4-Aminobutanoic acid, 2TBDMS derivative
- Formula: C16H37NO2Si2
- Molecular weight: 331.6415
- IUPAC Standard InChI: InChI=1S/C16H37NO2Si2/c1-15(2,3)20(7,8)17-13-11-12-14(18)19-21(9,10)16(4,5)6/h17H,11-13H2,1-10H3
- IUPAC Standard InChIKey: OYVJHQPEPBFVSS-UHFFFAOYSA-N
- CAS Registry Number: 110024-92-5
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: Butanoic acid, 4-[(tert-butyldimethylsilyl)amino]-, tert-butyldimethylsilyl ester; γ-Aminobutyric acid, diTBDMS; γ-Aminobutyric acid, bis-TBDMS; Butanoic acid, 4-amino, O,N-bis-DMTBS; Butanoic acid, 4-amino, (2TBDMS)-; (tert-Butyldimethylsilyl) 4-[(tert-butyldimethylsilyl)amino]butanoate; Butanoic acid, 4-amino, TBDMS; γ-Aminobutyric acid, TBDMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 1745. | N/A | 30. m/0.25 mm/0.25 μm, He; Tstart: 60. C; Tend: 270. C |
| Capillary | DB-5 | 1760. | Ohie, Fu, et al., 2000 | 30. m/0.25 mm/0.25 μm, 100. C @ 1. min, 10. K/min, 300. C @ 15. min |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Methyl Silicone | 1744. | Peng, Yang, et al., 1991 | Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Ohie, Fu, et al., 2000
Ohie, T.; Fu, X.; Iga, M.; Kimura, M.; Yamaguchi, S.,
Gas chromatography-mass spectrometry with tert .-butyldimethylsilyl derivatization: use of the simplified sample preparations and the automated data system to screen for organic acidemias,
J. Chromatogr. B, 2000, 746, 1, 63-73, https://doi.org/10.1016/S0378-4347(00)00105-5
. [all data]
Peng, Yang, et al., 1991
Peng, C.T.; Yang, Z.C.; Maltby, D.,
Prediction of retention indexes. III. Silylated derivatives of polar compounds,
J. Chromatogr., 1991, 586, 1, 113-129, https://doi.org/10.1016/0021-9673(91)80029-G
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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