Pyrazine, 2,5-dimethyl-
- Formula: C6H8N2
- Molecular weight: 108.1411
- IUPAC Standard InChIKey: LCZUOKDVTBMCMX-UHFFFAOYSA-N
- CAS Registry Number: 123-32-0
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 2,5-Dimethylpyrazine
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Normal alkane RI, polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-FFAP | HP-Innowax | FFAP | DB-Wax | CP-Wax |
Column length (m) | 25. | 15. | 30. | 60. | 60. |
Carrier gas | Helium | Helium | Nitrogen | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.50 | 0.50 | 0.50 | 0.50 | 0.25 |
Tstart (C) | 45. | 40. | 35. | 40. | 50. |
Tend (C) | 220. | 250. | 250. | 210. | 230. |
Heat rate (K/min) | 15. | 3. | 4. | 2. | 6. |
Initial hold (min) | 5. | 5. | 2. | ||
Final hold (min) | 45. | 70. | 15. | ||
I | 1339. | 1319. | 1330. | 1348. | 1337. |
Reference | Wanakhachornkrai and Lertsiri, 9999 | Puvipirom and Chaisei, 2012 | Budryn, Nebesny, et al., 2011 | Moon and Shibamoto, 2010 | Mo, Fan, et al., 2009 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | HP-Innowax | ZB-Wax | DB-Wax | Stabilwax |
Column length (m) | 60. | 50. | 60. | 30. | 60. |
Carrier gas | Helium | Helium | Helium | He | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.20 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.50 | 0.33 | 0.50 | 0.25 | 0.25 |
Tstart (C) | 40. | 50. | 40. | 50. | 40. |
Tend (C) | 210. | 250. | 220. | 230. | 240. |
Heat rate (K/min) | 2. | 10. | 4. | 4. | 3. |
Initial hold (min) | 5. | 5. | 5. | ||
Final hold (min) | 70. | 6. | 5. | 15. | 10. |
I | 1346. | 1308. | 1357. | 1321. | 1303. |
Reference | Moon and Shibamoto, 2009 | Du, Clery, et al., 2008 | Marin, Pozrl, et al., 2008 | Characterization of Pyrazines in Some Chinese Liquors and Their Approximate Concentrations, 2007 | Cros, Vandanjon, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | FFAP | DB-Wax | DB-Wax | TC-Wax | ZB-Wax |
Column length (m) | 30. | 60. | 30. | 60. | 30. |
Carrier gas | N2 | He | He | N2 | Helium |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | |
Tstart (C) | 35. | 50. | 60. | 70. | 40. |
Tend (C) | 320. | 200. | 180. | 220. | 250. |
Heat rate (K/min) | 4. | 2. | 2. | 3. | 5. |
Initial hold (min) | 5. | 5. | 2. | ||
Final hold (min) | 45. | 90. | 30. | 40. | 5. |
I | 1330. | 1302. | 1326. | 1338. | 1310. |
Reference | Nebesny, Budryn, et al., 2007 | Fujioka and Shibamoto, 2006 | Osada and Shibamoto, 2006 | Ishizaki, Tachihara, et al., 2005 | N/A |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | TC-Wax | DB-Wax | Stabilwax | DB-Wax | DB-Wax |
Column length (m) | 60. | 30. | 60. | 30. | 30. |
Carrier gas | He | He | Helium | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | 0.25 |
Tstart (C) | 40. | 50. | 40. | 30. | 30. |
Tend (C) | 230. | 180. | 240. | 250. | 250. |
Heat rate (K/min) | 3. | 3. | 3. | 4. | 4. |
Initial hold (min) | 8. | 5. | 1. | 1. | |
Final hold (min) | 40. | 10. | |||
I | 1332. | 1333. | 1303. | 1318. | 1321. |
Reference | Ishikawa, Ito, et al., 2004 | Yanagimoto, Ochi, et al., 2004 | Cros, Vandanjon, et al., 2003 | Tanaka, Yamauchi, et al., 2003 | Tanaka, Yamauchi, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-FFAP | DB-Wax | HP-FFAP | HP-Wax | DB-Wax |
Column length (m) | 25. | 60. | 25. | 60. | 60. |
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | 0.25 | 0.32 |
Phase thickness (μm) | 0.5 | 0.52 | 0.5 | 0.25 | |
Tstart (C) | 45. | 60. | 60. | 40. | 50. |
Tend (C) | 220. | 180. | 240. | 190. | 210. |
Heat rate (K/min) | 15. | 3. | 5. | 3. | 1.5 |
Initial hold (min) | 4. | 1. | 6. | 5. | |
Final hold (min) | 5. | 10. | |||
I | 1339. | 1331. | 1303. | 1347. | 1335. |
Reference | Wanakhachornkrai and Lertsiri, 2003 | Ito, Sugimoto, et al., 2002 | Qian and Reineccius, 2002 | Sanz, Maeztu, et al., 2002 | Chyau and Mau, 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-Wax | HP-Wax | DB-Wax | DB-Wax | CP-Wax 52CB |
Column length (m) | 60. | 60. | 30. | 60. | 50. |
Carrier gas | He | He | He | H2 | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
Phase thickness (μm) | 0.5 | 0.5 | 0.25 | 0.22 | |
Tstart (C) | 40. | 40. | 50. | 30. | 60. |
Tend (C) | 190. | 190. | 180. | 170. | 190. |
Heat rate (K/min) | 3. | 3. | 3. | 2. | 2. |
Initial hold (min) | 6. | 6. | 4. | 4. | |
Final hold (min) | 40. | 60. | 21. | ||
I | 1347. | 1347. | 1300. | 1320. | 1306. |
Reference | Maeztu, Sanz, et al., 2001 | Sanz, Ansorena, et al., 2001 | Lee and Shibamoto, 2000 | Buttery, Orts, et al., 1999 | Hwan and Chou, 1999 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | DB-Wax | CP-Wax 52CB | DB-Wax | PEG-20M |
Column length (m) | 30. | 60. | 50. | 60. | 50. |
Carrier gas | He | He | Nitrogen | ||
Substrate | |||||
Column diameter (mm) | 0.53 | 0.25 | 0.32 | 0.25 | 0.25 |
Phase thickness (μm) | 0.25 | 0.25 | |||
Tstart (C) | 60. | 30. | 50. | 60. | 60. |
Tend (C) | 210. | 170. | 210. | 180. | 180. |
Heat rate (K/min) | 4. | 2. | 1.5 | 2. | 2. |
Initial hold (min) | 4. | 5. | |||
Final hold (min) | 30. | 10. | |||
I | 1333. | 1320. | 1335. | 1339. | 1297. |
Reference | Iwatsuki, Mizota, et al., 1999 | Buttery and Ling, 1998 | Chyau, Lin, et al., 1997 | Sekiwa, Kubota, et al., 1997 | Kubota, Matsujage, et al., 1996 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | TC-Wax | Carbowax 20M | PEG-20M | DB-Wax |
Column length (m) | 30. | 60. | 60. | 50. | 60. |
Carrier gas | He | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.25 |
Phase thickness (μm) | 0.5 | 0.15 | |||
Tstart (C) | 40. | 80. | 60. | 60. | 40. |
Tend (C) | 210. | 240. | 180. | 180. | 200. |
Heat rate (K/min) | 3. | 3. | 2. | 2. | 2. |
Initial hold (min) | 1. | 5. | 4. | 4. | 2. |
Final hold (min) | 25. | ||||
I | 1317. | 1324. | 1308. | 1291. | 1320. |
Reference | Pollak and Berger, 1996 | Shuichi, Masazumi, et al., 1996 | Kawakami, Ganguly, et al., 1995 | Togari, Kobayashi, et al., 1995 | Umano, Hagi, et al., 1995 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Carbowax 20M | DB-Wax | DB-Wax | Carbowax 20M | Carbowax 20M |
Column length (m) | 80. | 60. | 30. | 50. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.2 | 0.25 | 0.25 | 0.33 | 0.25 |
Phase thickness (μm) | |||||
Tstart (C) | 70. | 60. | 60. | 60. | 60. |
Tend (C) | 170. | 180. | 240. | 200. | 180. |
Heat rate (K/min) | 2. | 4. | 3. | 3. | 2. |
Initial hold (min) | 4. | 10. | 4. | ||
Final hold (min) | 30. | ||||
I | 1306. | 1318. | 1303. | 1293. | 1308. |
Reference | Egolf and Jurs, 1993 | Eiserich, Macku, et al., 1992 | Hatsuko, Kazuko, et al., 1992 | Vernin, Metzger, et al., 1992 | Kawakami and Kobayashi, 1991 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | PEG-20M | DB-Wax | Carbowax 20M | FFAP | FFAP |
Column length (m) | 50. | 50. | 50. | 50. | |
Carrier gas | N2 | 30 | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.22 | 0.28 | 0.28 |
Phase thickness (μm) | |||||
Tstart (C) | 60. | 30. | 80. | 60. | 60. |
Tend (C) | 180. | 240. | 200. | 240. | 240. |
Heat rate (K/min) | 2. | 50. | 2. | 2. | 2. |
Initial hold (min) | 10. | 5. | 5. | ||
Final hold (min) | |||||
I | 1297. | 1291. | 1290. | 1297. | 1297. |
Reference | Kubota, Nakamoto, et al., 1991 | Pfannhauser, 1990 | Mihara and Masuda, 1988 | Vernin, Metzger, et al., 1988 | Vernin, Metzger, et al., 1988 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-Wax | Carbowax 20M | Carbowax 20M | Carbowax 20M | Carbowax 20M |
Column length (m) | 30. | 50. | 50. | 150. | 150. |
Carrier gas | He | Hydrogen | N2 | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.20 | 0.22 | 0.64 | 0.64 |
Phase thickness (μm) | |||||
Tstart (C) | 70. | 50. | 80. | 50. | 50. |
Tend (C) | 160. | 200. | 200. | 170. | 170. |
Heat rate (K/min) | 2. | 1. | 2. | 1. | 1. |
Initial hold (min) | 8. | 30. | 10. | ||
Final hold (min) | 35. | 60. | 60. | ||
I | 1320. | 1325. | 1290. | 1325. | 1320. |
Reference | Wong and Bernhard, 1988 | Wu, Liou, et al., 1987 | Mihara and Enomoto, 1985 | Buttery, Ling, et al., 1983 | Seifert and King, 1982 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary |
---|---|---|---|
Active phase | Carbowax 20M | Carbowax 20M | Carbowax 20M |
Column length (m) | 39. | 100. | 100. |
Carrier gas | H2 | ||
Substrate | |||
Column diameter (mm) | 0.30 | 0.25 | 0.25 |
Phase thickness (μm) | |||
Tstart (C) | 60. | 70. | 70. |
Tend (C) | 220. | 170. | 170. |
Heat rate (K/min) | 2. | 1. | 1. |
Initial hold (min) | |||
Final hold (min) | |||
I | 1312. | 1320. | 1321. |
Reference | Liardon and Ledermann, 1980 | Shibamoto and Russell, 1977 | Shibamoto and Russell, 1977 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Wanakhachornkrai and Lertsiri, 9999
Wanakhachornkrai, P.; Lertsiri, S.,
Comparison of determination method for volatile compounds in Thai soy sauce,
Analytical, Nutritional and Clinical Methods, 9999, 1-11. [all data]
Puvipirom and Chaisei, 2012
Puvipirom, J.; Chaisei, S.,
Contribution of roasted grains and seeds in aroma of oleang (Thai coffee drink),
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Budryn, Nebesny, et al., 2011
Budryn, G.; Nebesny, E.; Kula, J.; Majda, T.; Krysiak, W.,
HS-SPME/GC/MS Profiles of convectively and microwave roasted Ivory Coast Robusta coffee brews,
Czech. J. Food Sci., 2011, 29, 2, 151-160. [all data]
Moon and Shibamoto, 2010
Moon, J.-K.; Shibamoto, T.,
Formation of volatile chemicals from thermal degradation of less volatile cofee components: quinic acid, caffeic acid, and chlorogenic acid,
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Mo, Fan, et al., 2009
Mo, X.; Fan, W.; Xu, Y.,
Changes in volatile compounds of Chinese rice wine wheat qu during fermentation and storage,
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Moon and Shibamoto, 2009
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Role of roasting conditions in the profile of volatile flavor chemicals formed from coffee beans,
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Du, Clery, et al., 2008
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Volatile organic nitrogen-containing constituents in ambrette seed Abelmoschus moschatus Medik (Malvaceae),
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Marin, K.; Pozrl, T.; Zlatic, E.; Plestenjak, A.,
A new aroma index to determine the aroma quality of roasted and ground coffee during storage,
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Characterization of Pyrazines in Some Chinese Liquors and Their Approximate Concentrations, 2007
Characterization of Pyrazines in Some Chinese Liquors; Their Approximate Concentrations,
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Cros, Vandanjon, et al., 2007
Cros, S.; Vandanjon, L.; Jaouen, P.; Bourseau, P.,
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Nebesny, Budryn, et al., 2007
Nebesny, E.; Budryn, G.; Kula, J.; Majda, T.,
The effect of roasting method on headspace composition of robusta coffee bean aroma,
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Fujioka and Shibamoto, 2006
Fujioka, K.; Shibamoto, T.,
Quantitation of volatiles and nonvolatile acids in an extract from coffee beverages: correlation with antioxidant activity,
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Osada and Shibamoto, 2006
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Antioxidative activity of volatile extracts from Maillard model systems,
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Evaluation of odour-active compounds in roasted shrimp (Sergia lucens Hansen) by aroma extract dilution analysis,
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Solid-phase aroma concentrate extraction (SPACE ): a new headspace technique for more sensitive analysis of volatiles,
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Yanagimoto, Ochi, et al., 2004
Yanagimoto, K.; Ochi, H.; Lee, K.-G.; Shibamoto, T.,
Antioxidative activities of fractions obtained from brewed coffee,
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Cros, Vandanjon, et al., 2003
Cros, S.; Vandanjon, L.; Jaouen, P.; Bourseau, P.,
IMSTEC'03 Conference Proceedings, Processing of industrial mussel cooking juices by reverse osmosis: pollution abatement and aromas recovery, Universoty of New South Wales, Sydney, Australia, 2003, 6. [all data]
Tanaka, Yamauchi, et al., 2003
Tanaka, T.; Yamauchi, T.; Katsumata, R.; Kiuchi, K.,
Comparison of volatile components in commercial Itohiki-Natto by solid phase microextraction and gas chromatography,
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Wanakhachornkrai and Lertsiri, 2003
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Analytical, nutritional, and clinical methods. Comparison of determination method for volatile compounds in Thai soy sauce,
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Ito, Sugimoto, et al., 2002
Ito, Y.; Sugimoto, A.; Kakuda, T.; Kubota, K.,
Identification of potent odorants in Chinese jasmine green tea scented with flowers of Jasminum sambac,
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Qian and Reineccius, 2002
Qian, M.; Reineccius, G.,
Identification of aroma compounds in Parmigiano-Reggiano cheese by gas chromatography/olfactometry,
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Sanz, Maeztu, et al., 2002
Sanz, C.; Maeztu, L.; Zapelena, M.J.; Bello, J.; Cid, C.,
Profiles of volatile compounds and sensory analysis of three blends of coffee: influence of different proportions of Arabica and Robusta and influence of roasting coffee with sugar,
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Chyau and Mau, 2001
Chyau, C.-C.; Mau, J.-L.,
Effects of various oils on volatile compounds of deep-fried shallot flavouring,
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Maeztu, Sanz, et al., 2001
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Characterization of espresso coffee aroma by static headspace GC-MS and sensory flavor profile,
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Sanz, Ansorena, et al., 2001
Sanz, C.; Ansorena, D.; Bello, J.; Cid, C.,
Optimizing headspace temperature and time sampling for identification of volatile compounds in ground roasted Arabica coffee,
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Lee and Shibamoto, 2000
Lee, K.-G.; Shibamoto, T.,
Antioxidant properties of aroma compounds isolated from soybeans and mung beans,
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Buttery, Orts, et al., 1999
Buttery, R.G.; Orts, W.J.; Takeoka, G.R.; Nam, Y.,
Volatile flavor components of rice cakes,
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Hwan and Chou, 1999
Hwan, C.-H.; Chou, C.-C.,
Volatile components of the Chinese fermented soya bean curd as affected by the addition of ethanol in ageing solution,
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Iwatsuki, Mizota, et al., 1999
Iwatsuki, K.; Mizota, Y.; Kubota, T.; Nishimura, O.; Masuda, H.; Sotoyama, K.; Tomita, M.,
Aroma extract dilution analysis. Evluation of aroma of pasteurized and UHT processed milk by aroma extract dilution analysis,
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Buttery and Ling, 1998
Buttery, R.G.; Ling, L.C.,
Additional studies on flavor components of corn tortilla chips,
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Chyau, Lin, et al., 1997
Chyau, C.-C.; Lin, Y.-C.; Mau, J.-L.,
Storage stability of deep-fried shallot flavoring,
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Sekiwa, Kubota, et al., 1997
Sekiwa, Y.; Kubota, K.; Kobayashi, A.,
Characteristic flavor components in the brew of cooked clam (Meretrix lusoria) and the effect of storage on flavor formation,
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. [all data]
Kubota, Matsujage, et al., 1996
Kubota, K.; Matsujage, Y.; Sekiwa, Y.; Kobayashi, A.,
Identification of the characteristic volatile flavor compounds formed by cooking squid (Todarodes pacificus Steenstrup),
Food Sci. Technol., 1996, 2, 3, 163-166. [all data]
Pollak and Berger, 1996
Pollak, F.C.; Berger, R.G.,
Geosmin and Related Volatiles in Bioreactor-Cultured Streptomyces citreus CBS 109.60,
Appl. Environ. Microbiol., 1996, 62, 4, 1295-1299. [all data]
Shuichi, Masazumi, et al., 1996
Shuichi, H.; Masazumi, N.; Hiromu, K.; Kiyoshi, F.,
Comparison of volatile compounds berween the crude drugs, Onji-tsutsu and Onji-niki,
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Notes
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