p-Xylene

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1HP-1HP-1
Column length (m) 30.30.30.30.30.
Carrier gas      
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Temperature (C) 0.10.20.30.40.
I 859.848.4855.2852.1850.5
ReferenceWang, Liu, et al., 2005Wang, Liu, et al., 2005Wang, Liu, et al., 2005Wang, Liu, et al., 2005Wang, Liu, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-5HP-5Methyl Silicone
Column length (m) 30.30.60.60.15.
Carrier gas     He
Substrate      
Column diameter (mm) 0.250.250.250.250.24
Phase thickness (μm) 0.250.250.250.25 
Temperature (C) 50.60.100.120.150.
I 852.3856.7883.2888.1874.28
ReferenceWang, Liu, et al., 2005Wang, Liu, et al., 2005Pérez-Parajón, Santiuste, et al., 2004Pérez-Parajón, Santiuste, et al., 2004Berezkin, Korolev, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Temperature (C) 50.60.70.80.90.
I 847.6850.2852.7855.3857.8
ReferenceWick, Siepmann, et al., 2002Wick, Siepmann, et al., 2002Wick, Siepmann, et al., 2002Wick, Siepmann, et al., 2002Wick, Siepmann, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneHP-101OV-1OV-1
Column length (m) 30.30.50.50.25.
Carrier gas HeHeH2 N2
Substrate      
Column diameter (mm) 0.250.250.20.250.2
Phase thickness (μm) 0.250.250.2 0.33
Temperature (C) 100.110.60.100.150.
I 860.9863.5857.70867.5876.
ReferenceWick, Siepmann, et al., 2002Wick, Siepmann, et al., 2002Garay, 2000Zhu, Zhang, et al., 1999Zhang, Chen, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1CP Sil 2CP Sil 2DB-1
Column length (m) 25.25.100.100. 
Carrier gas N2N2  H2
Substrate      
Column diameter (mm) 0.20.20.250.25 
Phase thickness (μm) 0.330.330.250.250.25
Temperature (C) 150.150.60.80.60.
I 876.876.863.3871.2857.1
ReferenceZhang, Chen, et al., 1997Zhang, Chen, et al., 1997Estel, Mohnke, et al., 1995Estel, Mohnke, et al., 1995Krupcik, Skacani, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase PONAPONADB-1OV-101Squalane
Column length (m)     3.
Carrier gas H2H2H2H2H2
Substrate     Silanized white support (80-100 mesh)
Column diameter (mm)      
Phase thickness (μm) 0.50.51.0.2 
Temperature (C) 60.60.60.60.100.
I 857.0857.4857.6856.9863.
ReferenceKrupcik, Skacani, et al., 1994Krupcik, Skacani, et al., 1994Krupcik, Skacani, et al., 1994Krupcik, Skacani, et al., 1994Hongwei and Zhide, 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1HP-1SPB-1
Column length (m) 25.25.25.25.60.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm) 0.200.200.200.200.75
Phase thickness (μm)      
Temperature (C) 60.60.100.100.60.
I 857.857.867.867.856.
ReferenceZhang, Li, et al., 1992Zhang, Li, et al., 1992Zhang, Li, et al., 1992Zhang, Li, et al., 1992Castello, Vezzani, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1OV-101OV-1
Column length (m) 60.60.50.50. 
Carrier gas      
Substrate      
Column diameter (mm) 0.320.320.320.25 
Phase thickness (μm)      
Temperature (C) 100.120.90.100.60.
I 866.8871.3866.7866.866.
ReferenceEngewald and Maurer, 1990Engewald and Maurer, 1990Maurer, Engewald, et al., 1990Dimov and Mekenyan, 1989Engewald, Maurer, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1SqualaneSqualaneOV-101
Column length (m) 25.25.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.310.310.220.220.20
Phase thickness (μm) 0.520.520.210.21 
Temperature (C) 45.65.50.70.100.
I 854.2859.849.1854.866.
ReferenceGuan, Kiraly, et al., 1989Guan, Kiraly, et al., 1989Guan, Kiraly, et al., 1989Guan, Kiraly, et al., 1989Matisová, Kovacicová, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedCapillaryCapillaryCapillaryCapillary
Active phase SqualaneHP-1HP-1SqualaneSqualane
Column length (m) 2.25.25.50.50.
Carrier gas HeN2N2HeHe
Substrate Risorb (0.2-0.3 mm)    
Column diameter (mm)  0.200.200.220.22
Phase thickness (μm)      
Temperature (C) 70.60.60.50.70.
I 856.879.881.848.853.1
ReferenceSafina, Poznyak, et al., 1989Bangjie, Yijian, et al., 1988Bangjie, Yijian, et al., 1988Lunskii and Paizanskaya, 1988Lunskii and Paizanskaya, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101ApolaneOV-101OV-101OV-101
Column length (m) 278.200.278.278.278.
Carrier gas N2N2H2H2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)      
Temperature (C) 120.120.100.100.100.
I 871.890.866.866.866.
ReferenceMatisová, Moravcová, et al., 1988Matisová, Moravcová, et al., 1988Matisová, Rukríglová, et al., 1988Matisová, Rukríglová, et al., 1988Matisová, Rukríglová, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SqualaneSE-54SqualaneSqualane
Column length (m) 278. 25.45.180.
Carrier gas H2 N2N2 
Substrate      
Column diameter (mm) 0.25 0.220.50.25
Phase thickness (μm)      
Temperature (C) 100.100.115.115.50.
I 866.862.886.865.848.0
ReferenceMatisová, Rukríglová, et al., 1988Nabivach and Vasiliev, 1987Bermejo, Blanco, et al., 1986Bermejo, Blanco, et al., 1986Krupcik, Cellar, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedCapillaryCapillaryCapillary
Active phase OV-101SE-30OV-101OV-101OV-101
Column length (m) 50.3.85.85.85.
Carrier gas  ArN2N2N2
Substrate  Gas Chrom Q (80-100 mesh)   
Column diameter (mm) 0.27 0.280.280.28
Phase thickness (μm)      
Temperature (C) 80.150.100.100.100.
I 863.880.866.868.866.
ReferenceWang and Sun, 1985Tiess, 1984Boneva, Papazova, et al., 1983Boneva, Papazova, et al., 1983Boneva, Papazova, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101SqualaneSqualaneDB-1
Column length (m) 85.85.100.100.60.
Carrier gas N2N2HeHe 
Substrate      
Column diameter (mm) 0.280.28  0.264
Phase thickness (μm)      
Temperature (C) 110.90.106.96.60.
I 868.863.862.859.857.1
ReferenceBoneva, Papazova, et al., 1983Boneva, Papazova, et al., 1983Kugucheva and Mashinsky, 1983Kugucheva and Mashinsky, 1983Lubeck and Sutton, 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedCapillaryCapillary
Active phase DB-1SE-30SE-30SE-30SE-30
Column length (m) 60.15.2.100.100.
Carrier gas  N2   
Substrate   Gaschrom Q  
Column diameter (mm) 0.2590.25 0.50.5
Phase thickness (μm) 1.    
Temperature (C) 60.70.100.130.80.
I 857.6860.8868.876.864.
ReferenceLubeck and Sutton, 1983Tóth, 1983Winskowski, 1983Bredael, 1982Bredael, 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101SqualaneSqualane
Column length (m) 50.50.50.50.50.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm) 0.300.300.300.250.25
Phase thickness (μm)      
Temperature (C) 100.120.140.86.96.
I 868.872.878.859.861.2
ReferenceGerasimenko and Nabivach, 1982Gerasimenko and Nabivach, 1982Gerasimenko and Nabivach, 1982Macák, Nabivach, et al., 1982Macák, Nabivach, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-1SE-30
Column length (m) 50.50.50.150.64.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.30.30.30.500.25
Phase thickness (μm)      
Temperature (C) 100.120.140.60.80.
I 867.7872.5878.3860.860.3
ReferenceGerasimenko, Kirilenko, et al., 1981Gerasimenko, Kirilenko, et al., 1981Gerasimenko, Kirilenko, et al., 1981Nijs and Jacobs, 1981Albaigés and Guardino, 1980
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 100.1.100.100.50.
Carrier gas HeHe  N2
Substrate  Chromaton N-AW-HMDS   
Column diameter (mm) 0.25 0.250.25 
Phase thickness (μm)      
Temperature (C) 80.100.50.70.86.
I 854.2858.848.3853.4858.4
ReferenceAlbaigés and Guardino, 1980Nabivach and Kirilenko, 1980Bajus, Veselý, et al., 1979Bajus, Veselý, et al., 1979Nabivach and Kirilenko, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 50.50.50.50.50.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 86.86.86.70.70.
I 858.6859.0859.3854.1854.6
ReferenceNabivach and Kirilenko, 1979Nabivach and Kirilenko, 1979Nabivach and Kirilenko, 1979Nabivach and Kirilenko, 1979Nabivach and Kirilenko, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSqualaneSqualane
Column length (m) 50.50.50.50.100.
Carrier gas N2N2  N2
Substrate      
Column diameter (mm)   0.250.250.23
Phase thickness (μm)      
Temperature (C) 86.86.86.96.100.
I 859.0861.0859.0861.2865.
ReferenceNabivach and Kirilenko, 1979Nabivach and Kirilenko, 1979Nabivach, Bur'yan, et al., 1978Nabivach, Bur'yan, et al., 1978Engewald and Wennrich, 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedPacked
Active phase SqualaneSqualaneSqualaneSE-30SE-30
Column length (m) 120.120.100.6.16.1
Carrier gas HeHeH2N2N2
Substrate    Chrom WChrom W
Column diameter (mm) 0.250.250.25  
Phase thickness (μm)      
Temperature (C) 100.100.80.110.120.
I 861.861.855.73882.886.
ReferenceLulova, Leont'eva, et al., 1976Lulova, Leont'eva, et al., 1976Soják and Rijks, 1976Mitra, Mohan, et al., 1974Mitra, Mohan, et al., 1974
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SqualaneSqualaneSqualaneSE-30Squalane
Column length (m) 50.100.100.25.510.5
Carrier gas H2N2N2HeHe
Substrate      
Column diameter (mm) 0.20.250.250.50.25
Phase thickness (μm)      
Temperature (C) 100.50.70.65.100.
I 868.849.854.857.8861.8
ReferenceMitra, Mohan, et al., 1974, 2Rijks and Cramers, 1974Rijks and Cramers, 1974Svob and Deur-Siftar, 1974Svob and Deur-Siftar, 1974
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Vacuum Grease Oil (VM-4)Vacuum Grease Oil (VM-4)Vacuum Grease Oil (VM-4)Vacuum Grease Oil (VM-4)Vacuum Grease Oil (VM-4)
Column length (m)      
Carrier gas      
Substrate      
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 35.45.50.58.68.
I 863.867.868.872.875.
ReferenceSidorov, Petrova, et al., 1972Sidorov, Petrova, et al., 1972Sidorov, Petrova, et al., 1972Sidorov, Petrova, et al., 1972Sidorov, Petrova, et al., 1972
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedCapillaryCapillaryCapillary
Active phase SqualaneApiezon LSqualaneSqualaneSqualane
Column length (m) 100.3.100.45.200.
Carrier gas  CH4 N2N2
Substrate      
Column diameter (mm) 0.25 0.250.20.2
Phase thickness (μm)      
Temperature (C) 70.100.80.92.115.
I 850.908.858.1861.865.5
ReferenceDimov and Schopov, 1971Wagaman and Smith, 1971Wallaert, 1971Krupcík, Liska, et al., 1970Krupcík, Liska, et al., 1970
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPackedPackedPacked
Active phase SqualaneSqualaneApiezon LSqualaneSqualane
Column length (m) 200.200.2.315.15.
Carrier gas N2N2N2HeHe
Substrate   DCMS-treated Chromosorb WChromosorb PChromosorb P
Column diameter (mm) 0.20.2 0.250.25
Phase thickness (μm)      
Temperature (C) 115.86.100.27.49.
I 864.9858.1894.884.850.
ReferenceSoják and Bucinská, 1970Soják and Bucinská, 1970Brown, Chapman, et al., 1968Hively and Hinton, 1968Hively and Hinton, 1968
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SqualaneSqualaneApiezon LApiezon LApiezon L
Column length (m) 15.15.10.10.10.
Carrier gas HeHe   
Substrate Chromosorb PChromosorb PChromosorb PChromosorb PChromosorb P
Column diameter (mm) 0.250.25   
Phase thickness (μm)      
Temperature (C) 67.86.100.120.140.
I 855.860.894.901.907.
ReferenceHively and Hinton, 1968Hively and Hinton, 1968Bonastre and Grenier, 1967Bonastre and Grenier, 1967Bonastre and Grenier, 1967
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase Apiezon LSqualaneSqualane
Column length (m) 10.6.6.
Carrier gas    
Substrate Chromosorb PChromosorb PChromosorb P
Column diameter (mm)    
Phase thickness (μm)    
Temperature (C) 80.120.140.
I 888.862.870.
ReferenceBonastre and Grenier, 1967Bonastre and Grenier, 1967Bonastre and Grenier, 1967
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Wang, Liu, et al., 2005
Wang, Y.; Liu, J.; Li, N.; Shi, G.; Jiang, G.; Ma, W., Preliminary study of the retention behavior for different compounds using cryogenic chromatography at different initial temperatures, Microchem. J., 2005, 81, 2, 184-190, https://doi.org/10.1016/j.microc.2005.02.003 . [all data]

Pérez-Parajón, Santiuste, et al., 2004
Pérez-Parajón, J.M.; Santiuste, J.M.; Takács, J.M., Sensitivity of the methylbenzenes and chlorobenzenes retention index to column temperature, stationary phase polarity, and number and chemical nature of substituents, J. Chromatogr. A, 2004, 1048, 2, 223-232, https://doi.org/10.1016/j.chroma.2004.07.028 . [all data]

Berezkin, Korolev, et al., 2002
Berezkin, V.G.; Korolev, A.A.; Malyukova, I.V.; Popova, T.P.; Shiryaeva, V.E.; Khotimskii, V.S., Poly[1-(trimethylsilyl)-1-propine] as chromatographic adsorbent and prospects of its application in packed and capillary columns, J. Chromatogr. A, 2002, 960, 1-2, 151-158, https://doi.org/10.1016/S0021-9673(02)00333-3 . [all data]

Wick, Siepmann, et al., 2002
Wick, C.D.; Siepmann, I.; Klotz, W.L.; Schure, M.R., Temperature effects on the retention of n-alkanes and arenes in helium-squalane gas-liquid chromatography. Experiment and molecular simulation, J. Chromatogr. A, 2002, 954, 1-2, 181-190, https://doi.org/10.1016/S0021-9673(02)00171-1 . [all data]

Garay, 2000
Garay, F., Application of a flow-tunable, serially coupled gas chromatographic capillary column system for the analysis of complex mixtures, Chromatographia Sup., 2000, 51, 1, s108-s120, https://doi.org/10.1007/BF02492792 . [all data]

Zhu, Zhang, et al., 1999
Zhu, X.; Zhang, L.; Chen, J.; Wang, L.; Che, X., The application quantitative structure-retention relationship of GC to aid MS qualitative analysis, Chin. J. Chromatogr., 1999, 17, 4, 351-353. [all data]

Zhang, Chen, et al., 1997
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Estel, Mohnke, et al., 1995
Estel, D.; Mohnke; Biermans; Rotzsche, The analysis of C4-C11 hydrocarbons in naphtha and reformate with a new apolar fused silica column, J. Hi. Res. Chromatogr., 1995, 18, 7, 403-412, https://doi.org/10.1002/jhrc.1240180703 . [all data]

Krupcik, Skacani, et al., 1994
Krupcik, J.; Skacani, I.; Benicka, E.; Sandra, P., Dependence of gas chromatographic retention data of hydrocarbons on the film thickness of the polydimethylsiloxane stationary phase, Collect. Czech. Chem. Commun., 1994, 59, 11, 2390-2396, https://doi.org/10.1135/cccc19942390 . [all data]

Hongwei and Zhide, 1992
Hongwei, Z.; Zhide, H., Utilization of total solubility parameter for calculating retention indices of alkylbenzenes, Chromatographia, 1992, 33, 11/12, 575-580, https://doi.org/10.1007/BF02262251 . [all data]

Zhang, Li, et al., 1992
Zhang, M.J.; Li, S.D.; Chen, B.J., Compositional studies of high-temperature coal tar by GC/FTIR analysis of light oil fractions, Chromatographia, 1992, 33, 3/4, 138-146, https://doi.org/10.1007/BF02275894 . [all data]

Castello, Vezzani, et al., 1991
Castello, G.; Vezzani, S.; Gerbino, T., Gas chromatographic separation and automatic identification of complex mixtures of organic solvents in indrustrial wates, J. Chromatogr., 1991, 585, 2, 273-280, https://doi.org/10.1016/0021-9673(91)85088-W . [all data]

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Maurer, Engewald, et al., 1990
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Dimov, N.; Mekenyan, Ov., Quantitative Relationships Between the Structure of Alkylbenzenes and Their Gas Chromatographic Retention on Stationary Phasses with Different Polarity, J. Chromatogr., 1989, 471, 227-236, https://doi.org/10.1016/S0021-9673(00)94170-0 . [all data]

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Notes

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