6-Azathymine, bis(trimethylsilyl) ether
- Formula: C10H21N3O2Si2
- Molecular weight: 271.4636
- IUPAC Standard InChI: InChI=1S/C10H21N3O2Si2/c1-8-9(14-16(2,3)4)11-10(13-12-8)15-17(5,6)7/h1-7H3
- IUPAC Standard InChIKey: WFMAXSXEHMITKR-UHFFFAOYSA-N
- CAS Registry Number: 17331-64-5
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 6-Azathymine, TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-101 | 160. | 1459.8 | Miller, Pacáková, et al., 1976 | Ar, AW-DMCS Chromosorb W HP; Column length: 2. m |
| Packed | SE-30 | 150. | 1500. | Pacakova, Miller, et al., 1971 | |
| Packed | OV-101 | 150. | 1500. | Pacakova, Miller, et al., 1971 |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 1467.6 | Tret'yakov, 2007 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Miller, Pacáková, et al., 1976
Miller, V.; Pacáková, V.; Smolková, E.,
Gas-liquid chromatographic analysis of trimethylsilyl derivatives of pyrimidine and purine bases and nucleosides,
J. Chromatogr., 1976, 119, 355-367, https://doi.org/10.1016/S0021-9673(00)86799-0
. [all data]
Pacakova, Miller, et al., 1971
Pacakova, V.; Miller, V.; Cernohorsky, I.J.,
Gas-Liquid Chromatography of Some Pyrimidine Derivatives,
Anal. Biochemistry, 1971, 42, 2, 549-554, https://doi.org/10.1016/0003-2697(71)90071-6
. [all data]
Tret'yakov, 2007
Tret'yakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2007. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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