Uridine, 3TMS derivative
- Formula: C18H36N2O6Si3
- Molecular weight: 460.7447
- IUPAC Standard InChI: InChI=1S/C18H36N2O6Si3/c1-27(2,3)23-12-13-15(25-28(4,5)6)16(26-29(7,8)9)17(24-13)20-11-10-14(21)19-18(20)22/h10-11,13,15-17H,12H2,1-9H3,(H,19,21,22)
- IUPAC Standard InChIKey: PMTYSPPFEFHVGD-UHFFFAOYSA-N
- CAS Registry Number: 10457-16-6
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: Uridine, 2',3',5'-tris-O-(trimethylsilyl)-; Uridine, 2',3',5'-tris-O-TMS; Uridine, 2',3',5'-tris(O-TMSi); Uridine, tris-TMS
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
| Column type | Active phase | Temperature (C) | I | Reference | Comment |
|---|---|---|---|---|---|
| Packed | OV-1 | 230. | 2444. | Quilliam, Ogilvie, et al., 1980 | N2, Gas-Chrom Q |
| Packed | OV-1 | 230. | 2444. | Quilliam and Westmore, 1978 | Gas Chrom Q; Column length: 1. m |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | VF-5MS | 2450. | Tretyakov, 2011 | 30. m/0.25 mm/0.25 μm, He; Program: Multi-step temperature program; T(initial)=60C; T(final)=270C |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5 | 2470. | Isidorov, Lech, et al., 2008 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min, 300. C @ 30. min; Tstart: 50. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-5 | 2469. | Isidorov, Lech, et al., 2008 | 30. m/0.25 mm/0.25 μm, Helium; Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Quilliam, Ogilvie, et al., 1980
Quilliam, M.A.; Ogilvie, K.K.; Sadana, K.L.; Westmore, J.B.,
Gas chromatographic retention data for silyl and acyl derivatives of nucleosides,
J. Chromatogr., 1980, 196, 3, 367-378, https://doi.org/10.1016/S0021-9673(00)84739-1
. [all data]
Quilliam and Westmore, 1978
Quilliam, M.A.; Westmore, J.B.,
Sterically crowded trialkylsilyl derivatives for chromatography and mass spectrometry of biologically-important compounds,
Anal. Chem., 1978, 50, 1, 59-68, https://doi.org/10.1021/ac50023a020
. [all data]
Tretyakov, 2011
Tretyakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2011. [all data]
Isidorov, Lech, et al., 2008
Isidorov, V.A.; Lech, P.; Zolciak, A.; Rusak, N.; Szczepaniak, L.,
Gas Chromatographic - nass spectrometric investigation of metabolites from the needles and roots of pine seedlings at early stages of pathogenic fungi Armillaria ostoyae attack,
Trees, 2008, 22, 4, 531-542, https://doi.org/10.1007/s00468-008-0213-z
. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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