Isoborneol


Phase change data

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: William E. Acree, Jr., James S. Chickos

Enthalpy of sublimation

ΔsubH (kcal/mol) Temperature (K) Method Reference Comment
9.82388.AStephenson and Malanowski, 1987Based on data from 373. to 457. K. See also Grekhnev, 1936.

Gas Chromatography

Go To: Top, Phase change data, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30100.1154.6Tudor, 199740. m/0.35 mm/0.35 μm

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-11140.Srivastava, Srivastava, et al., 200630. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 3. min; Tstart: 60. C
CapillaryHP-5MS1160.Baranauskiene, Venskutonis, et al., 200330. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 4. K/min, 280. C @ 10. min
CapillaryHP-5MS1146.Couladis, Chinou, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryBP-11158.Raina, Lal, et al., 200260. m/0.32 mm/0.25 μm, N2, 5. K/min; Tstart: 60. C; Tend: 220. C
CapillaryBP-11159.Raina, Srivastava, et al., 200225. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryBP-11148.Raina, Srivastava, et al., 2002, 225. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryBP-11144.Shawl, Srivastava, et al., 200230. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 13. min; Tstart: 60. C
CapillaryDB-11154.Nagalakshmi, Thangadurai, et al., 200128. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 4.5 K/min; Tend: 270. C
CapillaryDB-51156.Adams, 200030. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryBP-11188.Vera and Chane-Ming, 199950. m/0.25 mm/0.25 μm, 2. K/min; Tstart: 60. C; Tend: 260. C
CapillaryOV-1011156.Menut, Molangui, et al., 1995N2, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 200. C
CapillaryBP-11152.Ekundayo, Laakso, et al., 1988H2, 65. C @ 2. min, 5. K/min; Column length: 50. m; Column diameter: 0.33 mm; Tend: 220. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCP Sil 8 CB1169.Radusiene, Judzentiene, et al., 200550. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C
CapillaryBP-11142.Raina, Srivastava, et al., 200325. m/0.32 mm/0.25 μm, N2; Program: 60C => 5C/min => 220C(5min) => 3C/min => 245C(5min)

Kovats' RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M1656.Vera and Chane-Ming, 199950. m/0.32 mm/0.2 μm, 2. K/min; Tstart: 60. C; Tend: 260. C
CapillaryCarbowax 20M1660.Vera and Chane-Ming, 199950. m/0.32 mm/0.2 μm, 2. K/min; Tstart: 60. C; Tend: 260. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryZB-51155.Simoniatto, Bonani, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5MS1162.5Zeng, Zhao, et al., 200730. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 80. C; Tend: 300. C
CapillaryDB-51161.Batista-Pereira, Fernandes, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryBP-11146.Bousmaha, Boti, et al., 200650. m/0.25 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillarySPB-11174.Radulovic, Mananjarasoa, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryHP-5MS1159.Vujisic L., Vuckovic I., et al., 200630. m/0.25 mm/0.25 μm, H2, 4.3 K/min; Tstart: 50. C; Tend: 285. C
CapillarySPB-11175.Boskovic, Radulovic, et al., 200530. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryDB-51148.Boskovic, Radulovic, et al., 200530. m/0.2 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryDB-11134.Dob, Dahmane, et al., 200530. m/0.32 mm/0.25 μm, 50. C @ 8. min, 2. K/min; Tend: 250. C
CapillarySE-541156.Simionatto, Porto, et al., 200525. m/0.25 mm/0.2 μm, H2, 4. K/min; Tstart: 50. C; Tend: 250. C
CapillarySPB-11144.Cavaleiro, Salgueiro, et al., 200430. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryDB-5MS1164.Mardarowicz, Wianowska, et al., 200430. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min; Tend: 280. C
CapillarySPB-11145.Cavaleiro, Salgueiro, et al., 200330. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryDB-51153.bin Jantan, Yassin, et al., 200330. m/0.25 mm/0.25 μm, N2, 75. C @ 10. min, 3. K/min; Tend: 230. C
CapillaryDB-11130.7Sun and Stremple, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 325. C
CapillaryRTX-51158.Mondello, Zappia, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min, 300. C @ 10. min
CapillaryCP Sil 5 CB1139.Pino, Marbot, et al., 200225. m/0.25 mm/0.25 μm, N2, 60. C @ 6. min, 4. K/min; Tend: 280. C
CapillaryCP Sil 5 CB1138.Pino, Marbot, et al., 2002, 250. m/0.32 mm/0.4 μm, He, 60. C @ 10. min, 3. K/min, 280. C @ 60. min
CapillaryRTX-51156.Shellie, Mondello, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min; Tend: 250. C
CapillaryRTX-51159.Shellie, Mondello, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min; Tend: 250. C
CapillaryHP-51154.Couladis, Tsortanidou, et al., 200130. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 380. C
CapillarySE-301153.bin Jantan, Basni, et al., 2001N2, 60. C @ 10. min, 3. K/min, 180. C @ 1. min; Column length: 25. m; Column diameter: 0.20 mm
CapillaryBP-11142.Rezzi, Cavaleiro, et al., 200150. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-51153.Bartley and Jacobs, 200060. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryOV-11131.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 μm, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryDB-51156.Isidorov, Zenkevich, et al., 199830. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryBP-11145.Mariotti, Tomi, et al., 199750. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryMethyl Silicone1159.Píry, Príbela, et al., 199525. m/0.2 mm/0.3 μm, He, 2. K/min; Tstart: 40. C; Tend: 200. C
CapillaryCP Sil 5 CB1137.Chanegriha and Baaliouamer, 199325. m/0.22 mm/0.11 μm, He, 80. C @ 8. min, 1. K/min, 230. C @ 16. min

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBPX-51181.Cardeal, da Silva, et al., 200630. m/0.25 mm/0.25 μm; Program: 35C(5min) => 3C/min => 210C => 40C/min => 240C (4min)
CapillaryCP Sil 5 CB1157.Chanegriha, Baaliouamer, et al., 1998Program: not specified
CapillarySE-521160.Mondello, Dugo, et al., 199560. m/0.32 mm/0.40 μm, He; Program: 45 C (6 min) 3 C/min -> 111 0C 2 C/min -> 160 C 3 C/min -> 300 C (15 min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-201664.Bousmaha, Boti, et al., 200650. m/0.25 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillarySupelcowax-101665.Cavaleiro, Salgueiro, et al., 200430. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryRTX-Wax1642.Mondello, Zappia, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min, 250. C @ 10. min
CapillaryAT-Wax1633.Pino, Marbot, et al., 2002, 260. m/0.32 mm/0.25 μm, He, 65. C @ 10. min, 2. K/min, 250. C @ 60. min
CapillaryDB-Wax1670.Bartley and Jacobs, 200060. m/0.5 mm/0.32 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryCarbowax 20M1672.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 μm, H2, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryBP-201671.Mariotti, Tomi, et al., 199750. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryCarbowax 20M1659.Mondello, Dugo, et al., 199560. m/0.32 mm/0.425 μm, He, 45. C @ 3. min, 3. K/min, 300. C @ 20. min
CapillaryCarbowax 20M1660.Píry, Príbela, et al., 199550. m/0.2 mm/0.2 μm, He, 30. C @ 2. min, 4. K/min, 170. C @ 20. min
CapillaryDB-Wax1672.Humpf and Schreier, 199130. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 4. K/min, 220. C @ 20. min

Van Den Dool and Kratz RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-201660.Chanegriha, Baaliouamer, et al., 1998He; Program: not specified
CapillaryCarbowax 20M1696.Whitfield, Shea, et al., 1981Column length: 150. m; Column diameter: 0.75 mm; Program: not specified

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51157.Georgiou, Koutsaviti, et al., 201030. m/0.32 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-5 MS1196.Mesa-Arango, Betancur-Galvis, et al., 201060. m/0.25 mm/0.25 μm, Helium, 40. C @ 15. min, 5. K/min, 250. C @ 15. min
CapillaryBP-11144.Mishra, Chaudhary, et al., 2010Nitrogen, 60. C @ 10. min, 5. K/min, 220. C @ 30. min
CapillaryDB-51162.Alim, Goze, et al., 200930. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51163.Scrivanti, Anton, et al., 200930. m/0.25 mm/0.25 μm, Nitrogen, 2. K/min; Tstart: 40. C; Tend: 230. C
CapillaryHP-51152.Bousaada, Ammar, et al., 200830. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 1. min, 5. K/min, 280. C @ 1. min
CapillaryUltra 21151.Byun and Shin, 200850. m/0.20 mm/0.11 μm, Helium, 60. C @ 5. min, 2. K/min, 230. C @ 30. min
CapillaryElite-11160.Raj, Baby, et al., 200830. m/0.32 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryHP-5MS1160.Basta, Pavlovic, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51149.Bos, Woerdenbag, et al., 200730. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51149.Elfami, Bos, et al., 200730. m/0.26 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryCol-Elite 5MS1166.Gudaityte and Venskutonis R.P., 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 30. C; Tend: 246. C
CapillarySPB-11145.Pinto, Salgueiro, et al., 200730. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryHP-51142.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-51146.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryDB-51149.Elfami, Komar, et al., 200630. m/0.26 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 290. C
CapillaryHP-11137.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.33 μm, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryHP-5 MS1145.Marzouk, Mansour, et al., 200630. m/0.25 mm/0.25 μm, Nitrogen, 5. K/min, 280. C @ 5. min; Tstart: 50. C
CapillaryHP-51145.Marzouk, Neffati, et al., 200630. m/0.25 mm/0.52 μm, N2, 5. K/min, 280. C @ 5. min; Tstart: 50. C
CapillaryCP-Sil 5 CB1145.Olawore, Usman, et al., 200625. m/0.25 mm/0.15 μm, Hydrogen, 3. K/min; Tstart: 50. C; Tend: 230. C
CapillaryDB-51158.Ozel, Gogus, et al., 200630. m/0.32 mm/0.25 μm, He, 60. C @ 0.5 min, 5. K/min, 280. C @ 2. min
CapillarySPB-51156.Stojanovic, Palic, et al., 2006He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min
CapillaryHP-51172.Wang, Yang, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 10. K/min, 250. C @ 10. min
CapillarySPB-11130.Wong, Sivasothy, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 4. K/min, 250. C @ 10. min
CapillaryDB-11160.Facundo, Pinto, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 5. K/min, 250. C @ 15. min
CapillaryDB-51151.de Oliveira, Dias, et al., 2005He, 40. C @ 1. min, 4. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 220. C
CapillaryMethyl Silicone1157.Ricci, Fraternale, et al., 200512.5 m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 270. C
CapillaryHP-5MS1158.Setzer, Noletto, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-5MS1163.Shams-Ardakani, Ghannadi, et al., 200530. m/0.25 mm/0.25 μm, He, 15. K/min; Tstart: 60. C; Tend: 275. C
CapillaryZB-51179.Jürgens and Dötterl, 200460. m/0.25 mm/0.25 μm, He, 40. C @ 4.6 min, 6. K/min, 260. C @ 1. min
CapillaryDB-51156.Kalvandi, Sefidkon, et al., 200460. m/0.25 mm/0.25 μm, He, 40. C @ 4. min, 4. K/min; Tend: 280. C
CapillaryDB-51155.Tellez, Khan, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-5HT1156.Yusufoglu, Celik, et al., 2004He, 50. C @ 2. min, 2. K/min, 250. C @ 20. min; Column length: 27. m; Column diameter: 0.25 mm
CapillaryMethyl Silicone1149.Curini, Bianchi, et al., 2003He, 4. K/min; Column length: 12.5 m; Column diameter: 0.25 mm; Tstart: 50. C; Tend: 270. C
CapillaryRSL-2001141.Jirovetz, Buchbauer, et al., 200330. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-11151.Mahalwal and Ali, 200330. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 80. C; Tend: 250. C
CapillaryDB-51156.Pino, Marbot, et al., 200330. m/0.25 mm/0.25 μm, H2, 60. C @ 10. min, 4. K/min, 280. C @ 40. min
CapillaryBP-11146.Das, Ram, et al., 200225. m/0.50 mm/0.25 μm, N2, 5. K/min, 220. C @ 10. min; Tstart: 60. C
CapillaryRSL-2001158.Jirovetz, Buchbauer, et al., 200230. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryOV-1011146.Orav, Kailas, et al., 200250. m/0.2 mm/0.5 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryZEBRON-51158.Öztürk, Akay, et al., 20026. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min, 200. C @ 15. min
CapillarySPB-51157.Cornu, Carnat, et al., 2001He, 40. C @ 5. min, 3. K/min, 220. C @ 15. min; Column length: 60. m; Column diameter: 0.32 mm
CapillaryHP-51162.Lis-Balchin and Roth, 2000He, 9. K/min, 200. C @ 10. min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 80. C
CapillaryDB-51156.Mitiku, Sawamura, et al., 200030. m/0.22 mm/0.25 μm, N2, 70. C @ 2. min, 4. K/min, 230. C @ 20. min
CapillaryOV-1011146.Menon, Chacko, et al., 1999N2, 1. K/min, 200. C @ 20. min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 80. C
CapillaryCP Sil 5 CB1132.Bos, Woerdenbag, et al., 199725. m/0.25 mm/0.25 μm, He, 6. K/min; Tstart: 60. C; Tend: 300. C
CapillaryDB-51158.Tellez, Estell, et al., 199730. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-11157.Nishimura, 199560. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 80. C; Tend: 210. C
CapillaryDB-11157.Tirado, Stashenko, et al., 199560. m/0.25 mm/0.25 μm, He, 70. C @ 5. min, 2.5 K/min; Tend: 270. C
CapillaryDB-11138.Habu, Flath, et al., 19853. K/min; Column length: 50. m; Column diameter: 0.32 mm; Tstart: 0. C; Tend: 250. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCBP-51160.de Morais, Oliveira, et al., 201230. m/0.25 mm/0.25 μm, Helium; Program: 60 0C 3 0C/min -> 240 0C 10 0C/min -> 280 0C (10 min)
Capillary5 % Phenyl polydimethyl siloxane1157.Chaverri, Diaz, et al., 2011Program: not specified
CapillaryHP-5 MS1158.Payo, Colo, et al., 2011Program: not specified
CapillaryHP-5 MS1160.Payo, Colo, et al., 2011Program: not specified
CapillaryOptima-5MS1153.HEuskin, Godin, et al., 200930. m/0.32 mm/0.25 μm, Helium; Program: 40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)
CapillaryCB-11151.Kannaste, Vongvanich, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)
CapillaryCB-11142.Kannaste, Vongvanich, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryElite-11162.Raj, Baby, et al., 200830. m/0.32 mm/0.25 μm, Helium; Program: not specified
CapillaryCP Sil 8 CB1169.Radusiene, Judzentiene, et al., 200750. m/0.32 mm/0.25 μm, Helium; Program: 60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min)
CapillaryHP-5MS1163.Yu, Huang, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 40C(3min) => 6C/min => 160C => 10C/min => 300C (10min)
CapillaryCP Sil 8 CB1162.Judzentiene and Buzelyte, 200650. m/0.32 mm/0.25 μm, He; Program: 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)
CapillaryBPX-51156.Judzentiene and Mockute, 200530. m/0.25 mm/0.25 μm; Program: 60C(0.2min) => 3K/min => 186C => 10C/min => 240C (5min)
CapillaryDB-51156.de Oliveira, Dias, et al., 2005He; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryHP-11153.Carpino, Mallia, et al., 200412. m/0.32 mm/0.52 μm; Program: 35C(3min) => 6C/min => 190C => 30C/min => 225C
CapillarySE-301150.Vinogradov, 2004Program: not specified
CapillaryCP-Sil 8CB-MS1156.Mockute, Bernotiene, et al., 2003Column length: 50. m; Column diameter: 0.32 mm; Program: 60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C
CapillarySE-301150.Li, Wu, et al., 2002He; Column length: 60. m; Column diameter: 0.25 mm; Program: 50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0C
CapillarySE-301150.Li, Wu, et al., 2002He; Column length: 60. m; Column diameter: 0.25 mm; Program: not specified
CapillaryOV-11155.Kökdil, 199850. m/0.32 mm/0.25 μm, He; Program: 1)50C(1min) => 4C/min => 180C => 2C/min => 250C(10min) 2)50C(1min) => 6C/min => 200C => 12C/min => 250C(5min)
CapillaryDB-51156.Isidorov, Zenkevich, et al., 1997Program: not specified
CapillaryPolydimethyl siloxanes1150.Zenkevich, 1997Program: not specified
CapillaryDB-11132.Barroso, Figueiredo, et al., 199630. m/0.25 mm/0.25 μm, H2; Program: 45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min)
Capillary5 % Phenyl methyl siloxane1155.Sagrero-Nieves and Bartley, 1995Program: not specified
CapillaryOV-1011157.Shibamoto, 1987Program: not specified
CapillaryOV-1011141.Zenkevich and Malamakhov, 1987He; Column length: 50. m; Column diameter: 0.24 mm; Program: not specified
CapillaryOV-1011157.Zenkevich and Malamakhov, 1987He; Column length: 50. m; Column diameter: 0.24 mm; Program: not specified
PackedOV-1011149.Swigar and Silverstein, 1981N2, Chromosorb G 60-80mesh DMCS; Column length: 2.5 m; Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-Innowax1698.Feng, Cui, et al., 201160. m/0.25 mm/0.25 μm, Helium, 60. C @ 1. min, 5. K/min, 220. C @ 5. min
CapillaryBP-201682.Mishra, Chaudhary, et al., 2010Nitrogen, 5. K/min; Tstart: 60. C; Tend: 200. C
CapillaryHP-Innowax1642.Bousaada, Ammar, et al., 200830. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 1. min, 5. K/min, 280. C @ 1. min
CapillarySupelcowax-101665.Pinto, Salgueiro, et al., 200730. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryInnowax1642.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryInnowax1652.Abdelwahed, Hayder, et al., 200630. m/0.25 mm/0.25 μm, N2, 50. C @ 3. min, 9. K/min, 280. C @ 3. min
CapillaryHP-Wax1642.Marzouk, Mansour, et al., 200630. m/0.25 mm/0.25 μm, Nitrogen, 5. K/min, 280. C @ 5. min; Tstart: 50. C
CapillaryHP-20M1642.Marzouk, Neffati, et al., 200630. m/0.25 mm/0.25 μm, N2, 5. K/min, 250. C @ 10. min; Tstart: 50. C
CapillarySupelcowax-101660.Wong, Sivasothy, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 1. min, 4. K/min, 250. C @ 10. min
CapillaryCarbowax 20M1649.Fernandez, Lizzani-Cuvelier, et al., 200550. m/0.2 mm/0.25 μm, 60. C @ 60. min, 2. K/min; Tend: 250. C
CapillaryHP-Innowax1664.Ong and Acree, 19984. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 35. C; Tend: 250. C
PackedCarbowax 20M1678.Stancher and Pertoldi, 1967Hydrogen, Gas-Chrom Z (80-100 mesh), 4. K/min; Column length: 2. m; Tstart: 65. C; Tend: 220. C
PackedCarbowax 20M1680.Stancher and Pertoldi, 1967Hydrogen, Gas-Chrom Z (80-100 mesh), 4. K/min; Column length: 2. m; Tstart: 65. C; Tend: 220. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax1669.Gyawali and Kim, 201260. m/0.20 mm/0.25 μm, Helium; Program: 40 0C (3 min) 2 0C/min -> 150 0C 4 0C/min -> 220 0C (20 min) 5 0C/min -> 230 0C
CapillaryHP-Innowax1664.Feng, Cui, et al., 201160. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryCarbowax 20M1660.Vinogradov, 2004Program: not specified
CapillaryHP-Innowax1682.Tabanca, Kirimer, et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryFFAP1655.Reddy, Angers, et al., 199825. m/0.2 mm/0.33 μm, H2; Program: 40C(5min) => 4C/min => 170C => 8C/min => 240C (12min)
CapillaryCarbowax 20M1654.Tirado, Stashenko, et al., 199560. m/0.25 mm/0.25 μm, He; Program: not specified
CapillaryCarbowax 20M1660.Chanegriha and Baaliouamer, 1993He; Program: not specified
CapillaryCarbowax 20M1660.Shibamoto, 1987Program: not specified

References

Go To: Top, Phase change data, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Chanegriha, N.; Baaliouamer, A.; Rolando, C., Polarity changes during capillary gas chromatographic and gas chromatographic-mass spectrometric analysis using serially coupled columns of different natures and temperature programming. Application to the identification of constituents of essential oils, J. Chromatogr. A, 1998, 819, 1-2, 61-65, https://doi.org/10.1016/S0021-9673(98)00449-X . [all data]

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Mondello, L.; Dugo, P.; Basile, A.; Dugo, G., Interactive use of linear retention indices, on polar and apolar columns, with a MS-library for reliable identification of complex mixtures, J. Microcolumn Sep., 1995, 7, 6, 581-591, https://doi.org/10.1002/mcs.1220070605 . [all data]

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Humpf, H.-U.; Schreier, P., Bound aroma compounds from the fruit and the leaves of blackberry (Rubus laciniata L.), J. Agric. Food Chem., 1991, 39, 10, 1830-1832, https://doi.org/10.1021/jf00010a028 . [all data]

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Georgiou, C.; Koutsaviti, A.; Bazos, I.; Tzakou, O., Chemical composition of Echinophora tenuifolia subsp. sibthorpiana essential oil from Greece, Rec. Nat. Prod., 2010, 4, 3, 167-170. [all data]

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Mesa-Arango, A.C.; Betancur-Galvis, L.; Montiel, J.; Bueno, J.G.; Baena, A.; Duran, D.C.; Martinez, J.R.; Stashenko, E.E., Antifungal activity and chemical composition of the essential oils of Lippia alba (Miller) N.E. Brown grown in different regions of Colombia, J. Essential Oil Res., 2010, 22, 6, 568-574, https://doi.org/10.1080/10412905.2010.9700402 . [all data]

Mishra, Chaudhary, et al., 2010
Mishra, R.K.; Chaudhary, S.; Pandey, R.; Gupta, S.; Mallavarapu, G.R.; Kumar, S., Analysis of linalool content in the inflorescence (flower) essential oil and leaf oil of Lippia alba cultivar Kavach, J. Essen. Oil Res., 2010, 22, 1, 3-7, https://doi.org/10.1080/10412905.2010.9700253 . [all data]

Alim, Goze, et al., 2009
Alim, A.; Goze, I.; Cetin, A.; Atas, A.; Vural, N.; Donmez, E., Antimicrobial activity of the essential oil of Cyclotrichimun niveum (Boiss.) Manden. Et Scheng, African J. Microbiol. Res., 2009, 3, 8, 422-425. [all data]

Scrivanti, Anton, et al., 2009
Scrivanti, L.R.; Anton, A.M.; Zygadlo, J.A., Essential oil conposition of Bothriochloa Kuntze (Poaceae) from South America and their chemotaxonomy, Biochem. Systematics Ecol., 2009, 37, 3, 206-213, https://doi.org/10.1016/j.bse.2009.03.009 . [all data]

Bousaada, Ammar, et al., 2008
Bousaada, O.; Ammar, S.; Saidana, D.; Chriaa, J.; Chraif, I.; Daami, M.; Helal, A.N.; Mighri, Z., Chemical composition and antimicrobial activity of volatile components from capitula and aerial parts of Rhaponticum acaule DC growing wild in Tunisia, Microbiol. Res., 2008, 163, 1, 87-95, https://doi.org/10.1016/j.micres.2007.02.010 . [all data]

Byun and Shin, 2008
Byun, Y.; Shin, S., Analysis of compounds and activity of essential oil from Chrysanthemum zawadskii var. latilobum and C. indicum agaunst antibiotic-resistant pathogenic bacteria, Nat. Prod. Sci., 2008, 14, 2, 138-142. [all data]

Raj, Baby, et al., 2008
Raj, G.; Baby, S.; Dan, M.; Thaha, A.R.M.; Sethuraman, M.G.; George, V., Volatile constituents from the rhisomes of Curcuma haritha Mangaly and Sabu from Sauthern India, Flavour Fragr. J., 2008, 23, 5, 348-352, https://doi.org/10.1002/ffj.1891 . [all data]

Basta, Pavlovic, et al., 2007
Basta, A.; Pavlovic, M.; Couladis, M.; Tzakou, O., Essential oil composition of the flowerheads of Chrysanthemum coronarium L. from Greece, Flavour Fragr. J., 2007, 22, 3, 197-200, https://doi.org/10.1002/ffj.1781 . [all data]

Bos, Woerdenbag, et al., 2007
Bos, R.; Woerdenbag, H.J.; Kayser, O.; Quax, W.J.; Ruslan, K.; Elfami, Essential oil constituents of Piper cubeba L. fils. from Indonesia, J. Essent. Oil Res., 2007, 19, 1, 14-17, https://doi.org/10.1080/10412905.2007.9699217 . [all data]

Elfami, Bos, et al., 2007
Elfami; Bos, R.; Ruslan, K.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential Oil Constituents of Piper cubeba from Indonesia, 2007, 53-60. [all data]

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Notes

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