart: 70. C; Tend: 150. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Buckingham and Donaghy, 1982
Buckingham, J.; Donaghy, S.M., Dictionary of Organic Compounds: Fifth Edition, Chapman and Hall, New York, 1982, 1. [all data]

Tuchman, Bowers, et al., 1984
Tuchman, M.; Bowers, L.D.; Fregien, K.D.; Crippin, P.J.; Krivit, W., Capillary Gas Chromatographic Separation of Urinary Organic Acids. Retention Indices of 101 Urinary Acids on a 5% Phenylmethyl Silicone Capillary Column, J. Chromatogr. Sci., 1984, 22, 5, 198-202, https://doi.org/10.1093/chromsci/22.5.198 . [all data]

Butts and Rainey, 1971
Butts, W.C.; Rainey, W.T., Jr., Gas Chromatography and Mass Spectrometry of the Trimethylsilyl Derivatives of Inorganic Anions, Anal. Chem., 1971, 43, 4, 538-542, https://doi.org/10.1021/ac60299a004 . [all data]


Notes

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