Citronellal

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Mass spectrum (electron ionization)

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Spectrum

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Additional Data

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Collection (C) 2014 copyright by the U.S. Secretary of Commerce
on behalf of the United States of America. All rights reserved.
NIST MS number 21640

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Gas Chromatography

Go To: Top, Mass spectrum (electron ionization), References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30100.1135.2Tudor, 199740. m/0.35 mm/0.35 μm
CapillaryPB-1130.1138.Engewald, Knobloch, et al., 1991Column length: 42. m; Column diameter: 0.32 mm
PackedSE-30160.1146.Hedin, Thompson, et al., 1972N2, Chromosorb W; Column length: 6.145 m
CapillarySF-96135.1143.Sakai, Maarse, et al., 1967Column length: 152. m; Column diameter: 0.8 mm

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-5MS1158.Jalali-Heravi, Zekavat, et al., 200660. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 3. K/min, 250. C @ 20. min
CapillaryHP-51157.Oliveira, Leitao, et al., 200625. m/0.2 mm/0.33 μm, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51159.Merle, Morón, et al., 200425. m/0.25 mm/0.25 μm, He, 60. C @ 6. min, 5. K/min, 180. C @ 15. min
CapillaryDB-51165.Baranauskiene, Venskutonis, et al., 200350. m/0.32 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min, 280. C @ 10. min
CapillaryBP-11133.Raina, Srivastava, et al., 200125. m/0.55 mm/0.25 μm, N2, 5. K/min, 220. C @ 15. min; Tstart: 60. C
CapillaryDB-11134.Abella, Cortella, et al., 200030. m/0.25 mm/0.25 μm, 4. K/min; Tstart: 80. C; Tend: 225. C
CapillarySE-541153.Adams, 200030. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51153.Adams, 2000, 230. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51153.Adams, 2000, 330. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51161.Rao, Rout, et al., 2000He, 2. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 180. C
CapillaryDB-51153.Adams, 199930. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryHP-51151.Sajjadi and Ghassemi, 199930. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 60. C; Tend: 280. C
CapillaryMethyl Silicone1134.Mallavarapu, Rao, et al., 1998N2, 5. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C; Tend: 220. C
CapillarySE-301138.Jantan, Ahmad, et al., 1996N2, 60. C @ 10. min, 3. K/min, 180. C @ 1. min; Column length: 25. m; Column diameter: 0.2 mm
CapillaryOV-1011134.Padrayuttawat, Tamura, et al., 199650. m/0.25 mm/0.2 μm, N2, 2. K/min, 200. C @ 60. min; Tstart: 80. C
CapillaryMethyl Silicone1122.3Rao, Rajanikanth, et al., 19894. K/min, 250. C @ 15. min; Column length: 12. m; Column diameter: 0.5 mm; Tstart: 70. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-11135.Rao, Kaul, et al., 200330. m/0.32 mm/0.25 μm, N2; Program: 60C => 5.5C/min => 220C => 3.5C/min => 245C
CapillaryHP-51153.Shellie and Marriott, 200330. m/0.25 mm/0.25 μm, He; Program: not specified
CapillaryDB-51153.Rao, Rout, et al., 2000He; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryDB-51153.Adams, 199830. m/0.26 mm/0.25 μm; Program: not specified

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryCarbowax 20M + Igepal (20:1)135.1491.Sakai, Maarse, et al., 1967He, GAS PAK F; Column length: 152. m; Column diameter: 0.8 mm

Kovats' RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M1479.Mallavarapu, Rao, et al., 1998N2, 5. K/min; Column length: 25. m; Column diameter: 0.5 mm; Tstart: 60. C; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryEquity-5MS1152.Belsito E.L., Carbone C., et al., 200730. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 10. min; Tstart: 50. C
CapillaryBP-11132.Duquesnoy, Castola, et al., 200750. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryHP-51155.Flamini, Tebano, et al., 200730. m/0.25 mm/0.25 μm, N2, 50. C @ 10. min, 5. K/min; Tend: 220. C
CapillaryDB-51152.Hongratanaworakit and Buchbauer, 200730. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51154.Silva, Barbosa, et al., 200730. m/0.22 mm/0.25 μm, He, 55. C @ 2. min, 3. K/min, 240. C @ 15. min
CapillaryDB-51150.Batista-Pereira, Fernandes, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryHP-5MS1170.Saroglou, Dorizas, et al., 200630. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C
CapillaryDB-51153.Su, Ho, et al., 200630. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryDB-51153.Su, Ho, et al., 2006, 230. m/0.25 mm/0.25 μm, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryDB-51161.Choi, 200560. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryMDN-51150.Dugo, Mondello, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-11133.Fanciullino, Gancel, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 20. min; Tstart: 40. C
CapillaryDB-51160.Fang and Qian, 200530. m/0.32 mm/1. μm, N2, 40. C @ 2. min, 4. K/min, 230. C @ 10. min
CapillaryDB-11131.Gancel, Ollitrault, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 20. min; Tstart: 40. C
CapillaryDB-11159.bin Jantan, Yalvema, et al., 200525. m/0.25 mm/0.25 μm, 60. C @ 10. min, 3. K/min, 180. C @ 10. min
CapillaryHP-5MS1148.Smadja, Rondeau, et al., 200560. m/0.2 mm/0.25 μm, He, 2. K/min, 200. C @ 10. min; Tstart: 60. C
CapillaryMega 5MS1146.Verzera, Trozzi, et al., 200530. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryRTX-51156.Dugo, Mondello, et al., 200430. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min, 300. C @ 10. min
CapillaryRSL-2001154.Ngassoum, Ousmaila, et al., 200430. m/0.32 mm/0.25 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryHP-51152.Stashenko, Jaramillo, et al., 200450. m/0.2 mm/0.2 μm, He, 40. C @ 15. min, 3. K/min, 250. C @ 40. min
CapillarySPB-11132.Chisholm, Jell, et al., 200330. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 4. K/min, 225. C @ 20. min
CapillarySPB-11132.Chisholm, Jell, et al., 200330. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 4. K/min, 225. C @ 20. min
CapillarySPB-11134.Chisholm, Wilson, et al., 200325. m/0.25 mm/0.25 μm, 35. C @ 10. min, 4. K/min; Tend: 225. C
CapillarySPB-11134.Chisholm, Wilson, et al., 200325. m/0.25 mm/0.25 μm, 35. C @ 10. min, 4. K/min; Tend: 225. C
CapillaryDB-51161.Choi, 200330. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-11131.Gancel, Ollitrault, et al., 200330. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 20. min; Tstart: 40. C
CapillaryDB-51159.Högnadóttir and Rouseff, 200330. m/0.32 mm/0.5 μm, 7. K/min, 265. C @ 5. min; Tstart: 40. C
CapillaryDB-51156.Högnadóttir and Rouseff, 200330. m/0.32 mm/0.5 μm, 7. K/min, 265. C @ 5. min; Tstart: 40. C
CapillaryDB-51159.Jantan, Ling, et al., 200330. m/0.25 mm/0.25 μm, He, 75. C @ 10. min, 3. K/min, 230. C @ 20. min
CapillaryDB-51153.bin Jantan, Yassin, et al., 200330. m/0.25 mm/0.25 μm, N2, 75. C @ 10. min, 3. K/min; Tend: 230. C
CapillaryMS51155.Shao, Marriott, et al., 200325. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 40. C; Tend: 180. C
CapillaryRTX-51152.Shellie, Marriott, et al., 200330. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min; Tend: 250. C
CapillaryHP-51155.Shellie and Marriott, 200330. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 40. C; Tend: 240. C
CapillaryMega 5MS1146.Verzera, Trozzi, et al., 200330. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryDB-11138.bin Jantan and bin Ahmad, 2002N2, 60. C @ 10. min, 3. K/min, 180. C @ 10. min; Column length: 25. m; Column diameter: 0.25 mm
CapillarySE-301138.bin Jantan, Ayop, et al., 200225. m/0.25 mm/0.25 μm, N2, 60. C @ 10. min, 3. K/min, 180. C @ 10. min
CapillaryBP-11130.Lota, de Rocca Serra, et al., 200250. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-51155.Mondello, Zappia, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min, 300. C @ 10. min
CapillaryHP-11130.Nath, Sarma, et al., 200224. m/0.32 mm/0.17 μm, He, 60. C @ 2. min, 4. K/min, 250. C @ 20. min
CapillarySPB-11134.Chisholm, Wilson, et al., 200115. m/0.25 mm/0.25 μm, 35. C @ 3. min, 6. K/min, 225. C @ 10. min
CapillaryDB-11138.Lin and Rouseff, 200130. m/0.32 mm/0.25 μm, 7. K/min, 240. C @ 5. min; Tstart: 40. C
CapillaryBP-11130.Lota, Serra, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 220. C
CapillaryHP-51152.Alonzo, Bosco, et al., 200030. m/0.20 mm/0.25 μm, He, 60. C @ 8. min, 4. K/min, 180. C @ 2. min
CapillaryDB-51137.Bartley and Jacobs, 200060. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryBP-11130.Lota, de Rocca Serra, et al., 200050. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-11130.Lota, de Rocca Serra, et al., 200050. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryRTX-51157.Mondello, Zappia, et al., 200010. m/0.1 mm/0.1 μm, He, 12.3 K/min; Tstart: 50. C; Tend: 350. C
CapillaryDB-51154.Song, Sawamura, et al., 200030. m/0.25 mm/0.25 μm, N2, 2. K/min; Tstart: 70. C; Tend: 230. C
CapillaryMega 5MS1146.Verzera, la Rosa, et al., 200030. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryMega 5MS1146.Verzera, Trozzi, et al., 200030. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 3. K/min; Tend: 240. C
CapillaryBP-11130.Lota, Serra, et al., 199950. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-11130.Lota, Serra, et al., 199950. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryDB-11146.Combariza, Tirado, et al., 199460. m/0.25 mm/0.25 μm, He, 70. C @ 5. min, 2.5 K/min, 250. C @ 15. min
CapillaryOV-1011132.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011135.Yang, Sugisawa, et al., 1992N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBPX-51160.Dharmawan, Kasapis, et al., 200730. m/0.25 mm/0.25 μm, He; Program: 35C => 4C/min => 200C => 30C/min => 300C (3min)
CapillarySE-521153.Sacchetti, Guerrini, et al., 200630. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C(10min)
Capillary5 % Phenyl methyl siloxane1153.Sacchetti, Maietti, et al., 200530. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min)
CapillaryDB-5MS1148.Zheng, Kim, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 40 (5min) => 4C/min => 140C => 4C/min => 200C (20min)
CapillarySE-521154.Frizzo, Lorenzo, et al., 200425. m/0.32 mm/0.43 μm, H2; Program: 60C(8min) => 3C/min => 180C => 20C/min => 250C(10min)
CapillarySE-521150.Lorenzo, Loayza, et al., 200325. m/0.25 mm/0.25 μm, He; Program: 60C(8min) => 3C/min => 180C => 20C/min => 230C
CapillarySE-521158.Lorenzo, Dellacassa, et al., 200025. m/0.25 mm/0.25 μm, He; Program: 60C(8min) => 3C/min => 180C => 20C/min => 230C
CapillarySE-521151.Mondello, Dugo, et al., 199560. m/0.32 mm/0.40 μm, He; Program: 45 C (6 min) 3 C/min -> 111 0C 2 C/min -> 160 C 3 C/min -> 300 C (15 min)

Van Den Dool and Kratz RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryBP-201488.Duquesnoy, Castola, et al., 200750. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1495.Mahattanatawee K., Perez-Cacho P.R., et al., 200730. m/0.32 mm/0.5 μm, He, 7. K/min, 240. C @ 5. min; Tstart: 40. C
CapillaryDB-Wax1488.Choi, 200560. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1460.Fanciullino, Gancel, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 20. min; Tstart: 40. C
CapillaryStabilwax1508.Fang and Qian, 200530. m/0.32 mm/1. μm, N2, 40. C @ 2. min, 4. K/min, 230. C @ 10. min
CapillaryDB-Wax1464.Gancel, Ollitrault, et al., 200530. m/0.25 mm/0.25 μm, He, 3. K/min, 250. C @ 20. min; Tstart: 40. C
CapillaryDB-Wax1481.Njoroge, Koaze, et al., 200560. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySupelcowax-101442.Smadja, Rondeau, et al., 200560. m/0.2 mm/0.2 μm, He, 2. K/min, 200. C @ 10. min; Tstart: 60. C
CapillaryMegawax1457.Verzera, Trozzi, et al., 200530. m/0.25 mm/0.25 μm, He, 40. C @ 6. min, 2. K/min, 220. C @ 10. min
CapillaryDB-Wax1474.Brophy, Goldsack, et al., 200460. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 32. C; Tend: 220. C
CapillaryRTX-Wax1466.Dugo, Mondello, et al., 200430. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min, 240. C @ 10. min
CapillaryInnowax1487.Chisholm, Jell, et al., 200315. m/0.25 mm/0.25 μm, He, 35. C @ 5. min, 4. K/min, 225. C @ 20. min
CapillarySupelcowax1499.Chisholm, Wilson, et al., 200325. m/0.25 mm/0.25 μm, 35. C @ 5. min, 4. K/min, 225. C @ 10. min
CapillaryDB-Wax1485.Choi, 200360. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1464.Gancel, Ollitrault, et al., 200360. m/0.32 mm/0.25 μm, H2, 1.5 K/min, 245. C @ 20. min; Tstart: 40. C
CapillaryDB-Wax1488.Högnadóttir and Rouseff, 200330. m/0.32 mm/0.5 μm, 7. K/min, 240. C @ 5. min; Tstart: 40. C
CapillaryRTX-Wax1461.Shellie, Marriott, et al., 200330. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min; Tend: 250. C
CapillaryMegawax1457.Verzera, Trozzi, et al., 200330. m/0.25 mm/0.25 μm, He, 40. C @ 6. min, 2. K/min, 220. C @ 10. min
CapillaryBP-201473.Lota, de Rocca Serra, et al., 200250. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryRTX-Wax1459.Mondello, Zappia, et al., 200230. m/0.25 mm/0.25 μm, He, 45. C @ 6. min, 3. K/min, 250. C @ 10. min
CapillaryDB-Wax1495.Lin and Rouseff, 200130. m/0.32 mm/0.50 μm, He, 7. K/min, 240. C @ 5. min; Tstart: 40. C
CapillaryBP-201473.Lota, Serra, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min; Tstart: 60. C; Tend: 220. C
CapillaryDB-Wax1489.Bartley and Jacobs, 200060. m/0.5 mm/0.32 μm, He, 40. C @ 2. min, 4. K/min, 290. C @ 5. min
CapillaryDB-Wax1485.Brophy, Goldsack, et al., 200060. m/0.53 mm/1.0 μm, He, 3. K/min; Tstart: 50. C; Tend: 220. C
CapillaryDB-Wax1486.Choi and Sawamura, 200060. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryBP-201473.Lota, de Rocca Serra, et al., 200050. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-201473.Lota, de Rocca Serra, et al., 200050. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryMegawax1457.Verzera, Trozzi, et al., 200030. m/0.25 mm/0.25 μm, He, 40. C @ 6. min, 2. K/min, 220. C @ 10. min
CapillaryBP-201473.Lota, Serra, et al., 199950. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryBP-201473.Lota, Serra, et al., 199950. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryDB-Wax1467.Möllenbeck, König, et al., 199725. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 4. K/min; Tend: 240. C
CapillaryCarbowax 20M1472.Mondello, Dugo, et al., 199560. m/0.32 mm/0.425 μm, He, 45. C @ 3. min, 3. K/min, 300. C @ 20. min
CapillaryDB-Wax1472.Combariza, Tirado, et al., 199460. m/0.25 mm/0.25 μm, He, 50. C @ 10. min, 2. K/min, 150. C @ 20. min
CapillaryCP-Wax 52CB1475.Wu and Yang, 1994H2, 50. C @ 10. min, 1.5 K/min, 200. C @ 40. min; Column length: 50. m; Column diameter: 0.32 mm
CapillaryCarbowax 20M1461.Chen and Ho, 1988He, 1.5 K/min, 225. C @ 80. min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C

Van Den Dool and Kratz RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-Wax1489.Elston, Lin, et al., 2005Program: not specified
CapillaryRTX-Wax1457.Dugo, Mondello, et al., 2004Program: not specified
CapillaryBP-201458.Lorenzo, Loayza, et al., 200325. m/0.25 mm/0.25 μm, He; Program: 40C(8min) => 3C/min => 180C => 20C/min => 230C
CapillarySupelcowax-101491.Chisholm, Wilson, et al., 2001Program: not specified
CapillaryCarbowax 20M1432.Lorenzo, Dellacassa, et al., 2000Program: not specified
CapillarySupelcowax-101450.Schieberle and Grosch, 1988He; Column length: 30. m; Column diameter: 0.32 mm; Program: 35C => 60C/min => 50C (5min) => 4C/min => 220C

Normal alkane RI, non-polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryHP-51154.Bertuzzi, Tirillini, et al., 201330. m/0.25 mm/0.25 μm, Helium, 60. C @ 3. min, 4. K/min, 300. C @ 15. min
CapillaryRTX-5 MS1161.Pinheiro, de Queiros, et al., 2013Helium, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 240. C
CapillaryRTX-11129.Bendiabdellah, El Amine Dib, et al., 201260. m/0.22 mm/0.25 μm, Helium, 2. K/min, 230. C @ 5. min; Tstart: 60. C
CapillaryCP-Sil 5 CB1150.Ameen, Usman, et al., 201125. m/0.25 mm/0.15 μm, Helium; Tstart: 50. C; Tend: 220. C
CapillarySE-30 MS1156.Menichini, Tundis, et al., 201130. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 5. K/min, 250. C @ 10. min
CapillaryDB-5 MS1157.Mesa-Arango, Betancur-Galvis, et al., 201060. m/0.25 mm/0.25 μm, Helium, 40. C @ 15. min, 5. K/min, 250. C @ 15. min
CapillarySLB-5 MS1152.Scandinaro, Tranchida, et al., 201010. m/0.10 mm/0.10 μm, Helium, 10. K/min; Tstart: 50. C; Tend: 250. C
CapillarySLB-5 MS1152.Scandinaro, Tranchida, et al., 201010. m/0.10 mm/0.10 μm, Helium, 10. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-51149.El-Massry, El-Ghorab, et al., 200930. m/0.25 mm/0.25 μm, Helium, 3. K/min, 220. C @ 40. min; Tstart: 35. C
CapillaryDB-5 MS1153.Koba, Sanda, et al., 200930. m/0.25 mm/0.25 μm, Helium, 50. C @ 5. min, 2. K/min; Tend: 250. C
CapillaryBP-11134.Ottavioli, Bighelli, et al., 200950. m/0.22 mm/0.25 μm, Helium, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-1 MS1130.Seo, Kim, et al., 200930. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 6. K/min, 250. C @ 4. min
CapillaryDB-51126.Khokra, Prakash, et al., 200830. m/0.25 mm/0.25 μm, Helium, 100. C @ 2. min, 20. K/min, 300. C @ 10. min
CapillaryHP-5 MS1150.Sahraoui, Vian, et al., 200830. m/0.25 mm/0.25 μm, Helium, 60. C @ 8. min, 2. K/min, 250. C @ 15. min
CapillaryOV-11138.Wang, Yi, et al., 200830. m/0.25 mm/0.25 μm, Helium, 6. K/min; Tstart: 65. C; Tend: 260. C
CapillaryOV-11153.Wang, Yi, et al., 200830. m/0.25 mm/0.25 μm, Helium, 6. K/min; Tstart: 65. C; Tend: 260. C
CapillaryHP-5 MS1153.Adams, Beauchamp, et al., 200730. m/0.25 mm/0.25 μm, Helium, 50. C @ 10. min, 3. K/min, 230. C @ 10. min
CapillaryHP-5MS1167.Ferhat, Meklati, et al., 200730. m/0.25 mm/0.25 μm, He, 60. C @ 8. min, 2. K/min, 250. C @ 15. min
Capillary5 % Phenyl methyl siloxane1155.Gil A., Van Baren C.M., et al., 200760. m/0.25 mm/0.25 μm, He, 3. K/min, 225. C @ 15. min; Tstart: 90. C
CapillaryCP Sil 5 CB1142.Hnawia, Cabalion, et al., 200730. m/0.25 mm/0.25 μm, N2, 5. K/min; Tstart: 50. C; Tend: 200. C
CapillaryBP-11127.Boti, Muselli, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-11130.Boti, Yao, et al., 200650. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-11131.Fanciullino, Tomi, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-11131.Fanciullino, Tomi, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryFSOT-RSL-2001153.Jirovetz, Eller, et al., 200630. m/0.32 mm/0.25 μm, Hydrogen, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-11131.Lan Phi N.T., Nishiyama C., et al., 200660. m/0.25 mm/0.25 μm, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryBP-11130.Lesueur, Ban, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-51155.Ouamba, Ouabonzi, et al., 200625. m/0.25 mm/0.15 μm, N2, 50. C @ 3. min, 4. K/min; Tend: 200. C
CapillaryDB-51153.Silva, Oliveira, et al., 200630. m/0.20 mm/0.18 μm, H2, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51152.Chagonda and Chalchat, 200550. m/0.3 mm/0.25 μm, 2. K/min; Tstart: 60. C; Tend: 240. C
CapillaryDB-51159.Chagonda and Chalchat, 2005, 225. m/0.25 mm/0.15 μm, 40. C @ 5. min, 3. K/min; Tend: 220. C
CapillaryHP-51154.Duarte, Figueira, et al., 200525. m/0.2 mm/0.33 μm, He, 3. K/min, 240. C @ 7. min; Tstart: 60. C
CapillaryMethyl Silicone1147.Ricci, Fraternale, et al., 200512.5 m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 270. C
CapillaryDB-51152.Salehi, Sefidkon, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 4. min, 3. K/min; Tend: 220. C
CapillaryHP-5MS1154.Setzer, Noletto, et al., 200530. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 3. K/min; Tend: 280. C
CapillaryHP-51152.N/A30. m/0.32 mm/0.25 μm, Helium, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryDB-11141.Choi, 200460. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryHP-5MS1153.Mimica-Dukic, Bozin, et al., 200430. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C
CapillaryNB-301135.Raal, Arak, et al., 200450. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-11141.Sawamura, Son, et al., 200460. m/0.25 mm/0.25 μm, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-11141.Sawamura, Sou, et al., 200460. m/0.25 mm/0.25 μm, Nitrogen, 70. C @ 2. min, 2. K/min; Tend: 230. C
CapillaryDB-11141.Choi, 2003, 260. m/0.25 mm/0.25 μm, He, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySE-301131.Kambouche and El-Abed, 200312. m/0.22 mm/0.3 μm, He, 3. K/min; Tstart: 70. C; Tend: 220. C
CapillaryDB-11136.Mahalwal and Ali, 200330. m/0.25 mm/0.25 μm, N2, 4. K/min; Tstart: 80. C; Tend: 250. C
CapillaryHP-51153.Mookdasanit, Tamura, et al., 2003Helium, 2. K/min, 210. C @ 60. min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 70. C
CapillaryMPS-51148.Nakahara, Alzoreky, et al., 200370. C @ 2. min, 5. K/min; Tend: 180. C
CapillaryDB-11134.Tu, Onishi, et al., 200360. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-11126.Gancel, Ollé, et al., 200230. m/0.32 mm/0.25 μm, H2, 40. C @ 20. min, 3. K/min; Tend: 245. C
CapillaryBP-51165.Doimo, 200150. m/0.25 mm/1. μm, H2, 6. K/min; Tstart: 60. C; Tend: 270. C
CapillaryBP-11130.Lota, de Rocca Serra, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryOV-1011132.Orav and Kann, 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 50. C; Tend: 250. C
CapillaryOV-1011132.Yang, 2001N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryRSL-2001139.Jirovetz, Puschmann, et al., 200060. m/0.32 mm/0.25 μm, H2, 6. K/min; Tstart: 40. C; Tend: 250. C
CapillaryDB-51152.Mitiku, Sawamura, et al., 200030. m/0.22 mm/0.25 μm, N2, 70. C @ 2. min, 4. K/min, 230. C @ 20. min
CapillaryOV-11130.Oberhofer, Nikiforov, et al., 199925. m/0.25 mm/0.25 μm, H2, 40. C @ 5. min, 3. K/min, 220. C @ 5. min
CapillaryDB-51161.Sun and Petracek, 1999H2, 32. C @ 5. min, 7. K/min, 260. C @ 5. min; Column length: 30. m; Column diameter: 0.32 mm
CapillaryHP-51155.Poiana, Sicari, et al., 199825. m/0.2 mm/0.33 μm, He, 70. C @ 8. min, 3. K/min, 290. C @ 20. min
CapillaryOV-1011146.Chacko, Jayalekshmy, et al., 199650. m/0.25 mm/0.17 μm, N2, 5. K/min; Tstart: 50. C; Tend: 220. C
CapillaryBP-11137.Rajeswara, Kaul, et al., 1996N2, 5. K/min; Column length: 25. m; Column diameter: 0.50 mm; Tstart: 60. C; Tend: 220. C
CapillaryBP-11138.Rajeswara, Kaul, et al., 1996N2, 5. K/min; Column length: 25. m; Column diameter: 0.50 mm; Tstart: 60. C; Tend: 220. C
CapillaryDB-51161.Sohounhloue, Dangou, et al., 199640. C @ 2. min, 2. K/min, 210. C @ 33. min; Column length: 30. m; Column diameter: 0.25 mm
CapillaryDB-11131.Tirado, Stashenko, et al., 199560. m/0.25 mm/0.25 μm, He, 70. C @ 5. min, 2.5 K/min; Tend: 270. C
CapillaryDB-11131.Tirado, Stashenko, et al., 199560. m/0.25 mm/0.25 μm, He, 70. C @ 5. min, 2.5 K/min; Tend: 270. C
CapillaryMethyl Silicone1137.Gopalakrishnan, Menon, et al., 199350. m/0.25 mm/0.17 μm, N2, 2. K/min; Tstart: 80. C; Tend: 200. C
CapillaryMethyl Silicone1134.Gopalakrishnan, Menon, et al., 199350. m/0.25 mm/0.17 μm, N2, 3. K/min; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011132.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011135.Tamura, Yang, et al., 19932. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryUltra-11128.Okumura, 199125. m/0.32 mm/0.25 μm, He, 3. K/min; Tstart: 80. C; Tend: 260. C
CapillaryOV-1011137.Sugisawa, Yamamoto, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011132.Sugisawa, Yang, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillaryOV-1011135.Sugisawa, Yang, et al., 1989N2, 2. K/min; Column length: 50. m; Column diameter: 0.25 mm; Tstart: 80. C; Tend: 200. C
CapillarySE-30+Igepal1138.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillarySE-30+Igepal1140.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryRTX-5 MS1153.Pinheiro, de Queiros, et al., 2013Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: not specified
CapillaryRTX-11130.Bendiabdellah, El Amine Dib, et al., 201260. m/0.22 mm/0.25 μm, Helium; Program: not specified
CapillarySiloxane, 5 % Ph1151.VOC BinBase, 2012Program: not specified
CapillaryOV-11124.Chen and Li, 2011Helium; Column length: 30. m; Column diameter: 0.25 mm; Program: 40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min)
CapillaryPolydimethyl siloxane, 5 % phenyl1151.Skogerson, Wohlgemuth, et al., 2011Program: not specified
CapillarySLB-5 MS1152.Scandinaro, Tranchida, et al., 201010. m/0.10 mm/0.10 μm, Helium; Program: not specified
CapillaryZB-1 MS1125.Al-Reza, Rahman, et al., 200930. m/0.25 mm/0.25 μm, Helium; Program: 50 0C 3 0C/min -> 150 0C (10 min) 10 0C/min -> 250 0C
CapillaryDB-11138.Delort and Jaquier, 200960. m/0.25 mm/0.25 μm, Helium; Program: 50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)
CapillaryHP-5 MS1166.Dharmawan, Kasapis, et al., 200960. m/0.32 mm/1.0 μm, Helium; Program: 120 0C 2 0C/min -> 240 0C 10 0C/min -> 270 0C (2 min)
CapillaryHP-51153.Riahi, Pourbasheer, et al., 2009Column length: 30. m; Column diameter: 0.32 mm; Program: not specified
CapillaryCB-11128.Kannaste, Vongvanich, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)
CapillaryCB-11129.Kannaste, Vongvanich, et al., 200830. m/0.25 mm/0.25 μm, Helium; Program: not specified
CapillaryDB-51153.Nivinsliene, Butkiene, et al., 200750. m/0.32 mm/0.25 μm, Helium; Program: 60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C
CapillaryCP Sil 8 CB1153.Radusiene, Judzentiene, et al., 200750. m/0.32 mm/0.25 μm, Helium; Program: 60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min)
CapillaryOV-11130.Suschke, Sporer, et al., 200730. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (2 min) 6 0C/min -> 130 0C 10 0C/min -> 300 0C
CapillaryHP-5 MS1154.Schmidt, Noletto, et al., 200630. m/0.25 mm/0.25 μm, Helium; Program: 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
CapillaryHP-5MS1156.Singh G., Maurya S., et al., 200630. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 1.5C => 185C => 9C/min => 275C (2min)
CapillaryDB-51153.Blank, Fontes, et al., 200530. m/0.25 mm/0.25 μm, He; Program: 80 0C (1 min) 3 0C/min -> 180 0C 10 0C/min -> 300 0C (3 min)
CapillaryCP Sil 8 CB1153.Butkienë, Nivinskienë, et al., 200550. m/0.32 mm/0.25 μm, He; Program: 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
CapillaryHP-51145.Riu-Aumatell, Lopez-Tamames, et al., 2005Program: not specified
CapillaryHP-51156.Singh, Maurya, et al., 2005Column length: 30. m; Column diameter: 0.32 mm; Program: 65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min)
CapillaryBPX-51153.Koba, Sanda, et al., 200430. m/0.25 mm/0.25 μm, H2; Program: 50 0C (1 min) 3 0C/min -> 150 0C 5 0C/min -> 250 0C (5 min)
CapillarySE-301128.Vinogradov, 2004Program: not specified
CapillarySE-541156.Buettner, Mestres, et al., 200330. m/0.32 mm/0.25 μm; Program: 35C (2min) => 40C/min => 50C (2min) => 6C/min => 180C => 10C/min => 230C (10min)
CapillaryHP-11132.Betts, 200012. m/0.20 mm/0.33 μm, He; Program: 40 0C 6.7 0C/min -> 87 0C (9 min) 10 0C/min -> 187 0C
CapillaryDB-11121.Baratta, Dorman, et al., 199830. m/0.25 mm/0.25 μm, He; Program: 45C => 3C/min => 175C => 15C/min => 240C (10min)
CapillaryDB-11121.da Silva, Figueiredo, et al., 199830. m/0.25 mm/0.25 μm, H2; Program: 45C => 3C/min => 175C => 15C => 240C(10min)
CapillaryDB-51153.Isidorov, Zenkevich, et al., 1997Program: not specified
CapillaryPolydimethyl siloxanes1137.Zenkevich, 1997Program: not specified
CapillaryOV-1011137.Shibamoto, 1987Program: not specified
PackedOV-1011136.Swigar and Silverstein, 1981N2, Chromosorb G 60-80mesh DMCS; Column length: 2.5 m; Program: not specified

Normal alkane RI, polar column, temperature ramp

View large format table.

Column type Active phase I Reference Comment
CapillaryTC-Wax1483.Miyazawa, Fujita, et al., 2010Helium, 40. C @ 3. min, 3. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 230. C
CapillaryBP-201486.Ottavioli, Bighelli, et al., 200950. m/0.22 mm/0.25 μm, Helium, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryInnowax1486.Seo, Kim, et al., 200930. m/0.25 mm/0.25 μm, Helium, 40. C @ 1. min, 6. K/min, 250. C @ 4. min
CapillaryHP-Innowax1488.Charoensiddhi and Anprung, 200830. m/0.25 mm/0.25 μm, Helium, 50. C @ 10. min, 15. K/min, 240. C @ 19. min
CapillaryCarbowax1478.Ferhat, Meklati, et al., 200760. m/0.2 mm/0.25 μm, He, 60. C @ 8. min, 2. K/min, 250. C @ 15. min
CapillaryPEG-20M1481.Gil A., Van Baren C.M., et al., 200760. m/0.25 mm/0.25 μm, He, 3. K/min, 225. C @ 15. min; Tstart: 90. C
CapillaryBP-201472.Boti, Muselli, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-201478.Boti, Yao, et al., 200650. m/0.22 mm/0.25 μm, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1488.Choi H.S., 200660. m/0.25 mm/0.25 μm, He, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryBP-201479.Fanciullino, Tomi, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryBP-201479.Fanciullino, Tomi, et al., 200650. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-Wax1479.Lan Phi N.T., Nishiyama C., et al., 200660. m/0.25 mm/0.25 μm, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax Etr1501.Perestrelo, Fernandes, et al., 200630. m/0.25 mm/0.25 μm, He, 40. C @ 1. min, 2. K/min, 220. C @ 10. min
CapillaryStabilwax1465.Jirovetz, Buchbauer, et al., 200530. m/0.32 mm/0.5 μm, H2, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryStabilwax1465.Jirovetz, Buchbauer, et al., 2005, 230. m/0.32 mm/0.5 μm, 40. C @ 5. min, 6. K/min, 280. C @ 5. min
CapillaryDB-Wax1492.Njoroge, Koaze, et al., 2005, 260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1492.Njoroge, Koaze, et al., 2005, 360. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillarySupelcowax-101477.Vichi, Riu-Aumatell, et al., 200530. m/0.25 mm/0.25 μm, 40. C @ 5. min, 3. K/min, 220. C @ 10. min
CapillaryZB-Wax1457.N/A30. m/0.32 mm/0.25 μm, Helium, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryZB-Wax1457.Wu, Krings, et al., 200530. m/0.32 mm/0.25 μm, He, 40. C @ 2. min, 5. K/min, 250. C @ 10. min
CapillaryDB-Wax1488.Choi, 200460. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1485.Choi, 2004, 260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1479.Jiang and Kubota, 2004He, 60. C @ 4. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 220. C
CapillaryDB-Wax1479.Jiang and Kubota, 2004He, 60. C @ 4. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 220. C
CapillaryNB-20M1480.Raal, Arak, et al., 200450. m/0.2 mm/0.25 μm, He, 2. K/min; Tstart: 50. C; Tend: 250. C
CapillaryDB-Wax1497.Sawamura, Son, et al., 200460. m/0.25 mm/0.25 μm, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1497.Sawamura, Sou, et al., 200460. m/0.25 mm/0.25 μm, Nitrogen, 70. C @ 2. min, 2. K/min; Tend: 230. C
CapillaryDB-Wax1479.Mookdasanit, Tamura, et al., 2003Helium, 2. K/min, 210. C @ 60. min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 70. C
CapillaryPEG 20M1465.Nakahara, Alzoreky, et al., 200370. C @ 2. min, 5. K/min; Tend: 180. C
CapillaryDB-Wax1489.Tu, Onishi, et al., 2003, 260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1488.Tu, Onishi, et al., 200360. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1467.Gancel, Ollé, et al., 200260. m/0.32 mm/0.25 μm, H2, 1.5 K/min, 245. C @ 20. min; Tstart: 40. C
CapillaryDB-Wax1476.Tu, Onishi, et al., 200260. m/0.25 mm/0.25 μm, N2, 70. C @ 2. min, 2. K/min, 230. C @ 20. min
CapillaryDB-Wax1486.Tu, Thanh, et al., 200260. m/0.25 mm/0.25 μm, N2, 2. K/min; Tstart: 70. C; Tend: 230. C
CapillaryDB-Wax1465.Umano, Hagi, et al., 200260. m/0.25 mm/0.25 μm, He, 40. C @ 2. min, 2. K/min; Tend: 200. C
CapillaryDB-Wax1487.Christoph, 200160. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 45. C; Tend: 240. C
CapillaryDB-Wax1469.Jiang and Kubota, 2001He, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tstart: 40. C; Tend: 220. C
CapillaryCarbowax 20M1465.Kasali, Oyedeji, et al., 200130. m/0.25 mm/0.25 μm, He, 4. K/min; Tstart: 50. C; Tend: 215. C
CapillaryBP-201473.Lota, de Rocca Serra, et al., 200150. m/0.22 mm/0.25 μm, He, 2. K/min, 230. C @ 35. min; Tstart: 60. C
CapillaryPEG-20M1480.Orav and Kann, 2001He, 2. K/min; Column length: 50. m; Column diameter: 0.2 mm; Tstart: 70. C; Tend: 220. C
CapillaryBP-201494.Bignell, Dunlop, et al., 199725. m/0.33 mm/0.5 μm, 5. K/min; Tstart: 80. C; Tend: 220. C
CapillaryCarbowax 20M1472.Tirado, Stashenko, et al., 199560. m/0.25 mm/0.25 μm, He, 50. C @ 10. min, 2. K/min, 150. C @ 20. min
CapillaryCarbowax 20M1477.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
CapillaryCarbowax 20M1477.Shibamoto and Jennings, 19771. K/min; Column length: 100. m; Column diameter: 0.25 mm; Tstart: 70. C; Tend: 170. C
PackedCarbowax 20M1491.Stancher and Pertoldi, 1967Hydrogen, Gas-Chrom Z (80-100 mesh), 4. K/min; Column length: 2. m; Tstart: 65. C; Tend: 220. C

Normal alkane RI, polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillarySupelco CO Wax-101483.Prompona, Kandylis, et al., 201260. m/0.32 mm/0.25 μm, Helium; Program: 35 0C (6 min) 2 0C/min -> 60 0C (5 min) 5 0C/min -> 200 0C 25 0C/min -> 250 0C (6 min)
CapillaryInnowax FSC1487.Kosar, Özek, et al., 200560. m/0.25 mm/0.25 μm, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryCarbowax 20M1465.Vinogradov, 2004Program: not specified
CapillaryFFAP1469.Buettner, Mestres, et al., 200330. m/0.32 mm/0.25 μm; Program: 35C (2min) => 40C/min => 60C (2min) => 6C/min => 180C => 10C/min => 230C (10min
CapillaryCarbowax 20M1472.Tirado, Stashenko, et al., 199560. m/0.25 mm/0.25 μm, He; Program: not specified
CapillaryCarbowax 20M1465.Shibamoto, 1987Program: not specified

References

Go To: Top, Mass spectrum (electron ionization), Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Silva, Barbosa, et al., 2007
Silva, C.J.; Barbosa, L.C.A.; Maltha, C.R.A.; Pinheiro, A.L.; Ismail, F.M.D., Comparative study of the essential oils of seven Melaleuca (Myrtaceae) species grown in Brazil, Flavour Fragr. J., 2007, 22, 6, 474-478, https://doi.org/10.1002/ffj.1823 . [all data]

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Batista-Pereira, L.G.; Fernandes, J.B.; Correa, A.G.; da Silva, M.F.G.F.; Vieira, P.C., Electrophysiological responses of eucalyptus brown looper Thyrinteina arnobia to essential oils of seven Eucalyptus species, J. Braz. Chem. Soc., 2006, 17, 3, 555-561, https://doi.org/10.1590/S0103-50532006000300019 . [all data]

Saroglou, Dorizas, et al., 2006
Saroglou, V.; Dorizas, N.; Kypriotakis, Z.; Skaltsa, H.D., Analysis of the essential oil composition of eight Anthemis species from Greece, J. Chromatogr. A, 2006, 1104, 1-2, 313-322, https://doi.org/10.1016/j.chroma.2005.11.087 . [all data]

Su, Ho, et al., 2006
Su, Y.C.; Ho, C.L.; Wang, E.I.C., Analysis of leaf essential oils from the indigenous five conifers of Taiwan, Flavour Fragr. J., 2006, 21, 3, 447-452, https://doi.org/10.1002/ffj.1685 . [all data]

Su, Ho, et al., 2006, 2
Su, Y.-C.; Ho, C.-L.; Wang, E.I.-C.; Chang, S.-T., Antifungal activities and chemical compositions of essential oils from leaves of four eucalypts, Taiwan J. For. Sci., 2006, 21, 1, 49-61. [all data]

Choi, 2005
Choi, H.-S., Characteristic odor components of kumquat (Fortunella japonica Swingle) peel oil, J. Agric. Food Chem., 2005, 53, 5, 1642-1647, https://doi.org/10.1021/jf040324x . [all data]

Dugo, Mondello, et al., 2005
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Fanciullino, Gancel, et al., 2005
Fanciullino, A.-L.; Gancel, A.-L.; Froelicher, Y.; Luro, F.; Ollitrault, P.; Brillouet, J.-M., Effects of Nucleo-cytoplasmic Interactions on Leaf Volatile Compounds from Citrus Somatic Diploid Hybrids, J. Agric. Food Chem., 2005, 53, 11, 4517-4523, https://doi.org/10.1021/jf0502855 . [all data]

Fang and Qian, 2005
Fang, Y.; Qian, M., Aroma compounds in Oregon Pinot Noir wine determined by aroma extract dilution analysis (AEDA), Flavour Fragr. J., 2005, 20, 1, 22-29, https://doi.org/10.1002/ffj.1551 . [all data]

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bin Jantan, Yalvema, et al., 2005
bin Jantan, I.; Yalvema, M.F.; Ahmad, N.W.; Jamal, J.A., Insecticidal activities of the leaf oils of eight Cinnamomum species against Aedes aegypti and Aedes albopictus, Pharm. Biol., 2005, 43, 6, 526-532, https://doi.org/10.1080/13880200500220771 . [all data]

Smadja, Rondeau, et al., 2005
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Verzera, Trozzi, et al., 2005
Verzera, A.; Trozzi, A.; Zappala, M.; Condurso, C.; Cotroneo, A., Essential Oil Composition of Citrus meyerii Y. Tan. and Citrus medica L. cv. Diamante and Their Lemon Hybrids, J. Agric. Food Chem., 2005, 53, 12, 4890-4894, https://doi.org/10.1021/jf047879c . [all data]

Dugo, Mondello, et al., 2004
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Chisholm, Jell, et al., 2003
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Chisholm, Wilson, et al., 2003
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Choi, 2003
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Gancel, Ollitrault, et al., 2003
Gancel, A.-L.; Ollitrault, P.; Froelicher, Y.; Tomi, F.; Jacquemond, C.; Luro, F.; Brillouet, J.-M., Leaf volatile compounds of seven citrus somatic tetraploid hybrids sharing willow leaf mandarin (Citrus deliciosa Ten.) as their common parent, J. Agric. Food Chem., 2003, 51, 20, 6006-6013, https://doi.org/10.1021/jf0345090 . [all data]

Högnadóttir and Rouseff, 2003
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Jantan, Ling, et al., 2003
Jantan, I.; Ling, Y.E.; Romli, S.; Ayop, N.; Ahmad, A.S., A comparative study of the constituents of the essential oils of three Cinnamomum species from Malaysia, J. Essent. Oil Res., 2003, 15, 6, 387-391, https://doi.org/10.1080/10412905.2003.9698618 . [all data]

bin Jantan, Yassin, et al., 2003
bin Jantan, I.; Yassin, M.S.M.; Chin, C.B.; Chen, L.L.; Sim. N.L., Antifungal activity of the essential oils of nine Zingiberaceae species, Pharm. Biol., 2003, 41, 5, 392-397, https://doi.org/10.1076/phbi.41.5.392.15941 . [all data]

Shao, Marriott, et al., 2003
Shao, Y.; Marriott, P.; Shellie, R.; Hügel, H., Solid-phase micro-extraction-comprehensive two-dimensional gas chromatography of ginger (Zingiber officinale) volatiles, Flavour Fragr. J., 2003, 18, 1, 5-12, https://doi.org/10.1002/ffj.1133 . [all data]

Shellie, Marriott, et al., 2003
Shellie, R.; Marriott, P.; Zappia, G.; Mondello, L.; Dugo, G., Interactive use of linear retention indices on polar and apolar columns with an MS-Library for reliable characterization of Australian tea tree and other Melaleuca sp. oils, J. Essent. Oil Res., 2003, 15, 5, 305-312, https://doi.org/10.1080/10412905.2003.9698597 . [all data]

Verzera, Trozzi, et al., 2003
Verzera, A.; Trozzi, A.; Gazea, F.; Cicciarelloi, G.; Cotroneo, A., Effects of rootstock on the composition of bergamot (Citrus bergamia Risso et Poiteau) essential oil, J. Agric. Food Chem., 2003, 51, 1, 206-210, https://doi.org/10.1021/jf0206872 . [all data]

bin Jantan and bin Ahmad, 2002
bin Jantan, I.; bin Ahmad, F., Chemical constituents of the essential oils of Goniothalamus malayanus Hook. f. and Thoms., Flavour Fragr. J., 2002, 17, 5, 372-374, https://doi.org/10.1002/ffj.1107 . [all data]

bin Jantan, Ayop, et al., 2002
bin Jantan, I.; Ayop, N.; Hiong, A.B.; Ahmad, A.S., Chemical composition of the essential oils of Cinnamomum cordatum Kosterm, Flavour Fragr. J., 2002, 17, 3, 212-214, https://doi.org/10.1002/ffj.1075 . [all data]

Lota, de Rocca Serra, et al., 2002
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Jacquemond, C.; Casanova, J., Volatile components of peel and leaf oils of lemon and lime species, J. Agric. Food Chem., 2002, 50, 4, 796-805, https://doi.org/10.1021/jf010924l . [all data]

Mondello, Zappia, et al., 2002
Mondello, L.; Zappia, G.; Cotroneo, A.; Bonaccorsi, I.; Chowdhury, J.U.; Yusuf, M.; Dugo, G., Studies on the essential oil-bearing plants of Bangladesh. Part VIII. Composition of some Ocimum oils O. basilicum L. var. purpurascens; O. sanctum L. green; O. sanctum L. purple; O. americanum L., citral type; O. americanum L., camphor type, Flavour Fragr. J., 2002, 17, 5, 335-340, https://doi.org/10.1002/ffj.1108 . [all data]

Nath, Sarma, et al., 2002
Nath, S.C.; Sarma, K.K.; Vajezikova, I.; Leclercq, P.A., Comparison of volatile inflorescence oils and taxonomy of certain Cymbopogon taxa described as Cymbopogon flexuosus (Nees ex Steud.) Wats., Biochem. Syst. Ecol., 2002, 30, 2, 151-162, https://doi.org/10.1016/S0305-1978(01)00066-7 . [all data]

Chisholm, Wilson, et al., 2001
Chisholm, M.G.; Wilson, M.A.; Gaskey, G.M.; Jell, J.A.; Cass, D.M., Jr., Chapter 9. The identification of aroma compounds in key lime oil using solid-phase microextraction and gas chromatography-olfactometry, Am. Chem. Soc. Symp. Ser., 2001, 782, 100-112. [all data]

Lin and Rouseff, 2001
Lin, J.; Rouseff, R.L., Characterization of aroma-impact compounds in cold-pressed grapefruit oil using time-intensity GC-olfactometry and GC-MS, Flavour Fragr. J., 2001, 16, 6, 457-463, https://doi.org/10.1002/ffj.1041 . [all data]

Lota, Serra, et al., 2001
Lota, M.-L.; Serra, D.R.; Jacquemond, C.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of sour orange, Flavour Fragr. J., 2001, 16, 2, 89-96, https://doi.org/10.1002/1099-1026(200103/04)16:2<89::AID-FFJ950>3.0.CO;2-D . [all data]

Alonzo, Bosco, et al., 2000
Alonzo, G.; Bosco, S.F.D.; Palazzolo, E.; Saiano, F.; Tusa, N., Citrus somatic hybrid leaf essential oil, Flavour Fragr. J., 2000, 15, 4, 258-262, https://doi.org/10.1002/1099-1026(200007/08)15:4<258::AID-FFJ906>3.0.CO;2-F . [all data]

Bartley and Jacobs, 2000
Bartley, J.P.; Jacobs, A.L., Effects of drying on flavour compounds in Australian-grown ginger (Zingiber officinale), J. Sci. Food Agric., 2000, 80, 2, 209-215, https://doi.org/10.1002/(SICI)1097-0010(20000115)80:2<209::AID-JSFA516>3.0.CO;2-8 . [all data]

Lota, de Rocca Serra, et al., 2000
Lota, M.-L.; de Rocca Serra, D.; Tomi, F.; Casanova, J., Chemical variability of peel and leaf essential oils of mandarins from Citrus reticulata Blanco, Biochem. Syst. Ecol., 2000, 28, 1, 61-78, https://doi.org/10.1016/S0305-1978(99)00036-8 . [all data]

Mondello, Zappia, et al., 2000
Mondello, L.; Zappia, G.; Dugo, P.; Dugo, G.; Bonaccorsi, I.; Dugo, G., Identification of complex samples by Fast-GC/MS using linear retention indices in conjunction with the MS-library, Proceedings, 23rd ISCC; CD-ROM, 2000, retrieved from http://www.richrom.com/assets/CD23PDF. [all data]

Song, Sawamura, et al., 2000
Song, H.S.; Sawamura, M.; Ito, T.; Ido, A.; Ukeda, H., Quantitative determination and characteristic flavour of daidai (Citrus aurantium L. var. cyathifera Y. Tanaka) peel oil, Flavour Fragr. J., 2000, 15, 5, 323-328, https://doi.org/10.1002/1099-1026(200009/10)15:5<323::AID-FFJ918>3.0.CO;2-J . [all data]

Verzera, la Rosa, et al., 2000
Verzera, A.; la Rosa, G.; Zappalà, M.; Cotroneo, A., Essential oil composition of different cultivars of bergamot grown in Sicily, Ital. J. Food Sci., 2000, 12, 4, 493-501. [all data]

Verzera, Trozzi, et al., 2000
Verzera, A.; Trozzi, A.; Cotroneo, A.; Lorenzo, D.; Dellacassa, E., Uruguayan essential oil. 12. Composition of Nova and Satsuma mandarin oils, J. Agric. Food Chem., 2000, 48, 7, 2903-2909, https://doi.org/10.1021/jf990734z . [all data]

Lota, Serra, et al., 1999
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Notes

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