9H-Fluorene, 2-methyl-
- Formula: C14H12
- Molecular weight: 180.2451
- IUPAC Standard InChI: InChI=1S/C14H12/c1-10-6-7-14-12(8-10)9-11-4-2-3-5-13(11)14/h2-8H,9H2,1H3
- IUPAC Standard InChIKey: RKJHJMAZNPASHY-UHFFFAOYSA-N
- CAS Registry Number: 1430-97-3
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Fluorene, 2-methyl-; 2-Methylfluorene; 2-Methyl-9H-fluorene
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|
| Active phase | OV-1 | OV-1 | SE-52 | SE-52 |
| Column length (m) | 25. | 25. | 33.3 | 65. |
| Carrier gas | He | N2 | ||
| Substrate | ||||
| Column diameter (mm) | 0.2 | 0.2 | 0.50 | 0.3 |
| Phase thickness (μm) | 0.33 | 0.33 | ||
| Tstart (C) | 100. | 100. | 50. | 100. |
| Tend (C) | 180. | 180. | 320. | 300. |
| Heat rate (K/min) | 5. | 5. | 6. | 1.8 |
| Initial hold (min) | 5. | |||
| Final hold (min) | ||||
| I | 1694.8 | 1712.7 | 1673. | 1673. |
| Reference | Zhang, Shen, et al., 2000 | Zhang, Shen, et al., 2000 | Beernaert, 1979 | Carugno and Rossi, 1967 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Zhang, Shen, et al., 2000
Zhang, M.-J.; Shen, S.-D.; Chen, S.-Y.; Sun, Y.-H.,
Analysis of heavy oil fractions in high-temperature coal tar by capillary gas chromatography/fourier transform infrared spectrometry,
Chin. J. Chromatogr., 2000, 18, 3, 241-246. [all data]
Beernaert, 1979
Beernaert, H.,
Gas Chromatographic Analysis of Polyclylic Aromatic Hydrocarbons,
J. Chromatogr., 1979, 173, 1, 109-118, https://doi.org/10.1016/S0021-9673(01)80450-7
. [all data]
Carugno and Rossi, 1967
Carugno, N.; Rossi, S.,
Evaluation of polynuclear hydrocarbons in cigarette smoke by glass capillary columns,
J. Gas Chromatogr., 1967, 5, 2, 103-106, https://doi.org/10.1093/chromsci/5.2.103
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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