2-Cyclohexen-1-ol, 2-methyl-5-(1-methylethenyl)-, acetate, cis-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedApiezon L150.1317.ter Heide, 1968N2, Embacel; Column length: 2.5 m

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-11321.Raina, Srivastava, et al., 200225. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryBP-11326.Shawl, Srivastava, et al., 200230. m/0.32 mm/0.25 μm, N2, 5. K/min, 220. C @ 13. min; Tstart: 60. C

Kovats' RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryBP-11322.Dwivedi, Khan, et al., 200425. m/0.25 mm/0.25 μm, N2; Program: 60C => 5C/min => 220C(5min) => 3C/min => 245C(5min)
CapillaryOV-11362.El-Shazly, Dorai, et al., 200230. m/0.25 mm/0.25 μm, He; Program: 44C(4min) => 3C/min => 74C => 6C/min => 134C => 12C/min => 312C
CapillaryDB-51352.Roscigno, 199830. m/0.25 mm/0.25 μm; Program: 50C(5min) => 2C/min => 250C (60min) => 2C/min => 270C => 1C/min => 290C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1365.Benkaci-Ali, Baaliouamer, et al., 200730. m/0.25 mm/0.25 μm, He, 60. C @ 8. min, 2. K/min, 250. C @ 30. min
CapillaryRTX-11342.Muselli, Rossi, et al., 200760. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryDB-51362.Yu, Liao, et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 10. min; Tstart: 50. C
CapillaryHP-5MS1381.Chorianopoulos, Kalpoutzakis, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-51362.Economakis, Skaltsa, et al., 200230. m/0.25 mm/0.25 μm, 50. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-5MS1362.Skaltsa, Mavrommati, et al., 200130. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryOV-11310.Bicchi, Rubiolo, et al., 199825. m/0.25 mm/0.3 μm, 50. C @ 1. min, 3. K/min, 200. C @ 20. min
CapillaryOV-1011311.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011315.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-Wax1738.Muselli, Rossi, et al., 200760. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 30. min; Tstart: 60. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51367.Monsef-Esfahani, Miri, et al., 201030. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 3. K/min; Tend: 240. C
CapillaryRTX-11315.Museli, Pau, et al., 200960. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryRTX-11318.Museli, Pau, et al., 200960. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillaryDB-51363.Jardin, Jham, et al., 200830. m/0.25 mm/0.25 μm, Nitrogen, 60. C @ 1. min, 3. K/min, 240. C @ 9. min
CapillaryHP-51360.Yassa and Akhani, 200830. m/0.25 mm/0.32 μm, Helium, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillarySPB-51366.Raal, Orav, et al., 200730. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-5 MS1368.Vagionas, Graikou, et al., 200730. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryHP-51360.Yassa and Akhani, 200730. m/0.25 mm/0.32 μm, He, 60. C @ 30. min, 5. K/min; Tend: 250. C
CapillaryHP-11340.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.33 μm, He, 2. K/min, 250. C @ 40. min; Tstart: 60. C
CapillaryMethyl Silicone1360.Kitchlu, Bakshi, et al., 200625. m/0.25 mm/0.25 μm, He, 90. C @ 2. min, 7. K/min; Tend: 220. C
CapillaryHP-51362.Saeidnia, Gohari, et al., 2005He, 5. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 240. C
CapillaryPE-51322.Singh, Raina, et al., 200530. m/0.32 mm/0.25 μm, H2, 60. C @ 2. min, 5. K/min, 230. C @ 4. min
CapillaryHP-5MS1362.Mimica-Dukic, Bozin, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryDB-11366.Palá-Paúl, Velasco-Negueruela, et al., 200450. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 95. C; Tend: 240. C
CapillaryDB-51395.Edris, Shalaby, et al., 2003He, 3. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 220. C
CapillaryHP-51362.Mookdasanit, Tamura, et al., 2003Helium, 2. K/min, 210. C @ 60. min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C
CapillaryCP Sil 5 CB1349.Monfared, Davarani, et al., 2002He, 5. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 220. C
CapillarySE-541364.Silva A.D., Patitucci M.L., et al., 200230. m/0.32 mm/0.25 μm, H2, 5. K/min; Tstart: 40. C; Tend: 240. C
CapillaryHP-51364.Gallori, Flamini, et al., 200130. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51362.Santos-Gomes and Fernandes-Ferreira, 200130. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 285. C
CapillaryOV-1011311.Yang, 2001N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryRTX-11346.Kalemba, 199930. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 60. C; Tend: 300. C
CapillarySPB-51363.Doneanu and Anitescu, 199850. m/0.32 mm/0.25 μm, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C
CapillaryOV-1011311.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011315.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-51362.Nezhadali and Parsa, 201030. m/0.20 mm/0.32 μm, Helium; Program: 60 0C (1 min) 3 0C/min -> 140 0C 50 0C/min -> 250 0C (3 min)
CapillaryHP-51362.Riahi, Pourbasheer, et al., 2009Column length: 30. m; Column diameter: 0.32 mm; Program: not specified
CapillaryHP-51338.Qiao, Xie, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)
CapillarySE-301351.Vinogradov, 2004Program: not specified
CapillaryOV-1011315.Yang, 2001N2; Column length: 50. m; Column diameter: 0.25 mm; Program: not specified
CapillaryMethyl Silicone1351.Zenkevich, 1999Program: not specified

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-Wax1710.Museli, Pau, et al., 200960. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 30. min; Tstart: 60. C
CapillarySupelcowax-101731.Raal, Orav, et al., 200730. m/0.25 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryHP-20M1727.Filippi, Lanfranchi, et al., 200650. m/0.2 mm/0.1 μm, He, 2. K/min, 220. C @ 30. min; Tstart: 60. C
CapillaryFFAP1725.Kitchlu, Bakshi, et al., 200620. m/0.25 mm/0.25 μm, He, 6. K/min; Tstart: 90. C; Tend: 250. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-Innowax FSC1782.Suleimenov Y.M., Atazhanova G.A., et al., 200660. m/0.25 mm/0.25 μm, He; Program: 60(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryHP-Innowax1782.Baser, Demirci, et al., 200160. m/0.25 mm/0.25 μm, He; Program: 60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

ter Heide, 1968
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Qiao, Y.; Xie, B.J.; Zhang, Y.; Zhang, Y.; FAn, G.; Yao, X.L.; Pan, S.Y., Characterization of aroma active compounds in fruit juice and peel oil of Junchen sweet orange fruit (Citrus sinensis (L.) Osbeck) by GC-MS and GC-O, Molecules, 2008, 13, 6, 1333-1344, https://doi.org/10.3390/molecules13061333 . [all data]

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Suleimenov Y.M., Atazhanova G.A., et al., 2006
Suleimenov Y.M.; Atazhanova G.A.; Ozek T.; Demirci B.; Kulyyasov A.T.; Adekenov S.M.; Baser K.H.C., Essential oil composition of three species of Achillea from Kazakhstan, Chem. Nat. Compd. (Engl. Transl.), 2006, 37, 5, 447-450, https://doi.org/10.1023/A:1014471326724 . [all data]

Baser, Demirci, et al., 2001
Baser, K.H.C.; Demirci, B.; Tabanca, N.; Özek, T.; Gören, N., Composition of the essential oils of Tanacetum armenum (DC.) Schultz Bip., T. balsamita L., T. chiliophyllum (Fisch. Mey.) Schultz Bip. var. chiliophyllum and T. haradjani (Rech. fil.) Grierson and the enantiomeric distribution of camphor and carvone, Flavour Fragr. J., 2001, 16, 3, 195-200, https://doi.org/10.1002/ffj.977 . [all data]


Notes

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