2,6-Octadien-1-ol, 3,7-dimethyl-, acetate, (Z)-

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Equity-5MSHP-5MSHP-5HP-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.40.60.50.
Tend (C) 250.250.250.240.220.
Heat rate (K/min) 3.2.5.4.5.
Initial hold (min)  8.1.2.10.
Final hold (min) 10.30.10.  
I 1358.1367.1364.1366.1365.
ReferenceBelsito E.L., Carbone C., et al., 2007Benkaci-Ali, Baaliouamer, et al., 2007Benzo, Gilardoni, et al., 2007Dehghan, Solaimanian, et al., 2007Flamini, Tebano, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5RTX-1RTX-1Equity-5
Column length (m) 30.30.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.220.220.25
Phase thickness (μm) 0.250.50.250.251.
Tstart (C) 60.40.60.60.40.
Tend (C) 246.265.230.230.260.
Heat rate (K/min) 3.7.2.2.5.
Initial hold (min)     1.
Final hold (min)  5.35.35.15.
I 1381.1365.1342.1342.1386.
ReferenceHongratanaworakit and Buchbauer, 2007Mahattanatawee K., Perez-Cacho P.R., et al., 2007Paolini J., Costa J., et al., 2007Paolini, Muselli, et al., 2007Rocha, Coelho, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RTX-1DB-1SPB-1HP-5MS
Column length (m) 50.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.250.20.25
Phase thickness (μm) 0.250.250.250.20.25
Tstart (C) 60.60.50.70.60.
Tend (C) 220.230.265.220.280.
Heat rate (K/min) 2.2.2.53.4.
Initial hold (min)     5.
Final hold (min) 20.35. 15. 
I 1340.1342.1340.1342.1364.
ReferenceGonny, Cavaleiro, et al., 2006Paolini J., Desjobert J.M., et al., 2006Ramezani, Behravan, et al., 2006Salgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5RTX-1MDN-5DB-1
Column length (m) 30.30.60.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.50.40.
Tend (C) 250.250.220.250.250.
Heat rate (K/min) 5.5.2.3.3.
Initial hold (min) 2.2.   
Final hold (min)   20. 20.
I 1362.1362.1342.1355.1344.
ReferenceSu, Ho, et al., 2006Su, Ho, et al., 2006, 2Cozzani, Muselli, et al., 2005Dugo, Mondello, et al., 2005Fanciullino, Gancel, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1HP-5RTX-1HP-5MS
Column length (m) 50.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.50.60.60.
Tend (C) 220.250.250.230.250.
Heat rate (K/min) 2.3.4.2.4.
Initial hold (min)   5. 2.
Final hold (min) 20.20.15.35.20.
I 1344.1340.1357.1342.1365.
ReferenceFerrari, Tomi, et al., 2005Gancel, Ollitrault, et al., 2005Mahattanatawee, Goodner, et al., 2005Paolini, Costa, et al., 2005Pino, Mesa, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSMega 5MSRTX-5DB-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.45.60.60.
Tend (C) 200.240.300.240.240.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min)  2.6.  
Final hold (min) 10. 10.  
I 1365.1360.1364.1361.1361.
ReferenceSmadja, Rondeau, et al., 2005Verzera, Trozzi, et al., 2005Dugo, Mondello, et al., 2004Flamini, Cioni, et al., 2004Flamini, Cioni, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1BP-1DB-5BP-1BP-1
Column length (m) 30.30.30.50.50.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.320.250.220.22
Phase thickness (μm) 0.20.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 220.220.240.230.230.
Heat rate (K/min) 3.5.3.2.2.
Initial hold (min)      
Final hold (min) 15.13.30.35.35.
I 1342.1334.1365.1345.1345.
ReferenceMoldão-Martins, Beirão-da-Costa, et al., 2004Raina, Kumar, et al., 2004Bader, Caponi, et al., 2003Bianchini, Tomi, et al., 2003Bianchini, Tomi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-5DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas  He HeN2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.50.250.25
Tstart (C) 35.40.40.75.75.
Tend (C) 225.250.265.230.230.
Heat rate (K/min) 4.3.7.3.3.
Initial hold (min) 10.  10.10.
Final hold (min)  20.5.20. 
I 1345.1340.1376.1367.1365.
ReferenceChisholm, Wilson, et al., 2003Gancel, Ollitrault, et al., 2003Högnadóttir and Rouseff, 2003Jantan, Ling, et al., 2003bin Jantan, Yassin, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Mega 5MSDB-5DB-5BP-1RTX-5
Column length (m) 30.30.30.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.70.60.60.45.
Tend (C) 240.230.260.220.300.
Heat rate (K/min) 3.4.4.2.3.
Initial hold (min) 2.2.  6.
Final hold (min)  20. 20.10.
I 1360.1367.1365.1340.1366.
ReferenceVerzera, Trozzi, et al., 2003Choi, Kim. M.-S.L., et al., 2002Javidnia, Miri, et al., 2002Lota, de Rocca Serra, et al., 2002Mondello, Zappia, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1HP-5RTX-5RTX-5
Column length (m) 25.50.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.45.45.
Tend (C) 280.220.280.250.250.
Heat rate (K/min) 4.2.3.3.3.
Initial hold (min) 6.  6.6.
Final hold (min)  20.   
I 1341.1341.1339.1356.1371.
ReferencePino, Marbot, et al., 2002Pintore, Usai, et al., 2002Pitarokili, Couladis, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5BP-1SPB-1RTX-5 MSSE-30
Column length (m) 30.50.15.30.25.
Carrier gas HeHe HeN2
Substrate      
Column diameter (mm) 0.250.220.250.250.20
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.35.70.60.
Tend (C) 280.230.225.210.180.
Heat rate (K/min) 3.2.6.4.3.
Initial hold (min) 5. 3.10.10.
Final hold (min)  35.10.10.1.
I 1364.1345.1342.1369.1365.
ReferenceAligiannis, Kalpoutzakis, et al., 2001Bianchini, Tomi, et al., 2001Chisholm, Wilson, et al., 2001Hudaib, Grazia Bellardi, et al., 2001bin Jantan, Basni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1HP-5BP-1RTX-5
Column length (m) 50.50.30.50.10.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.200.220.1
Phase thickness (μm) 0.250.250.250.250.1
Tstart (C) 60.60.60.60.50.
Tend (C) 220.220.180.230.350.
Heat rate (K/min) 2.2.4.2.12.3
Initial hold (min)   8.  
Final hold (min)   2.35. 
I 1340.1340.1365.1340.1370.
ReferenceLota, Serra, et al., 2001Lota, Serra, et al., 2001Alonzo, Bosco, et al., 2000Lota, de Rocca Serra, et al., 2000Mondello, Zappia, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Mega 5MSMega 5MSBP-1BP-1
Column length (m) 30.30.30.50.50.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.40.40.60.60.
Tend (C) 230.240.240.230.230.
Heat rate (K/min) 2.3.3.2.2.
Initial hold (min)  2.2.  
Final hold (min)    35.35.
I 1364.1360.1360.1340.1340.
ReferenceSong, Sawamura, et al., 2000Verzera, la Rosa, et al., 2000Verzera, Trozzi, et al., 2000Lota, Serra, et al., 1999Lota, Serra, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5BP-1DB-5Methyl Silicone
Column length (m) 60.30.50.30.25.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.220.320.2
Phase thickness (μm) 0.250.250.25 0.3
Tstart (C) 50.50.60.80.40.
Tend (C) 250.250.230.200.200.
Heat rate (K/min) 2.53.2.2.2.
Initial hold (min) 5.    
Final hold (min)   35.30. 
I 1326.1364.1342.1359.1352.
ReferenceStashenko, Cervantes, et al., 1999Isidorov, Zenkevich, et al., 1998Mariotti, Costa, et al., 1997Vahirua-Lechat, Menut, et al., 1996Píry, Príbela, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101DB-5OV-101OV-1
Column length (m) 50.50.60.50.30.
Carrier gas N2N2HeH2He
Substrate      
Column diameter (mm) 0.250.250.320.320.5
Phase thickness (μm)   1. 0.8
Tstart (C) 80.80.40.50.40.
Tend (C) 200.200.220.200.220.
Heat rate (K/min) 2.2.3.2.2.
Initial hold (min)      
Final hold (min)      
I 1341.1344.1363.1341.1341.
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Le Quere and Latrasse, 1990Pieribattesti, Smadja, et al., 1988De Pooter, Omar, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-1
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm) 0.5
Phase thickness (μm) 0.8
Tstart (C) 40.
Tend (C) 220.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 1342.
ReferenceDe Pooter, Omar, et al., 1985
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References